IP Library Granted Patent US 8,956,525
Granted Patent B2
US 8,956,525 · App. 13/509,674 · Granted Feb 17, 2015

Buffered cobalt oxide catalysts

Inventors: James B. Gerken (Madison, WI); Shannon S. Stahl (Madison, WI)
Assignee: Wisconsin Alumni Research Foundation
C01B13/0207C25B1/04C25B11/0442B01J23/75B01J37/348Y02E60/366
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Quick Facts
Patent No.
US 8,956,525
App. No.
13/509,674
Granted
Feb 17, 2015
Kind
B2
Abstract

Disclosed are electrolysis catalysts formed from cobalt, oxygen and buffering electrolytes (e.g. fluoride). They can be formed as a coating on an anode by conducting an electrolysis reaction using an electrolyte containing cobalt and an anionic buffering electrolyte. The catalysts will facilitate the conversion of water to oxygen and hydrogen gas at a range of mildly acidic conditions. Alternatively, these anodes can be used with cathodes that facilitate other desirable reactions such as converting carbon dioxide to methanol.

Claims (8)

1. A method for generating a gas selected from the group consisting of oxygen and hydrogen from water via an electrolysis reaction, comprising:

using an external source of electricity to drive the electrolysis reaction where there is an anode and cathode in water, at a time when the anode comprises a substrate having a catalyst coating, the catalyst coating comprising cobalt, oxygen and an anion selected from the group consisting of trifluoromethyl sulfonamide, other perfluoroalkyl sulfonamides, perfluoro-tert-butoxide, other perfluorinated tertiary alkoxides, deprotonated hexafluoroacetone hydrate, and other anions of perfluorinated dialkyl ketone hydrates;

whereby the gas is thereby generated.

2. The method of claim 1 , wherein the gas is both hydrogen and oxygen, hydrogen is generated at the cathode, and oxygen is generated at the anode.

3. The method of claim 1 , wherein a cobalt cation is present in an aqueous solution adjacent the anode at a concentration of between 0.1 and 100 mM.

4. The method of claim 1 , wherein the anion is present in an aqueous solution adjacent the anode at a concentration between 0.01 and 2 M.

5. The method of claim 1 , wherein the substrate further comprises a tin oxide.

6. The method of claim 1 , wherein the water is part of an aqueous solution having a pH of between 3 and 6.8, and at least a portion of the aqueous solution adjacent the anode comprises water, cobalt cation and an anion electrolyte.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 14, 2017
From: GERKEN, JAMES; STAHL, SHANNON
To: WISCONSIN ALUMNI RESEARCH FOUNDATION
Reel/Frame 041567/0912 →
CONFIRMATORY LICENSE Recorded Jun 15, 2012
From: WISCONSIN ALUMNI RESEARCH FOUNDATION
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 028381/0847 →
Continuity (2)
Provisional Application 61380915 · Sep 8, 2010
Related Publication 20120305408A1 · Dec 6, 2012