IP Library Granted Patent US 9,867,784
Granted Patent B2
US 9,867,784 · App. 15/019,195 · Granted Jan 16, 2018

Pharmaceutical formulation containing gelling agent

Inventors: Curtis Wright (Rockport, MA); Benjamin Oshlack (Boca Raton, FL); Christopher Breder (Bethesda, MD)
Assignees: Purdue Pharma L.P.; The P.F. Laboratories, Inc.; Purdue Pharmaceuticals L.P.
A61K9/2054A61J3/10A61K9/0002A61K9/006A61K9/0053A61K9/06A61K9/08A61K9/1635A61K9/1641A61K9/1652A61K9/20A61K9/205A61K9/2009A61K9/2013A61K9/2018A61K9/2027A61K9/2031A61K9/2095A61K9/28A61K9/284A61K9/2806A61K9/2813A61K9/2846A61K9/2853A61K9/2866A61K9/2893A61K9/48A61K9/485A61K9/4808A61K9/4833A61K9/4858A61K9/4866A61K9/4891A61K9/5047A61K9/5078A61K9/5089A61K9/70A61K31/137A61K31/167A61K31/192A61K31/439A61K31/4458A61K31/48A61K31/485A61K45/06A61K47/02A61K47/08A61K47/10A61K47/12A61K47/14A61K47/26A61K47/32A61K47/34A61K47/36A61K47/38
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Quick Facts
Patent No.
US 9,867,784
App. No.
15/019,195
Granted
Jan 16, 2018
Kind
B2
Abstract

Disclosed in certain embodiments is a controlled release oral dosage form comprising a therapeutically effective amount of a drug susceptible to abuse together with one or more pharmaceutically acceptable excipients; the dosage form further including a gelling agent in an effective amount to impart a viscosity unsuitable for administration selected from the group consisting of parenteral and nasal administration to a solubilized mixture formed when the dosage form is crushed and mixed with from about 0.5 to about 10 ml of an aqueous liquid; the dosage form providing a therapeutic effect for at least about 12 hours when orally administered to a human patient.

Claims (24)

1. A method of preparing an abuse deterrent immediate release dosage form comprising:

(i) preparing a mixture comprising an opioid agonist and a gelling agent comprising microcrystalline cellulose and sodium carboxymethylcellulose;

(ii) compressing the mixture into a tablet; and

(iii) coating the tablet with a coating comprising polyvinyl alcohol and polyethylene glycol,

wherein the abuse deterrent dosage form forms a gel unsuitable for parenteral administration when the dosage form is subjected to tampering comprising dissolution in from about 0.5 ml to about 10 ml of an aqueous liquid;

the dosage form having a ratio of gelling agent to opioid agonist from about 1:1 to about 8:1;

the dosage form providing an immediate release of the opioid agonist when orally administered to a human patient; and

wherein the opioid agonist is the sole active agent in the dosage form.

2. The method of claim 1 , wherein the aqueous liquid is water.

3. The method of claim 1 , wherein the dissolution is in from about 1 ml to about 3ml of the aqueous liquid, and wherein the tampering further comprises crushing the dosage form.

4. The method of claim 1 , wherein the gel has a viscosity of about 10 cP or more.

5. The method of claim 1 , wherein the gel has a viscosity of about 60 cP or more.

6. The method of claim 1 , wherein the gel has a viscosity of about 120 cP or more.

7. The method of claim 1 , wherein the gel has a viscosity of about 375 cP or more.

8. The method of claim 1 , wherein the gel has a viscosity of about 2,000 cP or more.

9. The method of claim 1 , wherein the gel has a viscosity from about 120 cP to about 5,000 cP.

10. The method of claim 1 , wherein the opioid agonist is in hydrochloride salt form.

11. The method of claim 1 , wherein the dosage form further comprises polyvinyl pyrrolidone.

12. The method of claim 1 , wherein the dosage form further comprises lactose.

13. The method of claim 10 , wherein the amount of opioid agonist is about 75 ng to about 750 mg.

14. The method of claim 1 , wherein the gel is unsuitable for injection with an insulin syringe.

15. The method of claim 1 , wherein the gel is difficult to pull into an insulin syringe.

16. The method of claim 1 , wherein the gel cannot be filled into an insulin syringe without picking up pockets of air.

17. The method of claim 1 , wherein the gel has a milk like color.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 17, 2019
From: THE P.F. LABORATORIES, INC.; PURDUE PHARMA TECHNOLOGIES, INC.
To: PURDUE PHARMA L.P.
Reel/Frame 048932/0651 →
Continuity (8)
Continuation 14638685 · Mar 4, 2015
Continuation 13946418 · Jul 19, 2013
Continuation 13890874 · May 9, 2013
Continuation 13765368 · Feb 12, 2013
Continuation 12262015 · Oct 30, 2008
Continuation 10214412 · Aug 6, 2002
Provisional Application 60310534 · Aug 6, 2001
Related Publication 20160151277A1 · Jun 2, 2016