Salt bath ferritic nitrocarburizing of brake rotors
View Patent ↗Ferritic nitrocarburized surface treatment of cast iron brake rotors providing oxidation resistance, good braking performance and absence of distortion. Machined brake rotors are pre-heated, then immersed into a high temperature molten nitrocarburizing salt bath for a first predetermined dwell time. After removing the brake rotors from the nitrocarburizing salt bath, the brake rotors are directly immersed into an oxidizing salt bath at a lower temperature than the nitrocarburizing salt bath so that the brake rotors are thermally quenched. After a predetermined second dwell time in the oxidizing salt bath, the brake rotors are removed therefrom and further cooled to room temperature, either by water application thermal quenching or slow cooling in air. A fixture provides stable holding the brake rotors with a minimum of contact during placement in the salt baths.
1. A brake rotor comprising:
a pair of rotor cheeks, each rotor cheek consisting of pearlitic cast iron having a ferritic nitrocarburized surface defined by a compound zone and a diffusion zone, wherein:
said compound zone consists of an oxide layer consisting of Fe 3 O 4 ; and generally subjacent said oxide layer, predominantly epsilon iron nitride Fe 3 N and a smaller volume of gamma prime iron nitride Fe 4 N; and
disposed subjacent said compound zone, said diffusion zone consists of iron base ferrous material with a lower concentration of diffused nitrogen than that of said compound layer with the nitrogen in solid solution with the base ferrous material.
2. The brake rotor of claim 1 , wherein said compound and diffusion zones collectively comprise a case, wherein said compound zone has a depth of substantially 0.015 millimeters, and wherein said diffusion zone has a depth of substantially 0.15 millimeters and wherein said compound zone has a hardness of substantially at least HRC 50 equivalent.
3. The brake rotor of claim 1 , further comprising a hat connected to said pair of rotor cheeks, said hat having an exterior side; further comprising said exterior side of said hat having said ferritic nitrocarburized surface treatment defined by said compound zone and said diffusion zone.
4. The brake rotor of claim 3 , wherein said compound and diffusion zones collectively comprise a case, wherein said compound zone has a depth of substantially 0.015 millimeters, and wherein said diffusion zone has a depth of substantially 0.15 millimeters and wherein said compound zone has a hardness of substantially at least HRC 50 equivalent.
5. A brake rotor made according to a method comprising the steps of:
casting a cast iron brake rotor having mutually opposed first and second rotor cheeks;
providing a nitrocarburizing salt bath;
providing an oxidizing salt bath;
pre-heating the brake rotor to a first predetermined temperature;
immersing the brake rotor into the nitrocarburizing salt bath, wherein the nitrocarburizing salt bath is at a second predetermined temperature, and wherein the brake rotor is placed into the nitrocarburizing salt bath such that all surfaces of the first and second rotor cheeks are in contact with the nitrocarburizing salt bath;
removing the brake rotor from the nitrocarburizing salt bath after a first predetermined dwell time;
immersing the brake rotor into the oxidizing salt bath, wherein the oxidizing salt bath is at a third predetermined temperature, and wherein the brake rotor is placed into the oxidizing salt bath such that all surfaces of the first and second rotor cheeks are in contact with the oxidizing salt bath;
removing the brake rotor from the oxidizing salt bath after a second predetermined dwell time; and
cooling the brake rotor to substantially room temperature;
wherein the brake rotor made according to said method consists of pearlitic cast iron which, as a result of said method, the brake rotor has a ferritic nitrocarburized surface defined by a compound zone and a diffusion zone, wherein:
said compound zone consists of an oxide layer consisting of Fe 3 O 4 ; and generally subjacent said oxide layer, predominantly epsilon iron nitride Fe 3 N and a smaller volume of gamma prime iron nitride Fe 4 N; and
disposed subjacent said compound zone, said diffusion zone consists of iron base ferrous material with a lower concentration of diffused nitrogen than that of said compound layer with the nitrogen in solid solution with the base ferrous material.