IP Library Granted Patent US 9,962,644
Granted Patent B2
US 9,962,644 · App. 14/980,634 · Granted May 8, 2018

Process for increased selectivity and capacity for hydrogen sulfide capture from acid gases

Inventors: Carla S. Pereira (Somerville, NJ); Michael Siskin (Westfield, NJ); Thomas Ingram (Mannheim, DE); Gerald Vorberg (Speyer, DE); Martin Ernst (Heidelberg, DE)
Assignees: ExxonMobil Research and Engineering Company; BASF
B01D53/1493B01D53/1425B01D53/1468B01D53/18C10L3/10B01D2252/204B01D2252/20431B01D2252/20478B01D2252/20489B01D2257/304B01D2257/504
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Quick Facts
Patent No.
US 9,962,644
App. No.
14/980,634
Granted
May 8, 2018
Kind
B2
Abstract

A process for selectively separating H 2 S from a gas mixture which also comprises CO 2 is disclosed. A stream of the gas mixture is contacted with an absorbent solution comprising one or more amines, alkanolamines, hindered alkanolamines, capped alkanolamines, or mixtures thereof. The H 2 S/CO 2 selectivity of the absorbent solution is preferably greater than about 4.0 for an acid gas loading [mol(CO 2 +H 2 S)/mol(amine)] between about 0.2 and about 0.6, and is achieved by reducing pH of the absorbent solution.

Claims (13)

1. A process for selectively separating H 2 S from a gas mixture which also comprises CO 2 , the process comprising:

contacting a stream of the gas mixture with an absorbent solution comprising methoxyethoxyethoxyethanol-t-butylamine (M3ETB);

wherein the M3ETB concentration in the absorbent solution is between 20 and 30 wt %.

2. The process of claim 1 , wherein the M3ETB concentration in the absorbent solution is between 25 and 30 wt %.

3. The process of claim 1 , wherein the H 2 S/CO 2 selectivity of the absorbent solution is greater than about 5.0 over the entire acid gas loading [mol(CO 2 +H 2 S)/mol(amine)] range between 0.2 and 0.55.

4. The process of claim 1 , wherein the H 2 S/CO 2 selectivity of the absorbent solution is greater than about 6.0 over the entire acid gas loading [mol(CO 2 +H 2 S)/mol(amine)] range between 0.2 and 0.55.

5. The process of claim 1 , wherein the H 2 S/CO 2 selectivity of the absorbent solution is greater than about 7.0 over the entire acid gas loading [mol(CO 2 +H 2 S)/mol(amine)] range between 0.2 and 0.55.

6. A process for selectively separating H 2 S from a gas mixture which also comprises CO 2 , the process comprising:

contacting a stream of the gas mixture with an absorbent solution comprising methoxyethoxyethoxyethanol-t-butylamine (M3ETB);

wherein the M3ETB concentration in the absorbent solution is between 25 and 30 wt %.

7. The process of claim 6 , wherein the H 2 S/CO 2 selectivity of the absorbent solution is greater than about 5.0 over the entire acid gas loading [mol(CO 2 +H 2 S)/mol(amine)] range between 0.2 and 0.55.

8. The process of claim 6 , wherein the H 2 S/CO 2 selectivity of the absorbent solution is greater than about 6.0 over the entire acid gas loading [mol(CO 2 +H 2 S)/mol(amine)] range between 0.2 and 0.55.

9. The process of claim 6 , wherein the H 2 S/CO 2 selectivity of the absorbent solution is greater than about 7.0 over the entire acid gas loading [mol(CO 2 +H 2 S)/mol(amine)] range between 0.2 and 0.55.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 5, 2017
From: PEREIRA, CARLA S.; SISKIN, MICHAEL
To: EXXONMOBIL RESEARCH AND ENGINEERING COMPANY
Reel/Frame 040861/0405 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 5, 2017
From: INGRAM, THOMAS; VORBERG, GERALD; ERNST, MARTIN
To: BASF
Reel/Frame 040861/0656 →
Continuity (1)
Related Publication 20170182455A1 · Jun 29, 2017