Polyvinyl butyral resin pellet, and method for producing the same
According to the present invention, a polyvinyl butyral resin pellet is provided that gives off little odor when produced and handled, as well as has a high apparent density and favorable handleability. The present invention includes a method for producing a polyvinyl butyral resin pellet including the steps of: melting polyvinyl butyral resin powder with a water content of 0.01 to 6 wt % by means of a melt extruder that has at least one vent portion for devolatilization equipped with vacuum means, and cutting the melt of the polyvinyl butyral resin after extrusion of it from the melt extruder. The present invention further includes a polyvinyl butyral resin pellet having a total content of butyl aldehyde and 2-ethyl-2-hexenal of 100 ppm or less.
1. A method for producing a polyvinyl butyral resin pellet comprising:
adjusting a water content of polyvinyl butyral resin powder to 0.01 to 6 wt.%;
melting polyvinyl butyral resin powder with a water content of 0.01 to 6 wt% in a melt extruder that includes at least one vent portion for devolatilization equipped with a vacuum and extruding a melt of polyvinyl butyral resin without adding water to said extruder during melting and extruding; and
cutting a melt of the polyvinyl butyral resin after extrusion of the melt from the melt extruder
wherein said melt of the polyvinyl butyral resin after extrusion has a total content of butyl aldehyde and 2-ethyl-2-hexenal of 100 wt. ppm or less.
2. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein the water content of the polyvinyl butyral resin powder is 0.5 to 5 wt %.
3. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein melting of the polyvinyl butyral resin powder is carried out at a temperature ranging from the melt temperature of polyvinyl butyral resin to 280° C.
4. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein the water content of the polyvinyl butyral resin powder is 1 to 4 wt %.
5. The method for producing a polyvinyl butyral resin pellet according to claim 1 , further comprising washing said polyvinyl butyral resin powder followed by fluidized drying or airborne drying, prior to melting.
6. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said vacuum is 0.05 MPa or more.
7. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said vacuum is 0.07 MPa or more.
8. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said melt of the polyvinyl butyral resin after extrusion has a total content of butyl aldehyde and 2-ethyl-2-hexenal of 50 wt. ppm or less.
9. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said melt of the polyvinyl butyral resin after extrusion has a content of butyl aldehyde of 80 wt. ppm or less.
10. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said melt of the polyvinyl butyral resin after extrusion has a content of butyl aldehyde of 40 wt. ppm or less.
11. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said melt of the polyvinyl butyral resin after extrusion has a content of 2-ethyl-2-hexenal of 60 wt. ppm or less.
12. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said melt of the polyvinyl butyral resin after extrusion has a content of 2-ethyl-2-hexenal of 10 wt. ppm or less.
13. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said melt of the polyvinyl butyral resin after extrusion has an acid value of 0.7 mg KOH/g or less.
14. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said melt of the polyvinyl butyral resin after extrusion has an acid value of 0.5 mg KOH/g or less.
15. The method for producing a polyvinyl butyral resin pellet according to claim 1 , wherein said melt of the polyvinyl butyral resin after extrusion has an acid value of 0.25 mg KOH/g or less.