IP Library Granted Patent US 9,688,957
Granted Patent B2
US 9,688,957 · App. 14/684,062 · Granted Jun 27, 2017

Hydrogel compositions for use in promoting tubulogenesis

Inventors: William L. Murphy (Waunakee, WI); Ngoc Nhi Le (Norcross, GA); Michael P. Schwartz (Madison, WI); Eric Huy Dang Nguyen (Madison, WI); Stefan Zorn (Madison, WI); Hamisha Ardalani (Madison, WI); Matthew Zanotelli (Muskego, WI); Matthew Brian Parlato (Madison, WI); David Gregory Belair (Madison, WI); William T. Daly (Madison, WI)
Assignee: Wisconsin Alumni Research Foundation
C12N5/0606G01N33/4833B01J19/0046B01J2219/00596C12N2533/20C12N2533/30C12N2537/10G01N21/6452G01N2610/00
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Quick Facts
Patent No.
US 9,688,957
App. No.
14/684,062
Granted
Jun 27, 2017
Kind
B2
Abstract

Hydrogel Compositions and methods of using hydrogel compositions are disclosed. Advantageously, the hydrogel compositions offer the ability to rapidly screen substrate components for influencing cell attachment, spreading, proliferation, migration, and differentiation. In particularly suitable embodiments, the hydrogel compositions of the present disclosure may be used to promote tubulogenesis of endothelial cells.

Claims (27)

1. A method of screening for pro-tubulogenic agents and anti-tubulogenic agents, the method comprising:

preparing a hydrogel composition, wherein the hydrogel composition comprises an 8-arm, 20 kDa polyethylene glycol functionalized with norbornene, a crosslinking peptide, a cell adhesion peptide, and a soluble factor binder peptide;

providing an agent suspected of promoting or reducing tubulogenesis;

contacting a cell with the hydrogel composition and agent; and

analyzing the cell.

2. The method of claim 1 wherein the agent is coupled to the hydrogel composition.

3. The method of claim 1 wherein the agent is contained within a cell culture medium, and wherein the cell culture medium is contacted with the hydrogel composition.

4. The method of claim 1 wherein the cell adhesion peptide is selected from the group consisting of CRGDS (SEQ ID NO: 2), acetylated-GCYGRGDSPG (SEQ ID NO:31), cyclic RGD{Fd}C (SEQ ID NO:33), CRGD-(G) 13 -PHSRN (SEQ ID NO:29), CPHSRN-(SG) 5 -RGD (SEQ ID NO:30), RKRLQVQLSIRT (SEQ ID NO:37), IKVAV (SEQ ID NO:38), YIGSR (SEQ ID NO:39), KRTGQYKL (SEQ ID NO:40), TYRSRKY (SEQ ID NO:41), KRTGQYKLGSKTGPGQK (SEQ ID NO:42), QAKHKQRKRLKSSC (SEQ ID NO:43), and SPKHHSQRARKKKNKNC (SEQ ID NO:44).

5. The method of claim 1 wherein the crosslinking peptide comprises an amino acid sequence selected from the group consisting of KCGGPQGIWGQGCK (SEQ ID NO:27) and KCGGPQGIAGQGCK (SEQ ID NO:28).

6. The method of claim 1 wherein the soluble factor binder comprises an amino acid sequence selected from the group consisting of SEQ ID NOs:22-26.

7. The method of claim 1 wherein the cell is selected from the group consisting of an embryonic stem cell, an embryonic stem cell-derived neuron, an embryonic stem cell-derived neural progenitor cell, an embryonic stem cell-derived astrocyte, an embryonic stem cell-derived microglial cell, an embryonic stem cell-derived endothelial cell, an embryonic stem cell-derived retinal pigment epithelial cell, an induced pluripotent stem cell, an induced pluripotent stem cell-derived neural progenitor cell, an induced pluripotent stem cell-derived astrocyte, an induced pluripotent stem cell-derived microglial cell, an induced pluripotent stem cell-derived endothelial cell, an induced pluripotent stem cell-derived retinal pigment epithelial cell, a mesenchymal stem cell, an umbilical vein endothelial cell, an NIH 3T3 fibroblast, a dermal fibroblast, a fibrosarcoma cell, a valvular interstitial cell, a cardiomyocyte, an induced pluripotent stem cell-derived cardiomyocyte, an endothelial progenitor cell, a circulating angiogenic cell, a neuron, a pericyte, a cancer cell, a hepatocyte, a pancreatic beta cell, a pancreatic islet cell and combinations thereof.

8. A method of promoting tubulogenesis, the method comprising:

preparing a hydrogel composition, wherein the hydrogel composition comprises an 8-arm, 20 kDa polyethylene glycol functionalized with norbornene, a crosslinking peptide, a cell adhesion peptide, and a soluble factor binder peptide;

providing a culture media in contact with the hydrogel composition;

contacting a cell in the culture media in contact with the hydrogel composition; and

analyzing the cell.

