IP Library Granted Patent US 9,169,285
Granted Patent B2
US 9,169,285 · App. 14/033,563 · Granted Oct 27, 2015

Methods for purifying steviol glycosides and uses of the same

Inventors: Indra Prakash (Alpharetta, GA); Avetik Markosyan (Kuala Lumpur, MY); Venkata Sai Prakash Chaturvedula (Mission Viejo, CA); Mary Campbell (Acworth, GA); Rafael San Miguel (Atlanta, GA); Siddhartha Purkayastha (Lombard, IL); Marquita Johnson (Oak Lawn, IL)
Assignees: The Coca-Cola Company; Purecircle SDN BHD
C07H15/24A23L1/09A23L1/097A23L1/236A23L1/2363A23L1/2364A23L1/2366A23L2/00A23L2/60C07H1/08
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Quick Facts
Patent No.
US 9,169,285
App. No.
14/033,563
Granted
Oct 27, 2015
Kind
B2
Abstract

Methods for purifying steviol glycosides, including Rebaudioside X, are provided herein. Sweetener and sweetened containing Rebaudioside X are also provided herein. Methods of improving the flavor and/or temporal profile of sweetenable compositions, such as beverages, are also provided.

Claims (36)

1. A beverage comprising a sweetener composition comprising Reb X and a compound selected from the group consisting of Reb A, Reb B, Reb D, glucosylated steviol glycosides, Mogroside V, erythritol and combinations thereof, wherein the concentration of Reb X in the beverage is from about 50 ppm to about 600 ppm and the Reb X is present in an effective amount to provide a sucrose equivalence of greater than about 10% (w/v).

2. The beverage of claim 1 , wherein the compound is Reb A.

3. The beverage of claim 1 , wherein the compound is Reb B.

4. The beverage of claim 1 , wherein the compound is Reb D.

5. The beverage of claim 1 , wherein the compounds are Reb A and Reb D.

6. The beverage of claim 1 , wherein the compounds are Reb B and Reb D.

7. The beverage of claim 1 , wherein the pH of the beverage is from about 2 to about 5.

8. The beverage of claim 2 , wherein Reb A comprises from about 5% to about 40% by weight of the sweetener composition.

9. The beverage of claim 2 , wherein the concentration of Reb A in the beverage is about 10 ppm to about 500 ppm.

10. The beverage or claim 2 , wherein the concentration of Reb X is about 300 ppm and the concentration of Reb A in the beverage is about 100 ppm.

11. The beverage of claim 3 , wherein Reb B comprises from about 5% to about 40% by weight of the sweetener composition.

12. The beverage of claim 3 , wherein the concentration of Reb B in the beverage is about 10 ppm to about 150 ppm.

13. The beverage or claim 3 , wherein the concentration of Reb X is about 300 ppm and the concentration of Reb B in the beverage is from about 50 ppm to about 100 ppm.

14. The beverage of claim 4 , wherein Reb D comprises from about 5% to about 40% by weight of the sweetener composition.

15. The beverage of claim 4 , wherein the concentration of Reb D in the beverage is about 10 ppm to about 500 ppm.

16. The beverage or claim 4 , wherein the concentration of Reb X is about 300 ppm and the concentration of Reb D in the beverage is about 100 ppm.

17. The beverage of claim 1 , wherein the beverage is a zero-calorie beverage.

18. The beverage of claim 1 , further comprising a carbohydrate sweetener.

19. The beverage of claim 1 , wherein the beverage is selected from the group consisting of enhanced sparkling beverage, cola, lemon-lime flavored sparkling beverage, orange flavored sparkling beverage, grape flavored sparking beverage, strawberry flavored sparking beverage, grape flavored sparkling beverage, pineapple flavored sparkling beverage, ginger-ale, soft drink, root beer, fruit juice, fruit-flavored juice, juice drink, nectar, vegetable juice, vegetable-flavored juice, sports drink, energy drink, enhanced water drink, coconut water, tea-type drink, coffee, cocoa drink, beverage containing milk components, beverage containing cereal extract and a smoothie.

20. The beverage of claim 1 , further comprising at least one functional ingredient selected from the group consisting of saponin, antioxidant, dietary fiber source, fatty acid, vitamin, glucosamine, mineral, preservative, hydration agent, probiotic, prebiotic, weight management agent, osteoporosis management agent, phytoestrogen, long chain primary aliphatic saturated alcohol, phytosteroland combinations thereof.

21. The beverage of claim 19 , wherein the beverage is an enhanced water drink.

22. The beverage of claim 19 , wherein the beverage is a soft drink.

23. The beverage of claim 2 , wherein the concentration of Reb X is about 100 and the concentration of Reb A in the beverage is about 500.

24. The beverage of claim 2 , wherein the concentration of Reb A is between about 100 and about 200 ppm and the concentration of Reb X in the beverage is about 500 ppm.

25. The beverage of claim 4 , wherein the concentration of Reb X is about 500 and the concentration of Reb D in the beverage is about 100 ppm.

26. The beverage of claim 4 , wherein the concentration of Reb X is about 100 to about 200 ppm and the concentration of Reb D in the beverage is about 100 ppm.

27. The beverage of claim 1 , wherein the concentration of Reb X is at least about 100 ppm.

28. The beverage of claim 18 , wherein the carbohydrate sweetener is selected from the group consisting of glucose, fructose, sucrose and combinations thereof.

29. The beverage of claim 19 , wherein the beverage is a cola.

30. The beverage of claim 19 , wherein the beverage is a lemon-lime flavored sparkling beverage.

31. The beverage of claim 19 , wherein the beverage is a fruit juice.

32. The beverage of claim 19 , wherein the beverage is a sports drink or energy drink.

33. The beverage of claim 20 , wherein the at least one functional ingredient is a vitamin.

34. The beverage of claim 20 , wherein the at least one functional ingredient is an antioxidant.

35. The beverage of claim 20 , wherein the at least one functional ingredient is a mineral.

36. The beverage of claim 20 , wherein the at least one functional ingredient is a preservative.

Assignments (3)
NUNC PRO TUNC ASSIGNMENT Recorded Jun 26, 2015
From: PURKAYASTHA, SIDDHARTHA; JOHNSON, MARQUITA
To: PURECIRCLE SDN BHD
Reel/Frame 035914/0327 →
NUNC PRO TUNC ASSIGNMENT Recorded Oct 6, 2014
From: MARKOSYAN, AVETIK
To: PURECIRCLE SDN BHD
Reel/Frame 033894/0227 →
NUNC PRO TUNC ASSIGNMENT Recorded Oct 6, 2014
From: PRAKASH, INDRA; CHATURVEDULA, VENKATA SAI PRAKASH; CAMPBELL, MARY; SAN MIGUEL, RAFAEL
To: THE COCA-COLA COMPANY
Reel/Frame 033894/0328 →
Continuity (4)
Continuation PCTUS2012070562 · Dec 19, 2012
Provisional Application 61577202 · Dec 19, 2011
Provisional Application 61651099 · May 24, 2012
Related Publication 20140099403A1 · Apr 10, 2014