IP Library Granted Patent US 11,591,315
Granted Patent B2
US 11,591,315 · App. 17/179,705 · Granted Feb 28, 2023

Substituted pyrazole-pyrimidines, variants thereof, and uses therefore

Inventors: Ronald Charles Hawley (San Mateo, CA); Prabha Ibrahim (San Mateo, CA); Anthony P. Ford (Palto Alto, CA); Joel R. Gever (Palo Alto, CA)
Assignee: Merck Sharp & Dohme LLC
C07D403/12
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Quick Facts
Patent No.
US 11,591,315
App. No.
17/179,705
Granted
Feb 28, 2023
Kind
B2
Abstract

Disclosed herein are substituted pyrazole-pyrimidine compounds of Formula I and variants thereof for the treatment, for example, of diseases associated with P2X purinergic receptors: In one embodiment, the P2X3 and/or P2X2/3 antagonists disclosed herein are potentially useful, for example, for the treatment of visceral organ, cardiovascular and pain-related diseases, conditions and disorders.

Claims (45)

1. A compound of Formula I:

or a pharmaceutically acceptable salt thereof, wherein:

ring

is selected from the group consisting of:

W is CH 2 , NH, N—C 1-6 alkylene, O or S;

X 6 is N;

Y is hydrogen or —NHR d ; wherein R d is selected from the group consisting of hydrogen, C 1-12 alkyl, C 3-12 cycloalkyl, aryl, and heteroaryl; wherein each of the C 1-12 alkyl, C 3-12 cycloalkyl, aryl, and heteroaryl is optionally substituted with one to three substituents independently selected from halogen, hydroxyl and C 1-6 alkyl;

D is an optional oxygen;

each occurrence of R 1 is independently selected from the group consisting of hydrogen, hydroxyl, C 1-6 alkyl, C 2-6 alkenyl, and C 2-6 alkynyl; wherein each of the C 1-6 alkyl, C 2-6 alkenyl, and C 2-6 alkynyl is optionally substituted with one to three substituents independently selected from halogen and hydroxyl;

each occurrence of R 2 is independently selected from the group consisting of hydrogen, halogen, —NH—R f , —C(O)—NHR f , —C(O)—C 1-12 alkyl, C 2-12 alkenyl, C 2-12 alkynyl, and —O—C 1-12 alkyl;

each occurrence of R f is independently selected from the group consisting of hydrogen, C 1-12 alkyl, hydroxyl, —SO 2 —NH 2 , and —SO 2 —C 1-6 alkyl; and

R 7 is selected from the group consisting of hydrogen, C 1-12 alkyl, and C 3-12 cycloalkyl.

2. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein:

W is CH 2 or O;

X 6 is N;

Y is hydrogen or —NHR d ; wherein R d is selected from the group consisting of hydrogen or C 1-6 alkyl; wherein the C 1-6 alkyl is optionally substituted with one to three substituents independently selected from halogen and hydroxyl;

D is absent;

each occurrence of R 1 is independently selected from the group consisting of hydrogen and C 1-6 alkyl;

each occurrence of R 2 is independently selected from the group consisting of hydrogen, halogen, —NH—R f , —C(O)—NHR f , —C(O)—C 1-6 alkyl, C 2-6 alkenyl, and —O—C 1-6 alkyl;

each occurrence of R f is independently selected from the group consisting of hydrogen, C 1-6 alkyl, hydroxyl, —SO 2 —NH 2 , and —SO 2 —C 1-6 alkyl; and

R 7 is selected from the group consisting of hydrogen and C 1-6 alkyl.

3. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, having formulae Ia:

4. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein:

W is CH 2 or O;

R 1 is selected from the group consisting of hydrogen and C 1-6 alkyl;

R 2 is selected from the group consisting of hydrogen, halogen, —NH 2 ; —C(O)—NH 2 , —C(O)—C 1-6 alkyl, and —O—C 1-6 alkyl; and

R d is selected from the group consisting of hydrogen and C 1-6 alkyl,

or a pharmaceutically acceptable salt thereof.

5. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, having the following formula Ic or the following formula Id:

6. The compound of claim 5 or a pharmaceutically acceptable salt thereof, wherein:

W is CH 2 or O;

R 1 is selected from the group consisting of hydrogen and C 1-6 alkyl;

R 2 is selected from the group consisting of hydrogen, halogen, —NH 2 , —C(O)—NH 2 , —C(O)—C 1-6 alkyl, and —O—C 1-6 alkyl; and

R d is selected from the group consisting of hydrogen and C 1-6 alkyl,

or a pharmaceutically acceptable salt thereof.

7. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein W is O.

8. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein W is CH 2 .

9. A composition which comprises an inert carrier and a compound of claim 1 or a pharmaceutically acceptable salt thereof.

10. A compound of claim 1 or a pharmaceutically acceptable salt thereof for use in therapy.

11. The compound of claim 3 or a pharmaceutically acceptable salt thereof, wherin

W is CH 2 or O;

R 1 is selected from the group consisting of hydrogen and C 1-6 alkyl;

R 2 is selected from the group consisting of hydrogen, halogen, —NH 2 ; —C(O)—NH 2 , —C(O)—C 1-6 alkyl, and —O—C 1-6 alkyl; and

R d is selected from the group consisting of hydrogen and C 1-6 alkyl.

12. The compound of claim 11 or a pharmaceutically acceptable salt thereof, wherein W is CH 2 .

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE APPLICATION NUMBER 17197705 PREVIOUSLY RECORDED AT REEL: 061574 FRAME: 0579. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT . Recorded Dec 1, 2022
From: AFFERENT PHARMACEUTICALS, INC.
To: AFFERENT PHARMACEUTICALS, INC.
Reel/Frame 062036/0001 →
CHANGE OF ADDRESS Recorded Sep 30, 2022
From: AFFERENT PHARMACEUTICALS, INC.
To: AFFERENT PHARMACEUTICALS, INC.
Reel/Frame 061574/0579 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 19, 2021
From: HAWLEY, RONALD CHARLES; IBRAHIM, PRABHA; FORD, ANTHONY P.; GEVER, JOEL R.
To: AFFERENT PHARMACEUTICALS INC.
Reel/Frame 055331/0987 →
Continuity (3)
Continuation 16468446
Provisional Application 62434513 · Dec 15, 2016
Related Publication 20210171505A1 · Jun 10, 2021