IP Library › Granted Patent US 8,528,463
Granted Patent B2
US 8,528,463 · App. 13/555,664 · Granted Sep 10, 2013

Modular system for organosolv fractionation of lignocellulosic feedstock

Inventors: Christer Hallberg (Vancouver, CA); Donald O'Connor (Delta, CA); Michael Rushton (West Vancouver, CA); Edward Kendall Pye (Burnaby, CA); Gordon Gjennestad (Burnaby, CA); Alex Berlin (Burnaby, CA); John Ross MacLachlan (Burnaby, CA)
Assignee: Lignol Innovations Ltd.
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Quick Facts
Patent No.
US 8,528,463
App. No.
13/555,664
Granted
Sep 10, 2013
Kind
B2
Abstract

A modular process for organosolv fractionation of lignocellulosic feedstocks into component parts and further processing of said component parts into at least fuel-grade ethanol and four classes of lignin derivatives. The modular process includes a first processing module configured for physico-chemically digesting lignocellulosic feedstocks with an organic solvent thereby producing a cellulosic solids fraction and a liquid fraction, a second processing module configured for producing at least a fuel-grade ethanol and a first class of novel lignin derivatives from the cellulosic solids fraction, a third processing module configured for separating a second class and a third class of lignin derivatives from the liquid fraction and further processing the liquid fraction to produce a distillate and a stillage, a fourth processing module configured for separating a fourth class of lignin derivatives from the stillage and further processing the stillage to produce a sugar syrup.

Claims (45)

1. A modular system for organosolv fractionation of lignocellulosic feedstock into component parts and further processing of said component parts; the modular process comprising:

a first processing module configured for receiving, physically processing, and physico-chemically digesting a lignocellulose feedstock with a separately supplied organic solvent thereby extracting component parts therefrom said feedstock, and separating said component parts into a cellulosic solids fraction and a first liquid fraction;

a second processing module configured for receiving therein said cellulosic solids fraction and for separating therefrom at least ethanol, a first class of lignin derivatives, and a de-lignified first stillage;

a third processing module configured for separating the first liquid fraction into a second class of lignin derivatives, a third class of lignin derivatives and a filtrate, and for recovering a portion of the organic solvent from the filtrate by distillation thereby producing a second stillage; and

a fourth processing module configured for separating the second stillage into one or more of an acetic acid-containing liquid fraction, a fourth class of lignin derivatives, a sugar syrup, and a semi-solid waste material.

2. A modular system according to claim 1 , additionally provided with a fifth processing module configured for anaerobic digestion and processing of the semi-solid waste material separated by the fourth processing module, into at least a collectable biogas and an liquid effluent.

3. A modular system according to claim 1 , wherein the first processing module comprises a bin for receiving the lignocellulosic feedstock, a separating device, a digestion/extraction vessel, and a conveyance system for conveying the lignocellulosic feedstock from the bin to and through the separating device, and then into the digestion/extraction vessel.

4. A modular system according to claim 1 , wherein the first processing module is configured to continuously receive, physically process, and physico-chemically digest a lignocellulosic feedstock thereby continuously producing the cellulosic solids fraction and the first liquid fraction.

5. A modular system according to claim 1 , wherein the first processing module is configured to receive, physically process, and physico-chemically digest a batch of lignocellulosic feedstock thereby producing the cellulosic solids fraction and the first liquid fraction.

6. A modular system according to claim 1 , wherein the first processing module is provided with a temperature-controllable and pressure-controllable digestion vessel configured to:

receive therein the processed lignocellulosic feed stock at about a first end and to convey said feedstock therethrough to about a second end;

receive therein an organic solvent at about the second end, and to flow said organic solvent therethrough to about the first end;

discharge the cellulosic solids fraction through an outlet provided therefor approximate the second end; and

discharge the first liquid fraction through an outlet provided therefor approximate the first end.

