IP Library Granted Patent US 8,530,409
Granted Patent B1
US 8,530,409 · App. 13/494,295 · Granted Sep 10, 2013

Stable pexiganan formulation

Inventor: Nayan Desai (Santa Rosa, CA)
Assignee: Dipexium Pharmaceuticals LLC
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Quick Facts
Patent No.
US 8,530,409
App. No.
13/494,295
Granted
Sep 10, 2013
Kind
B1
Abstract

The invention provides chemically and physically stable topical formulations of pexiganan, and methods of preparing the same.

Claims (29)

1. A topical formulation comprising pexiganan or an acid addition salt thereof comprising a first hydrophilic surfactant having an HLB value between about 12 and about 17 and a second hydrophobic surfactant having an HLB value between about 3.5 and about 5.5, wherein the first hydrophilic and second hydrophobic surfactants comprise from about 1.5% w/w to about 5.0% w/w of the formulation and the weight ratio of the first to second surfactants is such that the blended HLB is between 12.5 and about 14.5, wherein the first hydrophilic surfactant is Tween 60 and the second hydrophobic surfactant is Span 60.

2. The topical formulation of claim 1 , wherein the first hydrophilic and second hydrophobic surfactants comprise from about 2% w/w to about 4.5% w/w of the formulation.

3. The topical formulation of claim 1 , wherein the first hydrophilic and second hydrophobic surfactants comprise about 3.5% w/w of the formulation.

4. The topical formulation of claim 1 , wherein the blended HLB of the first hydrophilic and second hydrophobic surfactants is 13.6.

5. A stable topical formulation comprising:

(i) 1.05 (% w/w) pexiganan acetate

(ii) 20.0 (% w/w) propylene glycol

(iii) 0.1 (% w/w) EDTA

(iv) 7.5 (% w/w) stearyl alcohol

(v) 2.0 (% w/w) cetyl alcohol

(vi) 1.0 (% w/w) isopropyl myristate

(vii) 0.1 (% w/w) BHT

(viii) 0.43 (% w/w) Span 60

(ix) 3.07 (% w/w) Tween 60

(x) 0.1 (% w/w) Tween 80 and

(xi) (q.s.a.d.) sodium acetate buffer.

6. A stable topical formulation comprising:

(i) 1.05 (% w/w) pexiganan acetate

(ii) 20.0 (% w/w) propylene glycol

(iii) 0.1 (% w/w) EDTA

(iv) 6.0 (% w/w) stearyl alcohol

(v) 2.0 (% w/w) cetyl alcohol

(vi) 3.0 (% w/w) isopropyl myristate

(vii) 0.1 (% w/w) BHT

(viii) 0.17 (% w/w) Span 60

(ix) 3.33 (% w/w) Tween 60

(x) 0.1 (% w/w) Tween 80 and

(xi) (q.s.a.d.) sodium acetate buffer.

7. A method of treating a skin or wound infection comprising topically applying to a patient in need thereof at the site of infection an effective amount of a topical formulation of claim 1 .

Assignments (4)
SECURITY INTEREST Recorded Aug 23, 2017
From: PLX PHARMA INC.
To: SILICON VALLEY BANK
Reel/Frame 043378/0473 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE'S NAME AND ADDRESS PREVIOUSLY RECORDED ON REEL 034512 FRAME 0173. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF NAME. Recorded Jan 9, 2015
From: DIPEXIUM PHARMACEUTICALS LLC
To: DIPEXIUM PHARMACEUTICALS, INC.
Reel/Frame 034747/0877 →
CHANGE OF NAME Recorded Dec 2, 2014
From: DIPEXIUM PHARMACEUTICALS LLC
To: DIPEXIUM PHARMACEUTICALS INC.
Reel/Frame 034512/0173 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 1, 2013
From: DESAI, NAYAN
To: DIPEXIUM PHARMACEUTICALS LLC
Reel/Frame 030719/0004 →