IP Library Granted Patent US 9,386,791
Granted Patent B2
US 9,386,791 · App. 14/355,803 · Granted Jul 12, 2016

Dairy product and process

Inventors: Rama Mohana Rao Gulla (Auckland, NZ); Roger Richard Schwarzenbach (Auckland, NZ); Esra Cakir-Fuller (Auckland, NZ)
Assignee: FONTERRA CO-OPERATIVE GROUP LIMITED
A23L1/296A23C21/08A23J1/20A23J3/08A23L1/3056A23V2002/00
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Quick Facts
Patent No.
US 9,386,791
App. No.
14/355,803
Granted
Jul 12, 2016
Kind
B2
Abstract

The invention relates to liquid nutritional compositions, particularly shelf stable liquid nutritional compositions including compositions comprising non-hydrolyzed whey protein, and methods of producing and using these compositions.

Claims (96)

1. A method of preparing a liquid nutritional composition, the method comprising

a) heat-treating a liquid composition having a pH of between 4 and 6 and comprising about 2% to about 25% by weight of non-hydrolysed whey protein, wherein the whey protein comprises or is provided by an ingredient that comprises at least about 55% of the heat-denaturable protein present in a denatured state, and wherein the heat treatment has an F 0 -value of at least equivalent to 90° C. for 40 s, and

b) recovering the liquid composition,

wherein the recovered liquid composition has

c) a viscosity of less than 200 cP when measured at 20° C. and shear rate of 100 s-1, or

d) an average particle size of less than 20 μm as categorised by the volume weighted average particle size parameter D[4,3], or

e) exhibits essentially no observable gelation or aggregation, or

f) any combination of two or more of (c) to (e) above.

2. The method of claim 1 wherein the heat treatment is at least equivalent to 121° C. for 10 minutes.

3. The method of claim 2 wherein the heat treatment is at least equivalent to 140° C. for 5 s.

4. The method of claim 1 wherein the liquid nutritional composition exhibits no observable gelation, or no observable aggregation, or both, after storage for at least 3 months at room temperature.

5. The method of claim 1 wherein the liquid nutritional composition comprises:

a) 30 to 175 mg sodium,

b) 80 to 295 mg potassium,

c) 30 to 175 mg chloride,

d) 35 to 175 mg calcium,

e) 30 to 80 mg phosphorus,

f) 7.5 to 25 mg magnesium,

g) 0.5 to 2.0 mg iron,

h) 0.5 to 1.5 mg zinc,

i) 60 to 500 μg copper,

j) 6.5 to 35 μg iodine,

k) 2.5 to 10 μg selenium,

l) 0.05 to 0.5 mg manganese,

m) 1.25 to 15 μg chromium,

n) 3.5 to 18 μg molybdenum, and

o) less than 0.2 mg fluoride

per 100 kcal of the liquid nutritional composition.

6. The method of claim 1 wherein the liquid nutritional composition has when undergoing the heat treatment

a) a pH of between about 4.7 to about 6.0, or

b) a pH of between about 4.8 to about 6.0, or

c) a pH of between about 4.9 to about 6.0, or

d) a pH of between about 5.0 to about 6.0, or

e) a pH of between about 4.5 to about 5.7, or

f) a pH of between about 4.5 to about 5.5, or

g) a pH of between about 4.5 to about 5.3, or

h) a pH of between about 4.5 to about 5.2, or

i) a pH of between about 4.7 to about 5.5, or

j) a pH of between about 4.7 to about 5.3, or

k) a pH of between about 4.7 to about 5.2, or

l) a pH of between about 4.8 to about 5.3, or

m) a pH of between about 4.8 to about 5.2, or

n) a pH of about 5, or

o) a pH of between about 4.2 to about 5.8, or

p) a pH of between about 4.4 to about 5.8, or

q) a pH of between about 4.6 to about 5.6, or

r) a pH of between about 4.8 to about 5.4, or

s) a pH of between about 4.9 to about 5.3, or

t) a pH of between about 5.0 to about 5.2, or

u) a pH of about 5.1, or

v) a pH of between about 4.3 to about 5.1, or

w) a pH of between about 4.6 to about 5.1, or

x) a pH of between about 4.8 to about 5.1, or

y) a pH of between about 5.1 to about 6.0, or

z) a pH of between about 5.1 to about 5.8, or

aa) a pH of between about 5.1 to about 5.6, or

bb) a pH of between about 5.1 to about 5.4.

