IP Library Granted Patent US 8,540,802
Granted Patent B2
US 8,540,802 · App. 12/598,855 · Granted Sep 24, 2013

Adsorptive gas separation of multi-component gases

Inventors: Omar M. Yaghi (Los Angeles, CA); Hideki Hayashi (Kumamoto, JP); Rahul Banerjee (Maharashtra, IN)
Assignee: The Regents of the University of California
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Quick Facts
Patent No.
US 8,540,802
App. No.
12/598,855
Granted
Sep 24, 2013
Kind
B2
Abstract

The disclosure relates generally to a gas-separation system for separating one or more components from a multi-component gas using Zeolitic imidazolate or imidazolate-derived framework.

Claims (15)

1. A method of separating a component gas from a multi-component gas, comprising contacting a functionalized zeolitic framework with the multi-component gas,

wherein a component of the multi-component gas is selectively adsorbed to the functionalized zeolitic framework by electrostatically interacting with the one or more electron withdrawing group of the pore walls, thereby separating the absorbed component from other components in the multi-component gas,

wherein the functionalized zeolitic framework is ZIF-68, ZIF-69, or ZIF-70, and

wherein the method comprises either (a) separating the component gas from a multicomponent gas, where the multicomponent gas is natural gas, or (b) separating the component gas from a multi-component gas that is rich in methane and contains CO 2 , where the component gas is CO 2 and the component gas is adsorbed by the zeolitic framework.

2. The method of claim 1 , wherein the functionalized zeolitic framework comprises a plurality of pores, each of the plurality of pores comprises a sufficient number of accessible sites for atomic or molecular adsorption.

3. The method of claim 2 , wherein a surface area of a pore of the plurality of pores is greater than about 2000 m 2 /g.

4. The method of claim 2 , wherein a surface area of a pore of the plurality of pores is about 3,000-18,000 m 2 /g.

5. The method of claim 2 , wherein a surface area of a pore of the plurality of pores is about 3,000-6,000 m 2 /g.

6. The method of claim 2 , wherein a pore of the plurality of pores comprises a pore volume 0.1 to 0.99 cm 3 /cm 3 .

7. The method of claim 2 , wherein a pore of the plurality of pores comprises a pore volume of 0.4-0.5 cm 3 /cm 3 .

8. The method of claim 1 , wherein the functionalized zeolitic framework has a framework density of about 0.17 g/cm 3 .

9. The method of claim 1 , wherein the adsorbed component is selected from the group consisting of ammonia, carbon dioxide, hydrogen, amines, oxygen, argon, nitrogen, organic dyes, polycyclic organic molecules, and combinations thereof.

10. A method of separating a component from a multi-component gas, comprising: passing a multi-component gas through a functionalized zeolitic imidazolate framework comprising one or more pore walls that are polar, wherein the component gas is selectively adsorbed to the polar pore walls of the functionalized zeolitic imidazolate framework, wherein the functionalized zeolitic imidazolate framework is ZIF-68, ZIF-69, or ZIF-70, and wherein the multicomponent gas is (a) natural gas, or (b) a multi-component gas that is rich in methane and contains CO 2 , where the component gas is CO 2 and the component gas is adsorbed by the zeolitic framework.

11. The method of claim 1 or 10 , wherein the multi-component gas is natural gas.

12. The method of claim 1 or 10 , wherein the multi-component gas is rich in methane and contains CO 2 and CO 2 is the component that is being selectively adsorbed by the functionalized zeolitic framework.

Assignments (3)
CONFIRMATORY LICENSE Recorded Mar 30, 2020
From: UNIVERSITY OF CALIFORNIA LOS ANGELES
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 052263/0226 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 5, 2010
From: YAGHI, OMAR M.; HAYASHI, HIDEKI; BANERJEE, RAHUL
To: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
Reel/Frame 024341/0207 →
CONFIRMATORY LICENSE Recorded Apr 2, 2010
From: UNIVERSITY OF CALIFORNIA, LOS ANGELES
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 024178/0511 →
Continuity (2)
Provisional Application 60917611 · May 11, 2007
Related Publication 20100132549A1 · Jun 3, 2010