IP Library Granted Patent US 9,845,245
Granted Patent B2
US 9,845,245 · App. 14/665,053 · Granted Dec 19, 2017

Foams of graphene, method of making and materials made thereof

Inventors: Daniel Alcazar Jorba (Remich, LU); Edwin Lorimer Thomas (Houston, TX)
Assignee: Massachusetts Institute of Technology
C01B31/0484B01F17/0042B82Y30/00B82Y40/00C01B31/043C01B31/0438
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Quick Facts
Patent No.
US 9,845,245
App. No.
14/665,053
Granted
Dec 19, 2017
Kind
B2
Abstract

Method for making a liquid foam from graphene. The method includes preparing an aqueous dispersion of graphene oxide and adding a water miscible compound to the aqueous dispersion to produce a mixture including a modified form of graphene oxide. A second immiscible fluid (a gas or a liquid) with or without a surfactant are added to the mixture and agitated to form a fluid/water composite wherein the modified form of graphene oxide aggregates at the interfaces between the fluid and water to form either a closed or open cell foam. The modified form of graphene oxide is the foaming agent.

Claims (11)

1. A method for making an open cell foam comprising:

making a liquid foam from graphene;

adding an immiscible fluid that contains a surfactant to produce a 3D bi-continuous fluid/water structure; and

removing volatile components;

wherein making the liquid foam from graphene comprises:

preparing an aqueous dispersion of graphene oxide;

adding a water miscible base compound to the aqueous dispersion of graphene oxide to produce a mixture including a reduced form of graphene oxide;

adding water to the mixture; and

agitating the mixture to produce a foamed phase with the reduced form or graphene oxide as a foaming agent.

2. The method of claim 1 wherein the base compound is isophorone diamine.

3. The method of claim 1 wherein the surfactant is an amphiphilic molecule.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 30, 2017
From: THOMAS, EDWIN LORIMER
To: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Reel/Frame 043451/0497 →
CONFIRMATORY LICENSE Recorded May 8, 2015
From: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 035635/0383 →
Continuity (2)
Division 13517751 · Jun 14, 2012
Related Publication 20150191359A1 · Jul 9, 2015