IP Library › Granted Patent US 9,145,541
Granted Patent B2
US 9,145,541 · App. 12/679,063 · Granted Sep 29, 2015

Microorganism concentration process

Inventors: Manjiri T. Kshirsagar (Woodbury, MN); Tushar A. Kshirsagar (Woodbury, MN); Thomas E. Wood (Stillwater, MN)
Assignee: 3M Innovative Properties Company
C12N1/02B01J20/0229B01J20/06B01J20/2803B01J20/28004C12N11/14C12Q1/04C12Q1/24G01N1/405G01N33/54313
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Quick Facts
Patent No.
US 9,145,541
App. No.
12/679,063
Granted
Sep 29, 2015
Kind
B2
Abstract

A process for capturing or concentrating microorganisms for detection or assay comprises (a) providing a particulate concentration agent that comprises gamma-FeO(OH); (b) providing a fluid sample comprising at least one microorganism strain; and (c) contacting the concentration agent with the sample such that at least a portion of the concentration agent is dispersed in the sample and at least a portion of the at least one microorganism strain is bound to or captured by the concentration agent.

Claims (14)

1. A process comprising:

(a) providing a particulate concentration agent that consists essentially of gamma-FeO(OH) that comprises microparticle agglomerates comprising acicular crystallites that are less than 1 micrometer in largest dimension, wherein the microparticle agglomerates have particle sizes in the range of 3 micrometers to 100 micrometers in largest dimension;

(b) providing a fluid sample comprising at least one microorganism strain selected from strains of bacteria, yeasts, bacterial endospores, bacteriophages, and combinations thereof;

(c) contacting said concentration agent with said sample such that at least a portion of said concentration agent is dispersed in said sample and at least a portion of said at least one microorganism strain is bound to or captured by said concentration agent to provide a microorganism-bound concentration agent;

(d) segregating the resulting microorganism-bound concentration agent, wherein said segregating is effected by gravitational settling of the microorganism-bound concentration agent, wherein the gravitational settling is achieved over a time period of about 5 minutes to about 30 minutes; and

(e) detecting the presence of at least one viable bound microorganism.

2. The process of claim 1 , wherein said microorganism strain is selected from strains of bacteria, yeasts, and combinations thereof.

3. The process of claim 2 , wherein said microorganism strain is selected from strains of bacteria and combinations thereof.

4. The process of claim 1 , wherein said microorganism strain is selected from strains of gram-negative bacteria and combinations thereof.

5. The process of claim 1 , wherein said contacting is carried out by mixing said concentration agent and said sample.

6. The process of claim 1 , wherein said detecting is carried out by a method selected from culture-based methods, microscopy and other imaging methods, genetic detection methods, immunologic detection methods, bioluminescence-based detection methods, and combinations thereof.

7. The process of claim 1 , wherein said process further comprises separating the resulting segregated concentration agent from said sample.

8. A kit comprising (a) a particulate concentration agent that consists essentially of gamma-FeO(OH) that comprises microparticle agglomerates comprising acicular crystallites that are less than 1 micrometer in largest dimension, wherein the microparticle agglomerates have particle sizes in the range of 3 to 100 micrometers in largest dimension, and wherein the microparticle agglomerates have particles sizes in a range from 3 micrometers to 100 micrometers in largest dimension; (b) a testing container; (c) instructions for using said concentration agent in carrying out the process of claim 1 ; and (d) at least one of a genetic detection assay component, a bioluminescence detection assay component, a microorganism count plate, an antibody, a polypeptide, an aptamer, a fluorescent dye, or an enzyme.

9. The method of claim 1 , wherein the contacting is carried out for a period of about 15 seconds to about 5 minutes.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 19, 2010
From: KSHIRSAGAR, MANJIRI T.; KSHIRSAGAR, TUSHAR A.; WOOD, THOMAS E.
To: 3M INNOVATIVE PROPERTIES COMPANY
Reel/Frame 024107/0011 →
Continuity (2)
Provisional Application 60977188 · Oct 3, 2007
Related Publication 20100248214A1 · Sep 30, 2010