IP Library Granted Patent US 8,563,676
Granted Patent B2
US 8,563,676 · App. 12/663,882 · Granted Oct 22, 2013

Reactive amine catalysts for polyurethane foam

Inventors: Jennifer Koch Pratt (Round Rock, TX); Robert A. Grigsby, Jr. (Spring, TX); Gene Wiltz (The Woodlands, TX); Ernest L. Rister (Round Rock, TX); Don Ridgway (Spring, TX); Gabor Felber (Veszprem, HU)
Assignee: Huntsman Petrochemical LLC
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Quick Facts
Patent No.
US 8,563,676
App. No.
12/663,882
Granted
Oct 22, 2013
Kind
B2
Abstract

Polyurethanes made using compounds of formula A: Q-(R6)-M-(R7)-NR3R4 where Q is OH or NR 1 R 2 ; M is O or NR 5 where R 5 is R 1 or H; R 1 is alkyl or an alkylene alcohol of from 1 to 6 carbons, especially CH 3 , CH 2 CH 3 , or CH 2 CH 2 OH; R 2 is alkyl or an alkylene alcohol of from 1 to 6 carbons, especially CH 3 , CH 2 CH 3 , or —CH 2 CH 2 OH; R 3 is hydrogen or alkyl of from 1 to 6 carbons, especially H, CH 3 or CH 2 CH 3 ; R 4 is hydrogen; where R 6 is an alkylene group of from 2 to 5 carbons; and wherein R 7 is an alkylene group of from 2 to 5 carbons. Illustrative catalysts of this invention include but are not limited to N,N,N′-trimethylbis(aminoethyl)ether, dimethylaminoethoxypropylamine, and (3-aminopropyl)(2-hydroxyethyl)methylamine.

Claims (3)

1. A polyurethane formed using at least one compound of formula A, wherein the compound of formula A is (3-aminopropyl)(2-hydroxyethyl)methylamine, and wherein the at least one compound of formula A is present in the polyurethane in an amount of from about 0.03 to about 10.0 weight percent.

2. A process for the preparation of polyurethane, comprising:

reacting an organic polyisocyanate with a polyol in the presence of a catalytic amount of at least one compound of formula A, wherein the compound of formula A is (3-aminopropyl)(2-hydroxyethyl)methylamine and wherein the at least one compound of formula A is present in the polyurethane in an amount of from about 0.03 to about 10.0 weight percent.

Assignments (4)
SECURITY INTEREST Recorded May 4, 2026
From: HUNTSMAN INTERNATIONAL LLC; HUNTSMAN ADVANCED MATERIALS AMERICAS LLC; HUNTSMAN NANOCOMP LLC; HUNTSMAN PETROCHEMICAL LLC
To: CITIBANK N.A.
Reel/Frame 075498/0663 →
PATENT SECURITY AGREEMENT Recorded Mar 10, 2026
From: HUNTSMAN INTERNATIONAL LLC; HUNTSMAN ADVANCED MATERIALS AMERICAS LLC; HUNTSMAN NANOCAMP LLC; HUNTSMAN PETROCHEMICAL LLC
To: CITIBANK, N.A.
Reel/Frame 075106/0238 →
CHANGE OF NAME Recorded Jan 21, 2010
From: HUNTSMAN PETROCHEMICAL CORPORATION
To: HUNTSMAN PETROCHEMICAL LLC
Reel/Frame 023829/0766 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 4, 2010
From: PRATT, JENNIFER KOCH; GRIGSBY, ROBERT A., JR.; WILTZ, GENE, JR.; RISLER, ERNEST L., JR.; RIDGWAY, DON; FELBER, GABOR
To: HUNTSMAN PETROCHEMICAL CORPORATION
Reel/Frame 023728/0739 →
Continuity (2)
Provisional Application 60936260 · Jun 19, 2007
Related Publication 20100179297A1 · Jul 15, 2010