IP Library Granted Patent US 8,415,358
Granted Patent B2
US 8,415,358 · App. 12/678,244 · Granted Apr 9, 2013

Pyrazine derivatives and their use as potassium channel modulators

Inventors: Birgitte L. Eriksen (Farum, DK); Ulrik Svane Sørensen (Søborg, DK); Charlotte Hougaard (Bagsvaerd, DK); Dan Peters (Malmö, SE); Palle Christophersen (Ballerup, DK)
Assignee: Neurosearch A/S
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Quick Facts
Patent No.
US 8,415,358
App. No.
12/678,244
Granted
Apr 9, 2013
Kind
B2
Abstract

Pyrazine compounds of the formula as well as stereoisomers thereof, N-oxides thereof, prodrugs thereof, and pharmaceutically acceptable salts thereof, wherein the variables in the formula are as defined in the specification. The compounds are useful as potassium channel modulating agents. Also, pharmaceutical compositions useful for the treatment or alleviation of diseases or disorders associated with the activity of potassium channels, and methods of using the pharmaceutical compositions.

Claims (36)

1. A pyrazine compound of Formula I

a stereoisomer thereof or a mixture of its stereoisomers, an N-oxide thereof, or a pharmaceutically acceptable salt thereof, wherein

n is 0;

X represents NH;

Y represents cycloalkyl or phenyl; which phenyl may optionally be substituted one or more times with substituents selected from the group consisting of halo and trifluoromethyl;

Het represents a heterocyclic group selected from pyrazolyl and pyrimidinyl, which pyrazolyl and pyrimidinyl may optionally be substituted one or two times with substituents selected from the group consisting of alkyl; and

R′ and R″, independent of each other, represent hydrogen, alkyl, alkoxy-alkyl, amino, amino-alkyl, alkyl-amino, N-alkyl-amino-alkyl, or N,N-dialkyl-amino-alkyl.

2. The pyrazine compound of claim 1 , a stereoisomer thereof or a mixture of its stereoisomers, an N-oxide thereof, or a pharmaceutically acceptable salt thereof, wherein Het represents pyrazolyl optionally substituted one or two times with alkyl.

3. The pyrazine compound of claim 1 , a stereoisomer thereof or a mixture of its stereoisomers, an N-oxide thereof, or a pharmaceutically acceptable salt thereof, wherein Het represents pyrimidinyl.

4. The pyrazine compound of claim 1 , a stereoisomer thereof or a mixture of its stereoisomers, an N-oxide thereof, or a pharmaceutically acceptable salt thereof, wherein Y represents phenyl which may optionally be substituted with halo.

5. The pyrazine compound of claim 1 , a stereoisomer thereof or a mixture of its stereoisomers, an N-oxide thereof, or a pharmaceutically acceptable salt thereof wherein R′ and R″, independent of each other, represent hydrogen, alkyl, alkoxy-alkyl, amino, amino-alkyl, alkyl-amino, N-alkyl-amino-alkyl, or N,N-dialkyl-amino-alkyl.

6. The pyrazine compound of claim 1 , which is

(4-Chloro-phenyl)-[6-(3,5-dimethyl-pyrazol-1-yl)-5-methoxymethyl-pyrazin-2-yl]-amine;

3-(4-Chloro-phenylamino)-5-(3,5-dimethyl-pyrazol-1-yl) -pyrazine-2-carbaldehyde oxime;

[5-Aminomethyl-6-(3,5-dimethyl-pyrazol-1-yl)-pyrazin-2-yl]-(4-chloro-phenyl)-amine;

N-[3-(4-Chloro-phenylamino)-5-(3,5-dimethyl-pyrazol-1-yl) -pyrazin-2-ylmethyl]-acetamide;

N-[5-(4-Chloro-phenylamino)-3-(3,5-dimethyl-pyrazol-1-yl) -pyrazin-2ylmethyl]acetamide;

5-(4-Chloro-phenylamino)-3-(3,5-dimethyl-pyrazol-1-yl) -pyrazine-2-amine; or

5-(4-Chloro-phenylamino)-3-(3,5-dimethyl-pyrazol-1-yl)-2-ethylamino-pyrazine; or a stereoisomer thereof or a mixture of its stereoisomers, an N-oxide thereof, or a pharmaceutically acceptable salt thereof.