7. A modular system according to claim 6 , wherein the temperature-controllable and pressure-controllable digestion vessel is configured to:

receive therein the processed lignocellulosic feed stock at about a first end and to convey said feedstock therethrough to about a second end;

receive therein an organic solvent at about the first end, and to circulate said organic solvent therethrough and thereabout;

discharge the cellulosic solids fraction through an outlet provided therefor approximate the second end; and

discharge the first liquid fraction through an outlet provided therefor approximate the second end.

8. A modular system according to claim 6 , wherein the temperature-controllable and pressure-controllable digestion vessel is configured to:

receive therein the processed lignocellulosic feed stock at about a first end and to convey said feedstock therethrough to about a second end;

receive therein an organic solvent interposed the first end and second end, and to circulate said organic solvent therethrough and thereabout;

discharge the cellulosic solids fraction through an outlet provided therefor approximate the second end; and

discharge the first liquid fraction through an outlet provided therefor approximate the first end.

9. A modular system according to claim 1 , wherein the first processing module is additionally provided with equipment configured to sequentially saturate and de-saturate the physically processed lignocellulosic feedstock prior to physico-chemically digesting said physically processed lignocellulosic feedstock.

10. A modular system according to claim 1 , wherein the second processing module comprises a plurality of equipment selected and configured for controllable and manipulable communication and cooperation for:

receiving therein the cellulosic solids fraction discharged from the first processing module;

reducing the viscosity of the cellulosic solids fraction;

enzymatic digestion of the reduced-viscosity cellulosic fraction thereby producing a liquid fraction comprising digestion products;

fermentation of the liquid fraction comprising digestion products thereby producing a beer therefrom;

distillation of the beer thereby producing a fuel-grade ethanol and a third stillage therefrom; and

separating a first class of lignin derivatives from said third stillage.

11. A modular system according to claim 10 , wherein the third stillage is recyclable for reducing the viscosity of the cellulosic solids fraction.

12. A modular system according to claim 10 , wherein the second processing module is provided with a vessel for containing therein concurrent enzymatic digestion of the reduced-viscosity cellulosic solids fraction and fermentation of the liquid fraction comprising digestion products produced therefrom.

13. A modular system according to claim 2 , wherein the fifth processing module is provided with a plurality of equipment configured for:

receiving and biologically hydrolyzing therein the semi-solid waste material separated by the fourth processing module thereby producing a second liquid fraction;

receiving and biologically acidifying therein the second fraction thereby producing a biologically acidified liquid fraction;

receiving and biologically acetifying therein the biologically acidified liquid fraction thereby producing at least acetic acid; and

receiving the at least acetic acid and biologically producing at least a biogas and a liquid effluent therefrom.

14. A modular system according to claim 13 , wherein the anaerobic digestion module is additionally configured for controllably receiving and commingling a portion of said sugar syrup separated in the fourth processing module with the a third liquid fraction.

15. A modular system according to claim 2 , additionally provided with a sixth processing module configured for receiving, fermenting and distilling therein said sugar syrup, and for separating therefrom a distillate and a fourth stillage.

16. A modular system according to claim 15 , wherein said distillate comprises at least 1,3 propanediol.

17. A modular system according to claim 15 , wherein said distillate comprises at least lactic acid.

18. A modular system according to claim 10 , wherein a portion of the sugar syrup separated in the fourth processing module is controllably delivered into the second module for production therein of ethanol therefrom.

19. A modular system according to claim 1 , wherein the ethanol is a fuel-grade ethanol.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2019
From: FIBRIA INNOVATIONS INC.
To: SUZANO CANADA INC.
Reel/Frame 051135/0966 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 21, 2017
From: LIGNOL INNOVATIONS LTD.
To: FIBRIA INNOVATIONS INC.
Reel/Frame 041327/0153 →
Continuity (6)
Division 12268417 · Nov 10, 2008
Continuation 12022831 · Jan 30, 2008
Continuation 12016932 · Jan 18, 2008
Continuation In Part 11839378 · Aug 15, 2007
Provisional Application 60941220 · May 31, 2007
Related Publication 20120289685A1 · Nov 15, 2012