IP Library Granted Patent US 9,901,040
Granted Patent B2
US 9,901,040 · App. 14/361,983 · Granted Feb 27, 2018

Cellulose blends with enhanced water retention and their use in irrigation

Inventors: Raed Hashaikeh (Abu Dhabi, AE); Ali Asghar (Abu Dhabi, AE)
Assignee: Khalifa University of Science and Technology
A01G25/00A01G1/00A01G7/00A01G9/1086A01G31/001C05F11/00C05G3/0047C05G3/04C08B16/00C08J3/075C08L1/04C09K17/32C08J2301/04C08J2471/02C08L1/02C09K8/90
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Quick Facts
Patent No.
US 9,901,040
App. No.
14/361,983
Granted
Feb 27, 2018
Kind
B2
Abstract

Water-retaining gel compositions, methods of making water-retaining gel compositions, and the uses thereof for enhancing soils, preparing plant growth media and facilitating the growth of plants therein are disclosed.

Claims (23)

1. A method of making a water-retaining gel composition, comprising:

dissolving hydrolyzed cellulose completely in a dissolution media to form a first mixture;

combining said first mixture with an antisolvent to form a precipitate, said antisolvent comprising a swellable hydrophilic polymer and water;

separating said precipitate from excess antisolvent and excess dissolution media;

optionally adjusting or neutralizing the pH of said precipitate; and

washing said precipitate with water to form said water-retaining gel composition.

2. The method of claim 1 , wherein said gel composition has a pH of from 4 to 9.

3. The method of claim 1 , wherein said hydrophilic polymer comprises polyethylene oxide.

4. The method of claim 1 , further comprising the step of drying said composition.

5. The method of claim 1 , further comprising the step of mixing said precipitate with particulate media to form a mixture thereof.

6. The method of claim 1 , wherein the cellulose comprises microcrystalline cellulose.

7. The method of claim 1 , wherein the dissolution media comprises sulfuric acid.

8. The method of claim 5 , wherein the particulate media comprises sand.

9. A method of making a hygroscopic water-retaining gel composition, comprising:

dissolving hydrolyzed cellulose completely in a dissolution media to form a first mixture;

combining said first mixture with an antisolvent to form a precipitate, said antisolvent comprising polyethylene oxide and water;

separating said precipitate from excess antisolvent and excess dissolution media;

mixing said precipitate with particulate media;

optionally adjusting or neutralizing the pH of said precipitate; and

washing said precipitate with water to form said water-retaining gel composition having a pH of from 4 to 9; and

drying said composition to produce said water-retaining gel hygroscopic composition.

10. The method of claim 9 , wherein said cellulose comprises microcrystalline cellulose, and said dissolution media comprises sulfuric acid.

11. The method of claim 9 , wherein said particulate media comprises sand.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 8, 2018
From: HASHAIKEH, RAED; ASGHAR, ALI
To: KHALIFA UNIVERSITY OF SCIENCE AND TECHNOLOGY
Reel/Frame 045016/0830 →
CHANGE OF NAME Recorded Jun 16, 2017
From: MASDAR INSTITUTE OF SCIENCE AND TECHNOLOGY
To: KHALIFA UNIVERSITY OF SCIENCE AND TECHNOLOGY
Reel/Frame 042874/0552 →
Continuity (2)
Provisional Application 61566180 · Dec 2, 2011
Related Publication 20140326029A1 · Nov 6, 2014