IP Library Granted Patent US 9,529,098
Granted Patent B2
US 9,529,098 · App. 14/041,831 · Granted Dec 27, 2016

X-ray monitoring optical elements

Inventors: Stanislav Stoupin (Willowbrook, IL); Yury Shvydko (Lisle, IL); John Katsoudas (Chicago, IL); Vladimir D. Blank (Moscow, RU); Sergey A. Terentyev (Moscow, RU)
Assignee: UChicago Argonne, LLC
G01T1/26
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Quick Facts
Patent No.
US 9,529,098
App. No.
14/041,831
Granted
Dec 27, 2016
Kind
B2
Abstract

An X-ray article and method for analyzing hard X-rays which have interacted with a test system. The X-ray article is operative to diffract or otherwise process X-rays from an input X-ray beam which have interacted with the test system and at the same time provide an electrical circuit adapted to collect photoelectrons emitted from an X-ray optical element of the X-ray article to analyze features of the test system.

Claims (28)

1. An X-ray article for processing a hard X-ray beam to measure features of the X-ray beam after interaction with a test system comprising,

an X-ray optical element comprising a single crystal x-ray diffracting crystal operative to receive a hard X-ray beam at an exposure surface of the X-ray optical element and process the hard X-ray beam which has interacted with the test system for analysis thereof;

the exposure surface configured to emit electrons;

a surface electrode electrically connected with the exposure surface and an electron supply configured to provide electrons to replace the emitted electrons, creating a current, the surface electrode positioned adjacent to the exposure surface so as not to receive the hard X-ray beam;

an amp meter positioned in electrical contact between the surface electrode and the electron supply for measuring the current; and

the X-ray optical element further including intrinsic optical states which can be excited by the hard X-ray beam, thereby producing emission of photoelectrons and enhancement of surface;

wherein the X-ray article includes a substrate and a second electrode electrically coupled to the substrate and to the surface electrode;

wherein the measured current is proportional to X-ray flux of the hard X-ray beam incident on the exposure surface.

2. The X-ray article as defined in claim 1 wherein the X-ray optical element is selected from the group of single crystals for X-ray optics including diamond, Si, Ge, Be, Al 2 O 3 , SiC and SiO 2 .

3. The X-ray article as defined in claim 1 wherein the hard x-ray beam and x-ray optical element exhibit Bragg diffraction.

4. The X-ray article as defined in claim 1 wherein the X-ray optical element is selected from the group of an X-ray refractive lens, diffractive lens, an X-ray reflective mirror, capillary optics, a collimating slit and a transmitting optical element, thereby enabling the X-ray optical element to analyze the X-ray beam which has interacted with the test system.

5. The X-ray article as defined in claim 1 wherein the X-ray article includes a substrate and another electrode coupled to the substrate.

6. The X-ray article as defined in claim 1 further including a third electrode having a positive potential and the-third electrode is disposed above the X-ray optical element to capture electrons escaping from the exposure surface, thereby accelerating the photoelectrons escaping from the X-ray optical element and preventing return of the photoelectrons to the X-ray optical element.

7. The X-ray article as defined in claim 1 further including a voltage source to lower electrical potential of a surface of the X-ray optical element and to enhance the electric current in the circuit due to a change in surface conductivity induced by the X-ray beam.

8. The X-ray article as defined in claim 6 wherein the additional electrode comprises a charged grid.

9. The X-ray article as defined in claim 1 further including an electrical circuit comprised of a first electrode and a second electrode and an ammeter coupled to ground.

10. A method of analyzing features of a test system, comprising:

applying a hard X-ray beam to the test system;

disposing X-ray article having a substrate and an X-ray optical element comprising a single crystal x-ray diffracting crystal operative to receive a hard X-ray beam at an exposure surface of the X-ray optical element and process the X-ray beam which has interacted with the test system for analysis thereof, the X-ray optical element including intrinsic optical states which can be excited by the hard X-ray beam, thereby producing emission of photoelectrons and enhancement of surface

coupling a second electrode to the substrate and the surface electrode;

emitting photoelectrons from the exposure surface of the X-ray optical element;

capturing photoelectrons with an electrode above the surface;

replacing emitted photoelectrons from an electron supply through a surface electrode, which is positioned adjacent to the exposure surface so as not to receive the hard X-ray beam, on the X-ray optical element causing a surface current; and

measuring surface current, with an amp meter positioned in electrical contact between the surface electrode and the electron supply, induced by the X-ray beam striking the X-ray optical element and also collecting X-rays which have interacted with the test system and processed by the X-ray optical element, thereby accumulating information from both the induced current and the processed X-rays for analysis of features of the test system;

wherein the measured current is proportional to X-ray flux of the hard X-ray beam incident on the exposure surface.

11. The method as defined in claim 10 further including the step of applying a bias voltage to the X-ray optical element, thereby accelerating the photoelectrons escaping from the X-ray optical element.

12. The method as defined in claim 11 wherein the bias voltage arises from an electrode being disposed adjacent the X-ray optical element.

13. The method as defined in claim 12 wherein the bias voltage electrode comprises a charged grid.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 16, 2015
From: STOUPIN, STANISLAV; SHVYDKO, YURY
To: UCHICAGO ARGONNE, LLC
Reel/Frame 035843/0213 →
CONFIRMATORY LICENSE Recorded Feb 5, 2014
From: UCHICAGO ARGONNE, LLC
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 032167/0086 →
Continuity (1)
Related Publication 20150092925A1 · Apr 2, 2015