IP Library Granted Patent US 8,697,879
Granted Patent B2
US 8,697,879 · App. 13/174,982 · Granted Apr 15, 2014

Chiral synthesis of pyrrolidine core compounds en route to neuronal nitric oxide synthase inhibitors

Inventors: Richard B. Silverman (Northbrook, IL); Fengtian Xue (Baton Rouge, LA)
Assignee: Northwestern University
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Quick Facts
Patent No.
US 8,697,879
App. No.
13/174,982
Granted
Apr 15, 2014
Kind
B2
Abstract

A chiral synthesis of pyrrolidine compounds en route to selective neuronal nitric oxide synthase inhibitors, and representative inhibitor compounds heretofore unattainable.

Claims (8)

1. A compound of a formula

wherein X 1 and X 2 are independently selected from H and F; and R is selected from H, alkyl and substituted alkyl moieties, and a salt, thereof.

2. The compound of claim 1 wherein each of X 1 and X 2 is F.

3. The compound of claim 2 wherein R is H.

4. The compound of claim 1 wherein said compound is an ammonium salt.

5. The compound of claim 4 wherein the counter ion of said ammonium salt is a conjugate base of a protic acid.

6. The compound of claim 2 selected from the (S,S) and (R,R) enantiomers.

7. The compound of claim 6 wherein said compound is the (R,R) enantiomer.

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE THE SECOND ASSIGNOR PREVIOUSLY RECORDED ON REEL 026706 FRAME 0410. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Aug 8, 2011
From: XUE, FENGTIAN
To: NORTHWESTERN UNIVERSITY
Reel/Frame 026713/0100 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2011
From: SILVERMAN, RICHARD B.; XU, FENGTIAN
To: NORTHWESTERN UNIVERSITY
Reel/Frame 026706/0410 →
CONFIRMATORY LICENSE Recorded Jul 28, 2011
From: NORTHWESTERN UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 026663/0351 →
Continuity (2)
Provisional Application 61360727 · Jul 1, 2010
Related Publication 20120004415A1 · Jan 5, 2012