IP Library › Granted Patent US 8,709,144
Granted Patent B2
US 8,709,144 · App. 12/748,926 · Granted Apr 29, 2014

Precursor sol of aluminum oxide and method for producing optical member

Inventors: Tomonari Nakayama (Yokohama, JP); Kenji Makino (Tokyo, JP)
Assignee: Canon Kabushiki Kaisha
C09D1/00C09D5/00G02B1/113G02B1/118B05D5/02
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Quick Facts
Patent No.
US 8,709,144
App. No.
12/748,926
Granted
Apr 29, 2014
Kind
B2
Abstract

A precursor sol of aluminum oxide includes a solvent and particles containing a hydrolysate of an aluminum compound and/or a condensate of the hydrolysate, in which the particles have an average particle size of 2.5 nm to 7 nm. A method for producing an optical member includes the steps of feeding the precursor sol of aluminum oxide described above onto a base to form an aluminum oxide film and immersing the aluminum oxide film in hot water with a temperature of 60° C. to 100° C. to form a textured structure comprising aluminum oxide boehmite.

Claims (16)

1. A precursor sol of aluminum oxide, comprising:

a solvent; and

particles containing a hydrolysate of an aluminum compound and/or a condensate of the hydrolysate,

wherein the particles have an average particle size of 2.5 nm to 7 nm, and

wherein the solvent contains 50% by weight to 90% by weight of a monohydric alcohol having 5 to 8 carbon atoms and 10% by weight to 50% by weight of a water-miscible solvent having a boiling point of 110° C. to 170° C.

2. The precursor sol of aluminum oxide according to claim 1 ,

wherein a particle size distribution curve of the particles includes at least one peak having a single peak top, and

wherein the at least one peak has an average particle size of 2.5 nm to 7 nm, and

the area of the peak having an average particle size of 2.5 nm to 7 nm is 90% or more of the total peak area of the particle size distribution curve.

3. The precursor sol of aluminum oxide according to claim 1 , wherein the water-miscible solvent is glycol ether.

4. The precursor sol of aluminum oxide according to claim 1 , wherein the particles are amorphous.

5. A method for producing an optical member, comprising the steps of:

(1) feeding the precursor sol of aluminum oxide according to claim 1 onto at least one surface of a base;

(2) spreading the precursor sol of aluminum oxide on the base;

(3) drying and/or firing the base to form an aluminum oxide film; and

(4) immersing the aluminum oxide film in hot water with a temperature of 60° C. to 100° C. to form a textured structure comprising aluminum oxide boehmite.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 26, 2010
From: NAKAYAMA, TOMONARI; MAKINO, KENJI
To: CANON KABUSHIKI KAISHA
Reel/Frame 024743/0475 →
Priority Claims (1)
JP 2009-087241 · Mar 31, 2009 · national
Continuity (1)
Related Publication 20100247758A1 · Sep 30, 2010