IP Library › Granted Patent US 9,028,590
Granted Patent B2
US 9,028,590 · App. 13/804,142 · Granted May 12, 2015

Process and apparatus for carbon dioxide and carbonyl sulfide capture via ion exchange resins

Inventors: Anthony P. Tirio (Pittsburgh, PA); Rudolf Wagner (Cologne, DE)
Assignees: LANXESS Deutschland GmbH; LANXESS Sybron Chemicals, Inc.
B01J41/046C07C7/12C10G25/02Y02C10/08B01J49/0013B01J49/0095B01D53/02B01D53/0462B01D53/047B01D2253/206B01D2257/504B01D2258/0283B01D2258/05B01D2257/308B01J41/125B01J49/0056
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Quick Facts
Patent No.
US 9,028,590
App. No.
13/804,142
Granted
May 12, 2015
Kind
B2
Abstract

A process for the reduction of carbon dioxide and carbonyl sulfide from various types of gas emitting sources containing carbon dioxide and/or gas or liquid emitting sources containing carbonyl sulfide, using ion exchange resin.

Claims (19)

1. A process for removing carbonyl sulfide from a carbonyl sulfide containing fluid stream, the process comprising:

contacting the carbonyl sulfide containing fluid stream and a benzyl amine-co-polystrene based ion exchange resin,

sorbing at least a portion of the carbonyl sulfide from the carbonyl sulfide containing stream by the on exchange resin, thereby forming a carbonyl-sulfide-form ion exchange resin, and

desorbing the attached carbonyl sulfide from the carbonyl-sulfide-form ion exchange resin by one of: heat, or heat and vacuum, thereby increasing the capacity of the resin to re-adsorb carbonyl sulfide.

2. The process according to claim 1 , wherein the carbonyl sulfide stream is a gaseous stream.

3. The process according to claim 2 , wherein the gaseous stream is from a synthesis gas stream or a light hydrocarbon gas stream.

4. The process according to claim 3 , wherein the light hydrocarbon gas stream is a propane, propylene, ethane, and/or ethylene gas stream.

5. The process according to claim 1 , wherein the carbonyl sulfide stream is a liquid stream.

6. The process according to claim 5 , wherein the liquid stream is a liquefied petroleum gas stream.

7. The process according to claim 6 , wherein the liquefied petroleum gas stream is a propane, propylene, ethane, and/or ethylene liquefied stream.

8. The process accordingly to claim 1 , wherein the benzyl amine-co-polystrene based resin is produced by a phthalimide addition process.

9. The process according to claim 1 , wherein the carbonyl sulfide sorbing and desorbing steps are primarily thermal swing driven operation steps.

10. The process according to claim 1 , wherein the carbonyl sulfide sorbing and desorbing steps are driven by a thermal swing operation in combination with a pressure swing operation.

11. The process according to claim 1 , wherein said ion exchange resin has a water content between about 1% by weight and 25% by weight, based on the total weight of the resin.

12. The process according to claim 1 , wherein said ion exchange resin has a water content of greater than about 5% by weight and less than about 15% by weight, based on the total weight of the resin.

13. The process according to claim 1 , wherein the on exchange resin comprises beads having a mean particle size of approximately 10 to 1000 μm.

14. The process according to claim 1 , wherein the on exchange resin comprises beads having a mean particle size of approximately 100 to 1000 μm.

15. The process according to claim 1 , wherein the ion exchange resin comprises beads having a mean particle size of approximately 100 to 700 μm.

16. The process according to claim 1 , wherein the ion exchange resin comprises beads haying a uniformity coefficient of the distribution less than or equal to 1.2.

Assignments (3)
MERGER Recorded Nov 14, 2019
From: LANXESS SYBRON CHEMICALS INC.
To: LANXESS CORPORATION
Reel/Frame 051004/0314 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE PREVIOUSLY RECORDED ON REEL 030213 FRAME 0980. ASSIGNOR(S) HEREBY CONFIRMS THE CORRECTIVE ASSIGNMENT TO RE-RECORD ASSIGNMENT PREVIOUSLY RECORDED AT 030213/0980 TO SHOW TWO (2) ASSIGNEES. Recorded Apr 24, 2013
From: TIRIO, ANTHONY P; WAGNER, RUDOLF
To: LANXESS SYBRON CHEMICALS, INC.; LANXESS DEUTSCHLAND GMBH
Reel/Frame 030291/0957 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 15, 2013
From: TIRIO, ANTHONY P; WAGNER, RUDOLF
To: LANXESS SYBRON CHEMICALS, INC.
Reel/Frame 030213/0980 →
Continuity (5)
Continuation In Part 13278539 · Oct 21, 2011
Continuation In Part 12900882 · Oct 8, 2010
Provisional Application 61252838 · Oct 19, 2009
Provisional Application 61695556 · Aug 31, 2012
Related Publication 20130193378A1 · Aug 1, 2013