IP Library Granted Patent US 9,791,390
Granted Patent B2
US 9,791,390 · App. 15/004,511 · Granted Oct 17, 2017

Devices and systems for spatial averaging of electron backscatter diffraction patterns

Inventors: Stuart Ian Wright (St. George, UT); Matthew McBride Nowell (Riverton, UT); Scott Perry Lindeman (Lehi, UT); Patrick Paul Camus (Pen Argyl, PA)
Assignee: EDAX, Incorporated
G01N23/20058
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Quick Facts
Patent No.
US 9,791,390
App. No.
15/004,511
Granted
Oct 17, 2017
Kind
B2
Abstract

A diffraction pattern is averaged with adjacent diffraction patterns to increase a signal to noise ratio thereof and improve indexing accuracy. The pixels of a diffraction pattern image are averaged with a correlated pixel from one or more adjacent diffraction patterns. Noise artifacts are reduced in intensity, while signals present in each of the patterns reinforce one another to produce an averaged diffraction pattern which is then indexed.

Claims (39)

1. A method for spatially averaging diffraction patterns comprising:

acquiring a central diffraction pattern and a plurality of adjacent diffraction patterns from an electron backscatter diffraction detector;

averaging the central diffraction pattern with one or more of the plurality of adjacent diffraction patterns to produce an averaged diffraction pattern; and

indexing the averaged diffraction pattern to produce an averaged crystal orientation.

2. The method of claim 1 , acquiring a central diffraction pattern and a plurality of adjacent diffraction patterns further comprising saving the central diffraction pattern and the plurality of adjacent diffraction patterns to a data storage device.

3. The method of claim 1 , averaging the central diffraction pattern with one or more of the plurality of adjacent diffraction patterns further comprising averaging a pixel intensity of the central diffraction pattern with a correlated pixel intensity of the at least one of the plurality of adjacent diffraction patterns.

4. The method of claim 1 , averaging the central diffraction pattern with one or more of the plurality of adjacent diffraction patterns further comprising averaging an electron band position of the central diffraction pattern with a correlated electron band position of the at least one of the plurality of adjacent diffraction patterns.

5. The method of claim 1 , the adjacent diffraction patterns being collected from sampling locations on a hexagonal grid.

6. The method of claim 1 , indexing the averaged diffraction pattern further comprising calculating an averaged confidence index.

7. The method of claim 1 , further comprising indexing the central diffraction pattern to produce a measured crystal orientation.

8. The method of claim 7 , further comprising comparing the measured crystal orientation to the averaged crystal orientation.

9. A system for spatially averaging diffraction patterns comprising:

an electron backscatter detector;

one or more hardware processors in data communication with the electron backscatter detector; and

one or more storage devices having stored computer-executable instructions which, when executed by the one or more hardware processors, are configured to cause the computing system to perform a method including:

acquiring a central diffraction pattern;

acquiring a plurality of adjacent diffraction patterns;

comparing the central diffraction pattern to one or more of the plurality of adjacent diffraction patterns;

averaging at the central diffraction pattern with one or more of the plurality of adjacent diffraction patterns to produce an averaged diffraction pattern; and

indexing the averaged diffraction pattern to produce an averaged crystal orientation.

10. The system of claim 9 , wherein the method further comprises:

indexing the central diffraction pattern to produce a measured crystallographic orientation;

indexing at least one of the plurality of the adjacent diffraction patterns to produce an adjacent crystallographic orientation; and

wherein comparing the central diffraction pattern to one or more of the plurality of adjacent diffraction patterns comprises comparing the measured crystal orientation with the adjacent crystal orientation against a misorientation tolerance.

11. The system of claim 9 , indexing the central diffraction pattern further comprising calculating a measured confidence index.

12. The system of claim 11 , indexing the averaged diffraction pattern further comprising calculating an averaged confidence index, and further comprising comparing the averaged confidence index and the measured confidence index and determining a lower value of the averaged confidence index and the measured confidence index.

13. The system of claim 12 , wherein the method further comprises discarding data associated with the lower value.

14. The system of claim 9 , acquiring a central diffraction pattern further comprising collecting a diffraction pattern from a sample.

15. The system of claim 9 , acquiring a plurality of adjacent diffraction patterns further comprising collecting a plurality of diffraction patterns from a sample.

16. A method for calculating crystallographic orientations comprising:

acquiring a diffraction pattern set having a plurality of diffraction patterns therein;

indexing a plurality of the diffraction patterns to calculate one or more misorientations;

correlating a plurality of misorientations to identify one or more grains;

averaging a central diffraction pattern with one or more adjacent diffraction patterns based upon the one or more grains to produce an averaged diffraction pattern; and

indexing the averaged diffraction pattern to produce an averaged orientation.

17. The method of claim 16 further comprising calculating a confidence index for the averaged diffraction pattern.

18. The method of claim 17 further comprising indexing and calculating a confidence index for the central diffraction pattern, comparing the confidence index for the central diffraction pattern and the confidence index for the averaged diffraction pattern.

19. The method of claim 16 , correlating a plurality of misorientations comprising identifying adjacent misorientations greater than 5°.

20. The method of claim 16 , further comprising collecting a diffraction pattern set with an electron backscatter detector.

Assignments (3)
MERGER Recorded Nov 4, 2025
From: EDAX LLC
To: GATAN INC.
Reel/Frame 072772/0184 →
CHANGE OF NAME Recorded Dec 12, 2024
From: EDAX INC.
To: EDAX, LLC
Reel/Frame 069618/0557 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 22, 2016
From: WRIGHT, STUART IAN; NOWELL, MATTHEW MCBRIDE; LINDEMAN, SCOTT PERRY; CAMUS, PATRICK PAUL
To: EDAX, INCORPORATED
Reel/Frame 037562/0596 →
Continuity (3)
Provisional Application 62106628 · Jan 22, 2015
Provisional Application 62196089 · Jul 23, 2015
Related Publication 20160216219A1 · Jul 28, 2016