IP Library Granted Patent US 9,068,700
Granted Patent B2
US 9,068,700 · App. 13/432,124 · Granted Jun 30, 2015

Molecular sieve depressurization recovery method

Inventors: Daniel W. Sonnek (Lake Crystal, MN); Gregory W. Loest (Utica, SD)
Assignee: IntegroEnergy Group, Inc.
F17D1/16
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Quick Facts
Patent No.
US 9,068,700
App. No.
13/432,124
Granted
Jun 30, 2015
Kind
B2
Abstract

A method of depressurizing a molecular sieve used in ethanol production is provided. The ethanol production system includes a plurality of on-line molecular sieve bottles for removing water from ethanol production. When the molecular sieve bottle becomes saturated with water it is taken off-line to depressurize it. The depressurization and removal of water is done from the product discharge end resulting in an approximately 5% to 10% reduction in external energy required to run the ethanol production line.

Claims (7)

1. A method of depressurizing a molecular sieve used in ethanol production comprising: providing an ethanol production system, said ethanol production system including a plurality of on-line molecular sieve columns for removing water from said ethanol production, said molecular sieve columns having a product input end and a product discharge end and including a media therewithin; taking at least one of said plurality of molecular sieve columns off-line to depressurize it when said media becomes saturated, said off-line molecular sieve column containing anhydrous ethanol located at the product discharge end and water in the remainder of the bottle; extracting at least a portion of said anhydrous ethanol from said product discharge end; routing said at least a portion of said anhydrous ethanol to a sweeten off condenser; discharging said at least a portion of said anhydrous ethanol to a flash vessel; combining said at least a portion of said anhydrous ethanol with other anhydrous ethanol produced by said ethanol production system; and routing said combination of anhydrous ethanol to a storage tank.

2. The method of claim 1 further comprising providing an automatic valve that opens to a 190-proof condenser in the system to lower pressure in said off-line molecular sieve column.

3. The method of claim 1 wherein said anhydrous ethanol is extracted from the molecular sieve column without reversing the product flow through said molecular sieve media to the product input end.

4. A method of depressurizing a molecular sieve used in ethanol production comprising: providing an ethanol production system, said ethanol production system including a rectifier for producing 190-proof ethanol vapor; a condenser for condensing the 190-proof ethanol; an economizer for heating the 190-proof ethanol; a vaporizer for vaporizing the 190-proof ethanol; a plurality of on-line molecular sieve columns for removing water from said 190-proof ethanol, said molecular sieve columns having a product input end and a product discharge end and including a media therewithin; taking at least one of said plurality of molecular sieve columns off-line to depressurize it when said media becomes saturated, said off-line molecular sieve column containing anhydrous ethanol located at the product discharge end and water in the remainder of the column; extracting at least a portion of said anhydrous ethanol from said product discharge end; routing said at least a portion of said anhydrous ethanol to a sweeten off condensing heat exchanger; discharging said at least a portion of said anhydrous ethanol to a flash vessel; combining said at least a portion of said anhydrous ethanol with other anhydrous ethanol produced by said ethanol production system; and routing said combination of anhydrous ethanol to a storage tank.

5. The method of claim 4 wherein said anhydrous ethanol is extracted from the molecular sieve column without reversing the product flow through said molecular sieve media to the product input end.

6. The method of claim 4 further comprising removing heat from the combined anhydrous alcohol by passing said anhydrous alcohol through said economizer.

7. The method of claim 6 further comprising feeding said heat to said vaporizer thereby increasing a temperature of 190-proof ethanol being routed from said vaporizer to said on-line molecular sieves columns.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 17, 2023
From: INTEGROENERGY GROUP, INC.
To: INTEGROENERGY TECHNOLOGIES, LLC
Reel/Frame 065248/0539 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 24, 2012
From: SONNEK, DANIEL W.; LOEST, GREGORY W.
To: INTEGROENERGY GROUP, INC.
Reel/Frame 028846/0256 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 12, 2012
From: SONNEK, DANIEL W.; LOEST, GREGORY W.
To: INTEGROENERGY GROUP, INC.
Reel/Frame 028357/0499 →
Continuity (2)
Provisional Application 61468800 · Mar 29, 2011
Related Publication 20120312385A1 · Dec 13, 2012