IP Library Granted Patent US 9,752,035
Granted Patent B2
US 9,752,035 · App. 14/764,929 · Granted Sep 5, 2017

Composite lubricating material, engine oil, grease, and lubricant, and method of producing a composite lubricating material

Inventors: Shoji Hasegawa (Tokyo, JP); Nagisa Kamiya (Tokyo, JP)
Assignee: GRAPHENE PLATFORM CORPORATION
C09C1/46C01B31/04C01B31/0423C01B31/0469C04B14/024C04B28/14C04B35/5611C04B35/6303C04B35/83C08K3/04C08L101/00C09C3/04C09D5/24C09D7/1216C09D11/03C09D11/037C09D11/52C10M125/02C10M169/04H01M4/02H01M4/366H01M4/587H01M4/625H01M10/0525C01P2002/72C01P2002/74C01P2002/77C01P2004/54C01P2004/61C04B2235/425C10M2201/041C10M2203/003C10M2203/022C10M2207/401C10N2230/10C10N2240/10C10N2250/10H01M10/052
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Quick Facts
Patent No.
US 9,752,035
App. No.
14/764,929
Granted
Sep 5, 2017
Kind
B2
Abstract

A composite lubricating material include at least a graphite-based carbon material and/or graphene-like graphite exfoliated from the graphite-based carbon material dispersed in a base material. The graphite-based carbon material is characterized by having a rhombohedral graphite layer ( 3 R) and a hexagonal graphite layer ( 2 H), wherein a Rate ( 3 R) of the rhombohedral graphite layer ( 3 R) and the hexagonal graphite layer ( 2 H), based on an X-ray diffraction method, which is defined by following Equation 1 is 31% or more: Rate ( 3 R)=P 3 /(P 3 +P 4 )×100 . . . Equation 1, wherein, P 3 is a peak intensity of a (101) plane of the rhombohedral graphite layer ( 3 R) based on the X-ray diffraction method, and P 4 is a peak intensity of a (101) plane of the hexagonal graphite layer ( 2 H) based on the X-ray diffraction method.

Claims (13)

1. A composite lubricating material comprising at least a graphene exfoliated from a graphite-based carbon material dispersed in a base oil,

the graphite-based carbon material having a rhombohedral graphite layer ( 3 R) and a hexagonal graphite layer ( 2 H), wherein a Rate ( 3 R) of the rhombohedral graphite layer ( 3 R) and the hexagonal graphite layer ( 2 H), based on an X-ray diffraction method, which is defined by following Equation 1 is 31% or more:

Rate(3 R )= P 3/( P 3+ P 4)×100  Equation 1

wherein

P 3 is a peak intensity of a (101) plane of the rhombohedral graphite layer ( 3 R) based on the X-ray diffraction method, and

P 4 is a peak intensity of a (101) plane of the hexagonal graphite layer ( 2 H) based on the X-ray diffraction method,

the graphene being a crystal of a mean size of 100 nm or more and formed in a flake-like or sheet-like shape having 10 layers or less.

2. The composite lubricating material according to claim 1 , wherein a weight ratio of the graphite-based carbon material to the base material is 1/10,000 or more to less than 1.

3. The composite lubricating material according to claim 1 , wherein the base oil is derived from mineral, synthetic chemicals, plants or animals.

4. The composite lubricating material according to claim 1 , comprising one or more kinds of additives for a purpose of preventing oxidative deterioration.

5. The composite lubricating material according to claim 4 , wherein the additive is a radioactive substance.

6. Engine oil comprising the composite lubricating material according to claim 1 .

7. Grease comprising the composite lubricating material according to claim 1 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 6, 2015
From: HASEGAWA, SHOJI; KAMIYA, NAGISA
To: GRAPHENE PLATFORM CORPORATION
Reel/Frame 036273/0213 →
Priority Claims (2)
WO PCT/JP2014/073838 · Sep 9, 2014 · international
WO PCT/JP2015/055977 · Feb 27, 2015 · international
Continuity (1)
Related Publication 20170175023A1 · Jun 22, 2017