IP Library Granted Patent US 9,302,921
Granted Patent B2
US 9,302,921 · App. 14/013,247 · Granted Apr 5, 2016

Water detoxification by a substrate-bound catecholamine adsorbent

Inventors: Phillip B. Messersmith (Clarendon Hills, IL); Haeshin Lee (Daejeon, KR)
Assignee: Northwestern University
C02F1/288B01J20/262B01J20/28019B01J20/3204B01J20/3206B01J20/3272B01J20/3293B01J20/345B01J20/3475C02F1/285C02F1/286C02F2101/006C02F2101/20C02F2101/22C02F2101/30C02F2101/38C02F2303/16
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Quick Facts
Patent No.
US 9,302,921
App. No.
14/013,247
Granted
Apr 5, 2016
Kind
B2
Abstract

A bio-inspired method for detoxifying contaminated water is disclosed. In the method, polydopamine, a mussel-inspired adhesive catecholamine was used as an adsorbent to effectively remove from contaminated water three major classes of toxic agents: heavy metal ions (e.g., Cr, Hg, Pb, Cu, and Cd), toxic organic species (e.g., 4-aminopyridine), and radioisotopes (e.g., Lutetium-177). Furthermore, the polydopamine adsorbent was regenerated by treatment with acid or hydrogen peroxide.

Claims (11)

1. A method for removing one or more contaminants from water, the method comprising contacting the water with an adsorbent comprising a polydopamine polymer, whereby the one or more contaminants are adsorbed to the polydopamine polymer and removed from the water; and

regenerating the adsorbent by contacting the adsorbent with dilute acid, whereby the contaminants are removed from the adsorbent.

2. The method of claim 1 , wherein the polydopamine polymer is the polymer obtained by contacting a substrate surface with an alkaline solution comprising dopamine.

3. The method of claim 1 , wherein the adsorbent is coated onto a substrate surface.

4. The method of claim 3 , wherein the substrate comprises a substance selected from the group consisting of glass, a metal, an oxide, a semiconductor, a ceramic, and a second synthetic polymer.

5. The method of claim 4 , wherein the substrate is a glass bead.

6. The method of claim 1 , wherein the water is contacted with the adsorbent comprising the polymer by batch or continuous flow, wherein the polymer is natural or synthetic.

7. The method of claim 1 wherein the dilute acid is acetic acid.

8. The method of claim 1 , wherein the one or more contaminants are metal ions.

9. The method of claim 8 , wherein the metal ion is the ion of a toxic metal.

10. The method of claim 9 , wherein the toxic metal ion is selected from the group consisting of copper (II), chromium (VI), mercury (II), cadmium (II), and lead (II).

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 3, 2015
From: MESSERSMITH, PHILLIP B.; LEE, HAESHIN
To: NORTHWESTERN UNIVERSITY
Reel/Frame 037201/0488 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 15, 2013
From: HERZOG, LAURIE L
To: NORTHWESTERN UNIVERSITY
Reel/Frame 031404/0049 →
CONFIRMATORY LICENSE Recorded Sep 17, 2013
From: NORTHWESTERN UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 031288/0121 →
Continuity (2)
Provisional Application 61694383 · Aug 29, 2012
Related Publication 20140061135A1 · Mar 6, 2014