IP Library › Granted Patent US 8,501,858
Granted Patent B2
US 8,501,858 · App. 11/435,471 · Granted Aug 6, 2013

Expanded graphite and products produced therefrom

Inventors: Lawrence T. Drzal (Okemos, MI); Hiroyuki Fukushima (Lansing, MI)
Assignee: Board of Trustees of Michigan State University
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Quick Facts
Patent No.
US 8,501,858
App. No.
11/435,471
Granted
Aug 6, 2013
Kind
B2
Abstract

Graphite nanoplatelets of expanded graphite and polymer composites produced therefrom are described. The graphite is expanded from an intercalated graphite by microwaves or radiofrequency waves in the presence of a gaseous atmosphere. The composites have barrier and/or conductive properties due to the expanded graphite.

Claims (18)

1. A composite composition which comprises in admixture:

(a) a polymer; and

(b) microwave or radiofrequency wave expanded graphite platelets, which were expanded from a graphite containing an intercalcant by boiling the intercalcant and which are optionally pulverized, in admixture in the polymer, wherein:

(i) the platelets are present in an amount which provides electrical conductivity properties or provides barrier properties to gases or liquids or a combination of these properties to the composite composition; and

(ii) the platelets in the composite composition have a number size distribution with an average diameter ranging from 15 μm to 200 μm.

2. The composition of claim 1 , wherein the expanded graphite platelets are present in the composite composition in an amount which provides electrical conductivity properties to the composition.

3. The composition of claim 1 , wherein the expanded graphite platelets are present in the composite composition in an amount which provides barrier properties to gases or liquids or both to the composition.

4. The composition of claim 1 , wherein the polymer comprises nylon.

5. The composition of claim 1 , wherein the platelets are about 0.5 to 40% by weight of the composition.

6. A composite composition which comprises in admixture:

(a) a polymer; and

(b) microwave or radiofrequency wave expanded graphite platelets, which were expanded from a graphite containing an intercalcant by boiling the intercalcant and are which optionally pulverized, in admixture in the polymer, wherein:

(i) the platelets are present in an amount which provides electrical conductivity properties or provides barrier properties to gases or liquids or a combination of these properties to the composite composition; and

(ii) the platelets in the composite composition have a number size distribution with an average diameter up to 1 μm.

7. The composition of claim 6 , wherein the expanded graphite platelets are present in the composite composition in an amount which provides electrical conductivity properties to the composition.

8. The composition of claim 6 , wherein the expanded graphite platelets are present in the composite composition in an amount which provides barrier properties to gases or liquids or both to the composition.

9. The composition of claim 6 , wherein the polymer comprises nylon.

10. The composition of claim 6 , wherein the platelets are about 0.5 to 40% by weight of the composition.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 16, 2006
From: DRZAL, LAWRENCE T.; FUKUSHIMA, HIROYUKI
To: TRUSTEES OF MICHIGAN STATE UNIVERSITY, BOARD OF
Reel/Frame 017909/0337 →
Continuity (3)
Continuation In Part 10659577 · Sep 10, 2003
Provisional Application 60410263 · Sep 12, 2002
Related Publication 20060231792A1 · Oct 19, 2006