IP Library Granted Patent US 8,575,321
Granted Patent B2
US 8,575,321 · App. 13/333,295 · Granted Nov 5, 2013

Benzylbenzene derivatives and methods of use

Inventors: Yuanwei Chen (North Haven, CT); Huawei Cheng (Pudong New District, CN); Shengbin Li (Shanghai, CN); Yuelin Wu (Pudong New District, CN); Yan Feng (Shanghai, CN); Binhua Lv (Shanghai, CN); Baihua Xu (Shanghai, CN); Brian Seed (Boston, MA); Michael Hadd (San Diego, CA); Yanli Song (Pudong New District, CN); Jiyan Du (Shanghai, CN); Congna Wang (Pudong New District, CN); Jacques Roberge (Shanghai, CN)
Assignee: Theracos, Inc.
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Quick Facts
Patent No.
US 8,575,321
App. No.
13/333,295
Granted
Nov 5, 2013
Kind
B2
Abstract

Provided are compounds having an inhibitory effect on sodium-dependent glucose cotransporter SGLT. The invention also provides pharmaceutical compositions, methods of preparing the compounds, synthetic intermediates, and methods of using the compounds, independently or in combination with other therapeutic agents, for treating diseases and conditions which are affected by SGLT inhibition.

Claims (31)

1. A compound having the formula

wherein

V is a member selected from the group consisting of oxygen and a single bond;

W is a member selected from the group consisting of C 1 -C 6 alkylene, C 2 -C 6 alkenylene, and C 2 -C 6 alkynylene, and

wherein alkylene, alkenylene, and alkynylene groups or portions are optionally partly or completely fluorinated and are optionally mono- or disubstituted by substituents independently selected from the group consisting of chlorine, hydroxy, C 1 -C 3 alkyl, C 1 -C 3 alkoxy, C 3 -C 6 cycloalkyl, C 3 -C 6 cycloalkyloxy, C 5 -C 10 cycloalkenyl and C 5 -C 10 cycloalkenyloxy;

X is oxygen;

Y is a member selected from the group consisting of C 3 -C 10 cycloalkyl, C 5 -C 10 cycloalkenyl, (C 3 -C 10 cycloalkyl)C 1 -C 4 alkyl, (C 5 -C 10 cycloalkenyl)C 1 -C 3 alkyl, (C 3 -C 10 cycloalkyl)C 1 -C 4 alkenyl, C 3 -C 6 cycloalkylidenmethyl, (C 5 -C 10 cycloalkenyl)C 2 -C 4 alkenyl, (C 3 -C 10 cycloalkyloxy)C 1 -C 3 alkyl, and (C 5 -C 10 cycloalkenyloxy)C 1 -C 3 alkyl;

wherein alkyl, alkenyl, cycloalkyl and cycloalkenyl groups or portions are optionally partly or completely fluorinated and are optionally mono- or disubstituted by substituents independently selected from the group consisting of chlorine, hydroxy, C 1 -C 3 alkyl, C 1 -C 3 alkoxy, C 3 -C 6 cycloalkyl, C 3 -C 6 cycloalkyloxy, C 5 -C 10 cycloalkenyl, C 5 -C 10 cycloalkenyloxy, and NR b R c , and in cycloalkyl and cycloalkenyl groups or portions one or two methylene groups are optionally replaced independently of one another by O, S, CO, SO, SO 2 or NR b , and one or two methyne groups are optionally replaced by N, wherein the heterocycle formed by said optional replacement is other than heteroaryl, and wherein

when V is a single bond and W is a member selected from the group consisting of C 2 -C 6 alkenylene, and C 2 -C 6 alkynylene, then Y is other than (C 3 -C 10 cycloalkyl)C 1 -C 4 alkyl; and

when V is oxygen, W is a member selected from the group consisting of C 2 -C 6 alkenylene and C 2 -C 6 alkynylene, and Y is a member selected from the group consisting of C 3 -C 10 cycloalkyl and C 5 -C 10 cycloalkenyl, then X can also represent a single bond;

