IP Library › Granted Patent US 8,518,219
Granted Patent B2
US 8,518,219 · App. 12/811,589 · Granted Aug 27, 2013

Process for the treatment of organic waste and product obtained thereof

Inventors: Yefim Plopski (Be'er Sheva, IL); Alexander Rogov (Be'er Sheva, IL)
Assignee: Metal Tech Ltd.
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Quick Facts
Patent No.
US 8,518,219
App. No.
12/811,589
Granted
Aug 27, 2013
Kind
B2
Abstract

Organic waste disposal technologies are disclosed herein. A multistage processing of sewage sludge into synthetic fuel and chemical products is carried out by means of a direct thermo-chemical liquefaction process. The process enables the minimization of coke formation by utilizing steam stripping in the processing of sewage sludge.

Claims (22)

1. A multi-stage process for the treatment of sewage sludge comprising the steps of:

(a) drying sewage sludge waste to reduce a water content of the sewage sludge waste to below about 15% so as to result in dried sewage sludge;

(b) mixing the dried sewage sludge with a first solvent medium so as to result in a slurry;

(c) subjecting the slurry to a thermo-chemical liquefaction process in the presence of a second solvent medium at a temperature ranging from about 275° C. to about 375° C. and a pressure of up to about 10 atmospheres so as to result in a first slurry product comprising a gaseous product, a liquid product and a solid product;

(d) separating the first slurry product into a second slurry product and a condensable gas, wherein the condensable gas comprises water and other liquid fractions boiling out at up to about 250° C.;

(e) steam stripping the second slurry product at a temperature ranging from about 250° C. up to about 400° C., separating therefrom liquid products from solid residue so as to result in mix vapors and solid char;

(f) cooling and separating the mix vapors so as to obtain two separate streams of an oil product and water; and

(g) subjecting the oil product to vacuum distillation so as to recover oil fractions having a boiling temperature between about 250° C. to about 350° C. and oil fractions having a boiling temperature above about 350° C.

2. A multi-stage process according to claim 1 wherein the second solvent medium used in the thermo-chemical liquefaction process of step (c) is a liquid product with a boiling point above about 350° C.

3. A multi-stage process according to claim 1 wherein the first solvent medium and the second solvent medium are the same.

4. A multi-stage process according to claim 1 further comprising the step of:

(h) recirculating the oil fractions having a boiling temperature above about 350° C. to the thermo-chemical liquefaction process of step (c) for use as the second solvent medium.

5. A multi-stage process according to claim 4 wherein the recirculated solvent medium serves as a hydrogen donor in step (c).

6. A multi-stage process according to claim 1 wherein step (e) is carried out at a temperature ranging from about 300° C. up to about 350° C.

7. A multi-stage process according to claim 1 wherein in step (a) the sewage sludge waste is dried to reduce the water content of the sewage sludge waste to below about 12%.

8. A multi-stage process according to claim 1 wherein in step (b) a ratio of solvent medium to dried sewage sludge is between about 0.75:1 and about 1.5:1.

9. A multi-stage process according to claim 1 wherein in step (b) a ratio of solvent medium to dried sewage sludge is about 1:1.

10. A multi-stage process according to claim 1 wherein step (e) is carried out at a temperature of about 350° C.

11. A multi-stage process according to claim 1 wherein step (e) is carried out by mix of water steam and inert gas.

12. A multi-stage process according to claim 1 wherein the condensable gas from step (d), the solid char from step (e) and the oil fractions having a boiling temperature above about 350° C. from step (g) are combined and employed as a combustion source in heat energy generation, wherein the energy is utilized in the multi-stage process.

13. A multi-stage process according to claim 1 wherein the oil product obtained in step (g) is a fuel product comprising oil distillates having a boiling temperature up to about 250° C. (Light Oil) and oil distillates having a boiling temperature between about 250° C. to about 350° C. (Middle Distillate).

14. A multi-stage process according to claim 1 wherein the sewage sludge waste is composed of organic materials.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 19, 2014
From: METAL TECH LTD.
To: TRIDACNA LTD.
Reel/Frame 032921/0235 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 16, 2010
From: PLOPSKI, YEFIM; ROGOV, ALEXANDER
To: METAL TECH LTD.
Reel/Frame 024996/0352 →
Priority Claims (1)
IL 188541 · Jan 2, 2008 · national
Continuity (1)
Related Publication 20100314241A1 · Dec 16, 2010