IP Library Granted Patent US 9,440,171
Granted Patent B2
US 9,440,171 · App. 13/932,886 · Granted Sep 13, 2016

Reactors for forming foam materials from high internal phase emulsions, methods of forming foam materials and conductive nanostructures therein

Inventor: Wilmot H. McCutchen (Orinda, CA)
Assignee: MCCUTCHEN CO.
B01D39/16B01D33/15B01D33/21B01D33/23B01D39/14B01D39/1638C08J9/0066C08J9/0071C08J9/28B01D33/0006B01D33/0041B01D33/0087B01D39/083B01D2239/025B01D2239/0258B01F7/00875B01J19/20C08F2/32C08J9/228C08J2201/028
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Quick Facts
Patent No.
US 9,440,171
App. No.
13/932,886
Granted
Sep 13, 2016
Kind
B2
Abstract

An RF inductor such as a Tesla antenna splices nanotube ends together to form a nanostructure in a polymer foam matrix. High Internal Phase Emulsion (HIPE) is gently sheared and stretched in a reactor comprising opposed coaxial counter-rotating impellers, which parallel-align polymer chains and also carbon nanotubes mixed with the oil phase. Stretching and forced convection prevent the auto-acceleration effect. Batch and continuous processes are disclosed. In the batch process, a fractal radial array of coherent vortices in the HIPE is preserved when the HIPE polymerizes, and helical nanostructures around these vortices are spliced by microhammering into longer helices. A disk radial filter produced by the batch process has improved radial flux from edge to center due to its area-preserving radial vascular network. In the continuous process, strips of HIPE are pulled from the periphery of the reactor continuously and post-treated by an RF inductor to produce cured conductive foam.

Claims (11)

1. A radial disk filter, composed of a high internal phase emulsion (HIPE) foam and having:

a periphery;

an axial exhaust port disposed central to the periphery of the radial disk filter;

a fractal vascular network extending through the radial disk filter from the periphery to the axial exhaust port, the fractal vascular network configured to filter a solution inward from the periphery, through the fractal vascular network, and into the axial exhaust port; and

an axial extraction pump in fluid communication with the axial exhaust port and configured to draw the solution through the radial disk filter and expel a filtrate remotely from the radial disk filter.

2. The radial disk filter of claim 1 , further comprising nanomaterials aligned within the high internal phase emulsion (HIPE) foam.

3. The radial disk filter of claim 2 , wherein the nanomaterials are carbon nanotubes.

4. The radial disk filter of claim 1 , comprising a radial array of conductive helices comprised of conductive nanomaterials aligned within the HIPE foam by a radio frequency inductor configured to induce an electrical current within the conductive nanomaterials.

5. The radial disk filter of claim 4 , wherein the radial array comprises carbon nanotubes linked by microhammering by the induced electrical current of the radio frequency inductor.

6. A plurality of radial disk filters of claim 1 arranged in an array, the axial exhaust port of each radial disk filter of the array aligned along a common axis with a single axial extraction pump located at an end of the axis and configured to draw the solution through the plurality of radial disk filters of the array and expel a filtrate remotely from the array.

7. The array of claim 6 , wherein the array is configured to be rotated to induce a shear lift effect upon particles suspended within the solution, the shear lift effect preventing the particles from contacting the rotating array.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 22, 2019
From: MCCUTCHEN CO.
To: VORSANA, INC.
Reel/Frame 048410/0419 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 1, 2013
From: MCCUTCHEN, WILMOT H.
To: MCCUTCHEN CO.
Reel/Frame 030723/0499 →
Continuity (3)
Continuation 12794693 · Jun 4, 2010
Provisional Application 61184666 · Jun 5, 2009
Related Publication 20130299415A1 · Nov 14, 2013