R 1 is selected from the group consisting of hydrogen, halo, hydroxy, C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, C 3 -C 10 cycloalkyl, C 5 -C 10 cycloalkenyl, C 1 -C 6 alkyloxy, C 3 -C 10 cycloalkyloxy, cyano and nitro, wherein alkyl and cycloalkyl groups or portions are optionally mono- or polysubstituted by fluorine

each R b is a member independently selected from the group consisting of H, C 1 -C 4 alkyl and (C 1 -C 4 alkyl)carbonyl, wherein alkyl groups or portions are optionally partly or completely fluorinated;

each R c is a member independently selected from the group consisting of H, C 1 -C 4 alkyl, C 3 -C 6 cycloalkyl, CHR d R e , SO 2 R d , C(O)OR d and C(O)NR d R e , wherein alkyl and cycloalkyl groups are optionally partly or completely fluorinated; and

R d and R e each independently represent H or C 1 -C 6 alkyl, wherein alkyl groups are optionally partly or completely fluorinated;

or a pharmaceutically acceptable salt thereof.

2. A compound of claim 1 , wherein

R 1 is a member selected from the group consisting of hydrogen, halo and C 1 -C 6 alkyl;

V is a member selected from the group consisting of oxygen and a single bond;

W is C 1 -C 6 alkylene;

X is oxygen; and

Y is C 3 -C 10 cycloalkyl, wherein in cycloalkyl groups or portions one or two methylene groups are optionally replaced by O.

3. A compound of claim 1 , wherein R 1 is halo.

4. A compound of claim 1 , wherein R 1 is Cl.

5. A compound of claim 1 , wherein V is oxygen.

6. A compound of claim 1 , wherein the compound has the formula:

7. A compound of claim 1 , wherein the compound is selected from the group consisting of:

(3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-((S)-tetrahydrofuran-3-yloxy)ethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol;

(3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethyl)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol;

(3R,4S,5S,6R)-2-(4-chloro-3-(4-(cyclopropoxymethyl)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol;

(3R,4S,5S,6R)-2-(4-chloro-3-(4-(3-cyclopropoxypropyl)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol; and

(2S,3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol.

Assignments (8)
CHANGE OF NAME Recorded Jan 10, 2023
From: THERACOS SUB, LLC
To: THERACOSBIO, LLC
Reel/Frame 062351/0605 →
SECURITY INTEREST Recorded Jan 19, 2016
From: THERACOS SUB, LLC
To: SEED, BRIAN
Reel/Frame 037522/0820 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2015
From: SEED, BRIAN
To: THERACOS, INC.
Reel/Frame 035703/0656 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2015
From: CHEN, YUANWEI; CHENG, HUAWEI; LI, SHENGBIN; WU, YUELIN; FENG, YAN; LV, BINHUA; XU, BAIHUA; SONG, YANLI; DU, JIYAN; WANG, CONGNA; ROBERGE, JACQUES Y.
To: EGRET PHARMA (SHANGHAI) LIMITED
Reel/Frame 035703/0684 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2015
From: EGRET PHARMA (SHANGHAI) LIMITED
To: THERACOS, INC.
Reel/Frame 035703/0712 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2015
From: HADD, MICHAEL J.
To: BIOFOCUS DPI, INC.
Reel/Frame 035703/0720 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2015
From: BIOFOCUS DPI, INC.
To: THERACOS, INC.
Reel/Frame 035703/0723 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2015
From: THERACOS, INC.
To: THERACOS SUB, LLC
Reel/Frame 035760/0114 →
Continuity (4)
Continuation 12917367 · Nov 1, 2010
Continuation 12197095 · Aug 22, 2008
Provisional Application 60957625 · Aug 23, 2007
Related Publication 20120329732A1 · Dec 27, 2012