IP Library › Granted Patent US 9,561,543
Granted Patent B2
US 9,561,543 · App. 14/391,269 · Granted Feb 7, 2017

Method for manufacturing metal powder

Inventors: Fumiyuki Shimizu (Tosu, JP); Masayuki Maekawa (Tosu, JP); Tomotaka Nishikawa (Tosu, JP)
Assignee: SHOEI CHEMICAL INC.
B22F9/14B22F9/06B22F9/12H05H1/48B22F3/003B22F2999/00H05H2001/483
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Quick Facts
Patent No.
US 9,561,543
App. No.
14/391,269
Granted
Feb 7, 2017
Kind
B2
Abstract

A method for manufacturing metal powder includes: melting at least a portion of a metal starting material in a reaction vessel by utilizing plasma so as to form molten metal; evaporating the molten metal so as to produce a metal vapor; and transferring the metal vapor from the reaction vessel to a cooling tube together with a carrier gas supplied into the reaction vessel so as to cool the metal vapor, and condensing the metal vapor in the cooling tube, thereby producing metal powder. The method further includes supplying an oxygen gas into the reaction vessel.

Claims (14)

1. A method for manufacturing metal powder comprising:

melting at least a portion of a metal starting material in a reaction vessel by utilizing plasma so as to form molten metal;

evaporating the molten metal so as to produce a metal vapor;

transferring the metal vapor from the reaction vessel to a cooling tube together with a carrier gas supplied into the reaction vessel so as to cool the metal vapor; and

condensing the metal vapor in the cooling tube, thereby producing metal powder, wherein

the method further comprises supplying an oxygen gas into the reaction vessel, during melting, and

at least a part of the reaction vessel is formed of an oxide ceramic material, the part contacting the molten metal.

2. The method for manufacturing metal powder according to claim 1 , wherein the oxide ceramic material is zirconia-based ceramic.

3. The method for manufacturing metal powder according to claim 1 , wherein the oxygen gas is supplied at an amount of 1500 mL/min or less for a metal powder production amount of 1 Kg/hr.

4. The method for manufacturing metal powder according to claim 1 further comprising supplying an additional element selected from sulfur, phosphorus, platinum, rhenium, zinc, tin, aluminum and boron into the reaction vessel, during melting.

5. The method for manufacturing metal powder according to claim 4 , wherein the additional element is supplied in a form of an organic compound and/or a hydrogen compound.

6. The method for manufacturing metal powder according to claim 1 , wherein the metal powder contains 50% by weight or more of a base metal and the base metal is nickel, copper, cobalt, iron, tantalum, titanium or tungsten.

7. The method for manufacturing metal powder according to claim 1 , wherein the plasma is transferred DC arc plasma.

8. The method for manufacturing metal powder according to claim 1 , wherein the oxygen gas is supplied at an amount of 0.05 mL/min or more for a metal powder production amount of 1 Kg/hr.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 8, 2014
From: SHIMIZU, FUMIYUKI; MAEKAWA, MASAYUKI; NISHIKAWA, TOMOTAKA
To: SHOEI CHEMICAL INC.
Reel/Frame 033912/0236 →
Priority Claims (1)
JP 2012-096480 · Apr 20, 2012 · national
Continuity (1)
Related Publication 20150101454A1 · Apr 16, 2015