IP Library Granted Patent US 9,493,679
Granted Patent B2
US 9,493,679 · App. 14/874,379 · Granted Nov 15, 2016

Methods of manufacturing abrasive particle and polishing slurry

Inventor: Seung Won Jung (Anyang-Si, KR)
Assignee: INDUSTRIAL BANK OF KOREA
C09G1/02C01F17/0043C09K3/1409C09K3/1445C09K3/1463C01P2004/40C01P2004/61C01P2004/62C01P2006/22
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Quick Facts
Patent No.
US 9,493,679
App. No.
14/874,379
Granted
Nov 15, 2016
Kind
B2
Abstract

Provided is a method of manufacturing an abrasive particle including a mother particle and a plurality of auxiliary particles formed on a surface of the mother particle, and a method of manufacturing a polishing slurry in which the abrasive particle is mixed with a polishing accelerating agent and a pH adjusting agent.

Claims (16)

1. A method of manufacturing a polishing slurry polishing a workpiece, wherein the method comprises:

mixing a first precursor material aqueous solution and a diluted alkaline solution and thermally treating the mixture solution to prepare a mother particle having a polyhedral crystal face;

adding an alkaline solution to a mixture solution in which the mother particle is mixed, mixing a second precursor material aqueous solution and thermally treating the mixture solution to form a plurality of auxiliary particles protruded outward from a surface of the mother particle, thereby preparing an abrasive particle; and

dispersing said abrasive particle in a dispersing agent containing deionized water,

wherein the mother particle is the same material as the auxiliary particle.

2. The method of claim 1 , wherein the auxiliary particle of the abrasive particle is formed from an edge where at least two of the polyhedral crystal faces meet.

3. The method of claim 2 , wherein a ratio of a size of the auxiliary particle to a size of the mother particle is 1:100 to 1:5.

4. The method of claim 3 , wherein the abrasive particle is contained in an amount ranging from approximately 0.1 wt % to approximately 5 wt % based on a solid component.

5. The method of claim 1 , further comprising adding a polishing accelerating agent,

wherein the polishing accelerating agent comprises a cationic low molecular weight polymer, a cationic high molecular weight polymer, a hydroxylic acid, and an amino acid, which convert a surface potential of the abrasive particle to a minus potential.

6. The method of claim 5 , wherein the polishing accelerating agent is contained in an amount of approximately 0.01 wt % to approximately 0.1 wt % based on 1 wt % of the abrasive particle.

7. The method of claim 6 , wherein the cationic low molecular and high molecular polymers comprise at least one of an oxalic acid, a citric acid, a polysulfonic acid, a polyacrylic acid, a polymethacrylic acid (Darvan C-N), copolymeric acids thereof, or salts thereof, the hydroxylic acid comprises at least one of a hydroxylbenzoic acid, an ascorbic acid, or salts thereof, and the amino acid comprises at least one of a picolinic acid, a glutaminic acid, a tryptophan acid, an aminobutylic acid, or salts thereof.

8. The method of claim 1 , further comprising adding a pH adjusting agent adjusting pH of the slurry,

wherein the pH of the slurry is maintained in a range of 4 to 9 by the pH adjusting agent.

9. The method of claim 5 , further comprising adding a pH adjusting agent adjusting pH of the slurry,

wherein the pH of the slurry is maintained in a range of 4 to 9 by the pH adjusting agent.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 3, 2022
From: SHIN-ETSU CHEMICAL CO., LTD.
To: UBMATERIALS INC.
Reel/Frame 059318/0078 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 4, 2017
From: INDUSTRIAL BANK OF KOREA
To: SHIN-ETSU CHEMICAL CO., LTD.
Reel/Frame 042406/0072 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 1, 2015
From: UBMATERIALS INC.
To: INDUSTRIAL BANK OF KOREA
Reel/Frame 037182/0395 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 1, 2015
From: JUNG, SEUNG WON
To: UBMATERIALS INC.
Reel/Frame 036930/0463 →
Priority Claims (1)
KR 10-2013-0109872 · Sep 12, 2013 · national
Continuity (2)
Division 14483140 · Sep 10, 2014
Related Publication 20160024350A1 · Jan 28, 2016