7. The pyrazine compound of claim 1 , which is

(4-Chloro-phenyl)-[6-pyrazol-1-yl-pyrazin-2-yl]amine;

Cyclohexyl-[6-(3,5-dimethyl-pyrazol-1-yl)-pyrazin-2-yl]-amine;

(4-Chloro-phenyl)-[6-(3,5-dimethyl-pyrazol-1-yl)-pyrazin-2-yl]-amine;

(4-Chloro-phenyl)-(6-pyrimidin-2-yl-pyrazin-2-yl)-amine;

(4-Chloro-phenyl)-[6-(1H-pyrazol-3-yl)-pyrazin-2-yl]-amine;

(4-Chloro-phenyl)-[3 -dimethylaminomethyl-6-(3,5-dimethyl-pyrazol -1-yl)-pyrazin-2-yl]-amine;

(4-Chloro-phenyl)-[6-(3,5-dimethyl-pyrazol-1-yl)-3-methylaminomethyl-pyrazin-2yl]-amine;

(4-Chloro-phenyl)-[5-dimethylaminomethyl-6-(3,5-dimethyl-pyrazol-1-yl)-pyrazin-2yl]-amine;

(4-Chloro-phenyl)-[6-(3,5-dimethyl-pyrazol-1-yl)-5-methylaminomethyl-pyrazin-2-yl]-amine;

(4-Chloro-phenyl)-[6-(3,5-dimethyl-pyrazol-1-yl)-3-methoxymethyl-pyrazin-2-yl]-amine; or

[3-Aminomethyl-6-(3,5-dimethyl-pyrazol-1-yl)-pyrazin-2-yl]-(4-chloro-phenyl)-amine; or

a stereoisomer thereof or a mixture of its stereoisomers, an N-oxide thereof, or a pharmaceutically acceptable salt thereof.

8. The pyrazine compound of claim 7 , which is

[3-aminomethyl-6-(3,5-dimethylpyrazol-1-yl)-pyrazin-2-yl]-(4-chlorophenyl)-amine; or

a stereoisomer thereof or a mixture of its stereoisomers, an N-oxide thereof, or a pharmaceutically acceptable salt thereof.

9. A pharmaceutical composition comprising a therapeutically-effective amount of a pyrazine compound according to claim 1 , a stereoisomer thereof or a mixture of its stereoisomers, an N-oxide thereof, or a pharmaceutically-acceptable addition salt thereof, together with at least one pharmaceutically-acceptable carrier or diluent.

Assignments (7)
MERGER Recorded Jul 17, 2023
From: ATAXION, INC.
To: LUC THERAPEUTICS, INC.
Reel/Frame 064277/0494 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 17, 2023
From: CADENT THERAPEUTICS, INC.
To: NOVARTIS AG
Reel/Frame 064277/0533 →
CHANGE OF NAME Recorded Jul 17, 2023
From: LUC THERAPEUTICS, INC.
To: CADENT THERAPEUTICS, INC.
Reel/Frame 064277/0542 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 6, 2013
From: ANIONA APS
To: ATAXION, INC.
Reel/Frame 030946/0329 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 20, 2013
From: NEUROSEARCH A/S
To: ANIONA APS
Reel/Frame 030049/0894 →
CORRECTIVE ASSIGNMENT TO CORRECT THE DOCKET NUMBER. PREVIOUSLY RECORDED ON REEL 024475 FRAME 0329. ASSIGNOR(S) HEREBY CONFIRMS THE CORRECT DOCKET NUMBER IS 2815-0424PUS2. Recorded Sep 16, 2010
From: ERIKSEN, BIRGITTE L.; SORENSEN, ULRIK SVANE; HOUGAARD, CHARLOTTE; PETERS, DAN; CHRISTOPHERSEN, PALLE
To: NEUROSEARCH A/S
Reel/Frame 024997/0092 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2010
From: ERIKSEN, BIRGITTE L.; SORENSEN, ULRIK SVANE; HOUGAARD, CHARLOTTE; PETERS, DAN; CHRISTOPHERSEN, PALLE
To: NEUROSEARCH A/S
Reel/Frame 024475/0329 →
Priority Claims (1)
DK 2007 01336 · Sep 17, 2007 · national
Continuity (2)
Provisional Application 60973255 · Sep 18, 2007
Related Publication 20100286161A1 · Nov 11, 2010