7. The method of claim 1 wherein the liquid nutritional composition has when undergoing the heat treatment

a) a pH of between about 4.1 to about 5.1, or

b) a pH of between about 4.3 to about 5.1, or

c) a pH of between about 4.5 to about 5.1, or

d) a pH of between about 4.7 to about 5.1, or

e) a pH of between about 4.9 to about 5.1, or

f) a pH of between about 5.1 to about 6.0, or

g) a pH of between about 5.1 to about 5.8, or

h) a pH of between about 5.1 to about 5.6, or

i) a pH of between about 5.1 to about 5.4, or

j) a pH of between about 5.1 to about 5.2, or

k) a pH of about 5.1.

8. The method of claim 1 wherein the liquid nutritional composition has when undergoing the heat treatment a pH of about 5.4.

9. The method of claim 1 wherein the liquid nutritional composition has when undergoing the heat treatment a pH of about 5.1.

10. The method of claim 1 wherein the liquid nutritional composition has when undergoing the heat treatment a pH of within about 0.5 of the average pI of the protein, or

a) a pH of within about 0.3 of the average pI of the protein, or

b) a pH of within about 0.1 of the average pI of the protein, or

c) a pH at about the average pI of the protein.

11. The method of claim 1 wherein the non-hydrolysed whey protein is provided by a dry ingredient that comprises a protein content of 35% to 95% by weight of the dry matter of the ingredient.

12. A liquid nutritional composition comprising

a) from about 2% to about 25% by weight of non-hydrolysed whey protein, wherein the whey protein comprises or is provided by an ingredient that comprises at least about 55% of the heat-denaturable protein present in a denatured state,

b) from 0 to about 30% by weight fat

c) from about 0% to about 45% by weight carbohydrate

and wherein the nutritional composition has when at a pH of between 4 and 6 undergone a heat treatment with an F 0 -value of at least equivalent to 90° C. for 40 s, and has

d) a viscosity of less than 200 cP when measured at 20° C. and shear rate of 100 s-1, or

e) an average particle size of less than 20 μM as categorised by the volume weighted average particle size parameter D[4,3], or

f) exhibits essentially no observable gelation or aggregation, or

g) any combination of two or more of (d) to (f) above.

13. The liquid nutritional composition of claim 12 wherein the nutritional composition has a pH of between about 4 to about 6, and a viscosity of less than 200 cP at a temperature of 20° C. and a shear rate of 100 s −1 and exhibits essentially no gelation or aggregation.

14. The liquid nutritional composition of claim 12 wherein the liquid nutritional composition has a viscosity of less than 150 cP at a temperature of 20° C. and a shear rate of 100 s −1 .

15. The liquid nutritional composition of claim 12 wherein the liquid nutritional composition has a viscosity of less than 50 cP at a temperature of 20° C. and a shear rate of 100 s −1 .

16. The liquid nutritional composition of claim 12 having

a) a pH of within about 0.5 of the average pI of the protein, or

b) a pH of within about 0.3 of the average pI of the protein, or

c) a pH of within about 0.1 of the average pI of the protein, or

d) a pH at about the average pI of the protein.

17. A powdered nutritional composition dispersible in water to form a liquid nutritional composition of claim 12 .

18. A method of providing nutrition to a person in need thereof, the method comprising the steps of administering to the person a nutritional composition of claim 12 .

19. A food or food product comprising, consisting essentially of, or consisting of a liquid nutritional composition of claim 12 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 8, 2016
From: GULLA, RAMA MOHANA RAO; SCHWARZENBACH, ROGER RICHARD; CAKIR-FULLER, ESRA
To: FONTERRA CO-OPERATIVE GROUP LIMITED
Reel/Frame 038844/0203 →
Continuity (3)
Provisional Application 61554926 · Nov 2, 2011
Provisional Application 61699709 · Sep 11, 2012
Related Publication 20140314851A1 · Oct 23, 2014