9. The method of claim 8 wherein the cell adhesion peptide is selected from the group consisting of CRGDS (SEQ ID NO: 2), acetylated-GCYGRGDSPG (SEQ ID NO:31), cyclic RGD{Fd}C (SEQ ID NO:33), CRGD-(G) 13 -PHSRN (SEQ ID NO:29), CPHSRN-(SG) 5 -RGD (SEQ ID NO:30), RKRLQVQLSIRT (SEQ ID NO:37), IKVAV (SEQ ID NO:38), YIGSR (SEQ ID NO:39), KRTGQYKL (SEQ ID NO:40), TYRSRKY (SEQ ID NO:41), KRTGQYKLGSKTGPGQK (SEQ ID NO:42), QAKHKQRKRLKSSC (SEQ ID NO:43), and SPKHHSQRARKKKNKNC (SEQ ID NO:44).

10. The method of claim 8 wherein the crosslinking peptide comprises an amino acid sequence selected from the group consisting of KCGGPQGIWGQGCK (SEQ ID NO:27) and KCGGPQGIAGQGCK (SEQ ID NO:28).

11. The method of claim 8 wherein the soluble factor binder comprises an amino acid sequence selected from the group consisting of SEQ ID NOs:22-26.

12. The method of claim 8 wherein the cell is selected from the group consisting of an embryonic stem cell, an embryonic stem cell-derived neuron, an embryonic stem cell-derived neural progenitor cell, an embryonic stem cell-derived astrocyte, an embryonic stem cell-derived microglial cell, an embryonic stem cell-derived endothelial cell, an embryonic stem cell-derived retinal pigment epithelial cell, an induced pluripotent stem cell, an induced pluripotent stem cell-derived neural progenitor cell, an induced pluripotent stem cell-derived astrocyte, an induced pluripotent stem cell-derived microglial cell, an induced pluripotent stem cell-derived endothelial cell, an induced pluripotent stem cell-derived retinal pigment epithelial cell, a mesenchymal stem cell, an umbilical vein endothelial cell, an NIH 3T3 fibroblast, a dermal fibroblast, a fibrosarcoma cell, a valvular interstitial cell, a cardiomyocyte, an induced pluripotent stem cell-derived cardiomyocyte, an endothelial progenitor cell, a circulating angiogenic cell, a neuron, a pericyte, a cancer cell, a hepatocyte, a pancreatic beta cell, a pancreatic islet cell and combinations thereof.

13. The method of claim 8 wherein the tubulogenesis comprises endothelial cell tubule network formation.

14. A hydrogel composition comprising an 8-arm, 20 kDa polyethylene glycol functionalized with norbornene, a crosslinking peptide, a cell adhesion peptide and a soluble factor binder peptide.

15. The hydrogel composition of claim 14 wherein the cell adhesion peptide is selected from the group consisting of CRGDS (SEQ ID NO: 2), CRGD-(G) 13 -PHSRN (SEQ ID NO:29), and CPHSRN-(SG) 5 -RGD (SEQ ID NO:30), Acetylated-GCYGRGDSPG (SEQ ID NO:31), CRDGS (SEQ ID NO:32), cyclic RGD{Fd}C (SEQ ID NO:33), RKRLQVQLSIRT (SEQ ID NO:37), IKVAV (SEQ ID NO:38), YIGSR (SEQ ID NO:39), KRTGQYKL (SEQ ID NO:40), TYRSRKY (SEQ ID NO:41), KRTGQYKLGSKTGPGQK (SEQ ID NO:42), QAKHKQRKRLKSSC (SEQ ID NO:43), and SPKHHSQRARKKKNKNC (SEQ ID NO:44).

16. The hydrogel composition of claim 14 wherein the soluble factor binder comprises an amino acid sequence selected from the group consisting of SEQ ID NOs:22-26.

17. The hydrogel composition of claim 14 having an elastic modulus range of from about 0.1 kPa to about 300 kPa.

18. The hydrogel composition of claim 14 wherein the concentration of polyethylene glycol is from about 36 mg/mL to about 70 mg/mL.

19. The hydrogel composition of claim 14 comprising an extent of crosslinking, wherein the extent of crosslinking is from about 30% to about 70%.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 11, 2018
From: WISCONSIN ALUMNI RESEARCH FOUNDATION
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 046137/0249 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 7, 2015
From: MURPHY, WILLIAM; NGUYEN, ERIC; SCHWARTZ, MICHAEL; ARDALANI, HAMISHA; ZANOTELLI, MATTHEW; PARLATO, MATTHEW; BELAIR, DAVID; DALY, WILLIAM; LE, NGOC NHI; ZORN, STEFAN
To: WISCONSIN ALUMNI RESEARCH FOUNDATION
Reel/Frame 036275/0536 →
Continuity (2)
Provisional Application 61978032 · Apr 10, 2014
Related Publication 20150291929A1 · Oct 15, 2015