IP Library › Granted Patent US 8,920,763
Granted Patent B2
US 8,920,763 · App. 13/482,254 · Granted Dec 30, 2014

Method for producing lithium carbonate

Inventors: Yuji Tanimura (Tokyo, JP); Kohei Mitsuhashi (Tokyo, JP); Ryo Kawarabuki (Tokyo, JP); Masanobu Kawata (Tokyo, JP); Yutaka Yamaguchi (Tokyo, JP)
Assignees: Nittetsu Mining Co., Ltd.; Sumitomo Corporation
C01D15/08C01D15/04
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,920,763
App. No.
13/482,254
Granted
Dec 30, 2014
Kind
B2
Abstract

The present invention relates to a method for producing lithium carbonate, the method including: mixing ammonia and carbon dioxide gas (carbonate gas) with an aqueous solution containing lithium chloride to conduct a carbonation reaction; and thereafter, recovering a produced solid by solid-liquid separation, and also relates to a method for producing high purity lithium carbonate.

Claims (10)

1. A method for producing lithium carbonate, said method comprising:

(i) thermally decomposing limestone to produce carbon dioxide (carbonate gas);

(ii) adding ammonia to an aqueous solution containing lithium chloride;

(iii) adding carbon dioxide to the resulting ammoniated aqueous solution containing lithium chloride of step (ii) to conduct a carbonation reaction to produce lithium carbonate; and

(iv) thereafter, recovering the produced lithium carbonate by solid-liquid separation,

wherein ammonia generated by reacting (a) ammonium chloride produced in step (iii) as a by-product with (b) burnt lime produced in step (i) as a by-product or hydrated product thereof is recycled as ammonia used in step (ii); and

wherein the thermal decomposition of limestone is conducted in a field where the carbonation reaction is conducted.

2. The method for producing lithium carbonate according to claim 1 , wherein the aqueous solution containing lithium chloride is prepared by concentrating a brine obtained from a salt lake.

3. The method for producing lithium carbonate according to claim 2 , wherein a lithium concentration of the brine after the concentration is from 2.0% by weight to saturated concentration.

4. A method for producing high purity lithium carbonate, said method comprising cleaning the lithium carbonate recovered in the method according to claim 1 with a highly-concentrated lithium carbonate aqueous solution.

Assignments (3)
NUNC PRO TUNC ASSIGNMENT Recorded Nov 30, 2023
From: SUMITOMO CORPORATION
To: NITTETSU MINING CO., LTD.
Reel/Frame 065711/0575 →
CHANGE OF ADDRESS Recorded Dec 6, 2018
From: SUMITOMO CORPORATION
To: SUMITOMO CORPORATION
Reel/Frame 047878/0688 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 29, 2012
From: TANIMURA, YUJI; MITSUHASHI, KOHEI; KAWARABUKI, RYO; KAWATA, MASANOBU; YAMAGUCHI, YUTAKA
To: NITTETSU MINING CO., LTD.; SUMITOMO CORPORATION
Reel/Frame 028280/0847 →
Priority Claims (1)
JP 2010-266077 · Nov 30, 2010 · national
Continuity (1)
Related Publication 20120237419A1 · Sep 20, 2012