IP Library Granted Patent US 8,475,995
Granted Patent B2
US 8,475,995 · App. 12/739,706 · Granted Jul 2, 2013

Toner having core-shell structure and method of preparing the same

Inventors: Dae Il Hwang (Daejeon, KR); Woo Young Yang (Daejeon, KR); Keon Il Kim (Daejeon, KR); Il Hyuk Kim (Daejeon, KR); Jae Bum Park (Daejeon, KR); Il Sun Hwang (Daejeon, KR); Jae Kwang Hwang (Daejeon, KR); Dae Woong Choi (Daejeon, KR); Dong Won Kim (Daejeon, KR); Duck Kyun Ahn (Daejeon, KR)
Assignee: Samsung Fine Chemicals Co., Ltd.
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Quick Facts
Patent No.
US 8,475,995
App. No.
12/739,706
Granted
Jul 2, 2013
Kind
B2
Abstract

A toner has a core-shell structure including a toner core portion having a resin with an active hydrogenactive hydrogen containing group, a colorant and at least one additive, and a toner shell portion surrounding the toner core portion, wherein the toner shell portion includes a cross-linked resin prepared by reaction of at least a portion of the active hydrogen containing group and the cross-linking agent.

Claims (13)

1. A method of preparing a toner, the method comprising:

forming an emulsion in which an organic solvent is dispersed in a dispersion medium in the form of a plurality of islands by mixing the dispersion medium and the organic solvent in a reactor;

forming a toner micro-suspension by adding a mixture including a resin having an active hydrogenactive hydrogen containing group, a colorant and at least one additive to the reactor and then mixing the resultant;

forming a toner core portion by removing the organic solvent from the toner micro-suspension; and

forming a toner shell portion surrounding the toner core portion by crosslinking reaction of at least a portion of the active hydrogen containing group and a cross-linking agent.

2. The method of claim 1 , further comprising:

forming a toner particle by separating a composite of the toner core portion and the toner shell portion and then washing and drying the composite.

3. The toner of claim 1 , wherein the resin having an active hydrogen containing group comprises a polyester resin including at least one selected from the group consisting of a hydroxyl group, a mercapto group, a carboxyl group, a phosphoric acid group, a sulfonate group and a sulfate group.

4. The method of claim 1 , wherein the cross-linking agent comprises an isocyanate compound or an epoxy compound.

5. The method of claim 1 , wherein the content of the cross-linking agent is in the range of 0.004 to 0.15 mol with respect to 1 mol of the active hydrogen containing group.

6. The method of claim 1 , wherein the colorant is in the form of a pigment master batch.

7. The method of claim 1 , wherein the additive comprises at least one of a charge control agent and a releasing agent.

8. The method of claim 1 , wherein the dispersion medium comprises at least one of a polar solvent, a surfactant and a thickener.

Assignments (2)
CHANGE OF NAME Recorded Mar 24, 2016
From: SAMSUNG FINE CHEMICALS CO., LTD.
To: LOTTE FINE CHEMICAL CO., LTD.
Reel/Frame 038609/0911 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 23, 2010
From: HWANG, DAE IL; YANG, WOO YOUNG; KIM, KEON IL; KIM, IL HYUK; PARK, JAE BUM; HWANG, IL SUN; HWANG, JAE KWANG; CHOI, DAE WOONG; KIM, DONG WON; AHN, DUCK KYUN
To: SAMSUNG FINE CHEMICALS CO., LTD.
Reel/Frame 024282/0959 →
Priority Claims (1)
KR 10-2007-0107416 · Oct 24, 2007 · national
Continuity (1)
Related Publication 20100232837A1 · Sep 16, 2010