IP Library Granted Patent US 10,071,521
Granted Patent B2
US 10,071,521 · App. 14/978,091 · Granted Sep 11, 2018

Method and apparatus for processing dielectric materials using microwave energy

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Quick Facts
Patent No.
US 10,071,521
App. No.
14/978,091
Granted
Sep 11, 2018
Kind
B2
Abstract

Methods and systems are provided for heating a dielectric preform material. An exemplary method includes inserting the preform material into a microwave cavity along a longitudinal axis of the microwave cavity and supplying the microwave cavity with microwave power having a frequency that corresponds to an axial wavelength along the longitudinal axis of the microwave cavity. The axial wavelength is greater than a length of the preform material along the longitudinal axis. The method includes heating the preform material within the microwave cavity by the microwave power and determining temperatures of the preform material at one or more locations on a surface of the preform material. The method further includes adjusting, based on the temperatures of the preform material, the microwave frequency to achieve substantially uniform heating at least on a sidewall of the preform material along the longitudinal axis.

Claims (28)

1. A method for heating a dielectric preform material, the method comprising:

inserting the preform material into a microwave cavity along a longitudinal axis of the microwave cavity;

supplying the microwave cavity with microwave power having a frequency that corresponds to an axial wavelength along the longitudinal axis of the microwave cavity, the axial wavelength greater than a length of the preform material along the longitudinal axis;

heating the preform material within the microwave cavity by the microwave power; and

during the heating, performing steps including:

determining temperatures of the preform material at one or more locations on a surface of the preform material; and

adjusting, in response to a change in the temperatures of the preform material, the microwave frequency to achieve uniform heating at least on a sidewall of the preform material along the longitudinal axis, the adjusting of the microwave frequency based on the change in the temperatures adapted to maintain the axial wavelength of the microwave power to greater than the length of the preform material, which corresponds to uniform electric field and uniform heating along the longitudinal axis of the microwave cavity.

2. The method of claim 1 , wherein adjusting the microwave frequency comprises maintaining the microwave frequency to be the same as a cutoff frequency of the TM 01 mode of the microwave cavity.

3. The method of claim 1 , further comprising inserting a dielectric spacer into the microwave cavity adjacent to the preform material to enhance the uniform electric field, if the preform material has a non-uniform thickness along the longitudinal axis.

4. The method of claim 1 , further comprising constructing the microwave cavity with varying cavity radii along the longitudinal axis to enhance the uniform electric field, if the perform material has a non-uniform thickness or shape along the longitudinal axis.

5. The method of claim 4 , further comprising increasing the cavity radius where the thickness of the preform material is smaller and decreasing the cavity radius where the thickness of the preform material is larger.

6. The method of claim 1 , wherein determining the temperatures of the preform material comprises:

positioning two or more temperature sensors at the one or more locations along the length of the preform material; and

measuring the temperatures by the two or more temperature sensors.

7. The method of claim 1 , wherein adjusting the microwave frequency comprises tuning the microwave frequency in response to the change in the temperatures of the preform material, which causes a change in a dielectric constant of the preform material during heating.

8. The method of claim 7 , wherein adjusting the microwave frequency comprises decreasing the microwave frequency with an increase in the dielectric constant of the preform material to maintain the uniform electric field.

9. The method of claim 1 , wherein adjusting the microwave frequency comprises tuning the microwave frequency based on a temperature gradient of the preform material during heating.

10. The method of claim 1 , further comprising coupling the microwave power via at least one annular inlet positioned along the length of the microwave cavity.

11. The method of claim 1 , further comprising

determining, during heating, an electric field gradient based on electric field measurements taken at one or more locations in the microwave cavity; and

adjusting, based on the electric field gradient, the microwave frequency to maintain the uniform electric field in the microwave cavity.

12. The method of claim 1 , further comprising positioning a microwave choke outside of an opening of the microwave cavity to reduce leakage of the microwave power from the microwave cavity.

13. The method of claim 1 , further comprising adjusting the microwave power to maintain a heating rate of the preform material to within a predetermined range.

14. The method of claim 1 , wherein the microwave frequency is between 2.40 giga Hertz (GHz) and 2.50 GHz.

15. The method of claim 1 , wherein the microwave power is between 100 Watts and 3000 Watts.

16. The method of claim 1 , further comprising adjusting, based on at least one of the temperatures of the preform material or efficiency of microwave power absorption, the microwave power to optimize at least one of a heating rate or energy efficiency.

17. The method of claim 2 , further comprising tuning the microwave frequency to deviate from the cutoff frequency for correcting non-uniformity in the temperatures at least on the sidewall of the preform material.

18. The method of claim 1 , further comprising positioning a dielectric spacer adjacent to a closed end of the preform material to increase electric field near the closed end.

Assignments (9)
RELEASE OF SECURITY INTEREST Recorded Aug 24, 2022
From: BARCLAYS BANK PLC
To: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION; ELECTRO SCIENTIFIC INDUSTRIES, INC.
Reel/Frame 063009/0001 →
RELEASE OF SECURITY INTEREST Recorded Aug 24, 2022
From: BARCLAYS BANK PLC
To: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION; ELECTRO SCIENTIFIC INDUSTRIES, INC.
Reel/Frame 062739/0001 →
SECURITY INTEREST Recorded Aug 19, 2022
From: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION; ELECTRO SCIENTIFIC INDUSTRIES, INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 061572/0069 →
CORRECTIVE ASSIGNMENT TO CORRECT THE REMOVE U.S. PATENT NO.7,919,646 PREVIOUSLY RECORDED ON REEL 048211 FRAME 0312. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT SECURITY AGREEMENT (ABL). Recorded Jan 14, 2021
From: ELECTRO SCIENTIFIC INDUSTRIES, INC.; MKS INSTRUMENTS, INC.; NEWPORT CORPORATION
To: BARCLAYS BANK PLC, AS COLLATERAL AGENT
Reel/Frame 055668/0687 →
PATENT SECURITY AGREEMENT (ABL) Recorded Feb 1, 2019
From: ELECTRO SCIENTIFIC INDUSTRIES, INC.; MKS INSTRUMENTS, INC.; NEWPORT CORPORATION
To: BARCLAYS BANK PLC, AS COLLATERAL AGENT
Reel/Frame 048211/0312 →
RELEASE OF SECURITY INTEREST Recorded Feb 1, 2019
From: DEUTSCHE BANK AG NEW YORK BRANCH
To: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION
Reel/Frame 048226/0095 →
SECURITY AGREEMENT Recorded May 4, 2016
From: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION
To: DEUTSCHE BANK AG NEW YORK BRANCH
Reel/Frame 038663/0265 →
SECURITY AGREEMENT Recorded May 4, 2016
From: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION
To: BARCLAYS BANK PLC; BARCLAYS BANK PLC
Reel/Frame 038663/0139 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 19, 2016
From: CHEN, XING; LAM, DAVID; WENZEL, KEVIN W.; POKIDOV, ILYA
To: MKS INSTRUMENTS, INC.
Reel/Frame 037519/0021 →