Granted Patent B2

US 6,844,259 · App. 10/331,724 · Granted Jan 18, 2005

Abstract

Claims (23)

1. A method for forming a contact plug in a semiconductor device, comprising the steps of:

forming a contact hole by etching an insulating layer on a substrate;

forming a first silicon film with a first doping concentration on the substrate in the contact hole so that the contact hole is partially filled;

flushing a doping gas on a surface of the first silicon film; and

forming a second silicon film having a second doping concentration higher than the first doping concentration on the first silicon film until filling the contact hole.

2. The method as recited in claim 1 , wherein the step of flushing the doping gas is proceeded in an in-situ environment after forming the first silicon film.

3. The method as recited in claim 1 , wherein the step of flushing the doping gas is carried out for about 5 seconds to 20 seconds while flowing about 20 sccm to about 500 sccm of the doping gas obtained by adding PH 3 to hydrogen.

4. The method as recited in claim 1 , wherein the step of flushing the doping gas is carried out at the identical temperature and pressure implemented for forming the first silicon film.

5. The method as recited in claim 1 , further comprising the step of cleaning the contact hole after forming the contact hole.

6. The method as recited in claim 1 , wherein the step of cleaning the contact hole includes the steps of:

performing a first cleaning in an ex-situ environment; and

performing a second cleaning in an in-situ environment.

7. The method as recited in claim 6 , wherein the step of performing the second cleaning is proceeded at a single wafer-type deposition equipment.

8. The method as recited in claim 6 , wherein the step of performing the second cleaning is proceeded by descending a temperature ascended instantaneously up to about 900° C. to about 950° C. with a heating rate ranging from about 10° C. per second to about 100° C. per second in an atmosphere of hydrogen.

9. The method as recited in claim 6 , wherein the step of performing the first cleaning is proceeded with a wet dip process.

10. The method as recited in claim 1 , wherein the first silicon film is formed in a single wafer-type chemical vapor deposition equipment in an in-situ environment.

11. The method as recited in claim 1 , wherein the first silicon film is deposited at a pressure ranging from about 5 Torr to about 50 Torr and a temperature ranging from about 500° C. to about 650° C. by providing a mixed gas of SiH 4 , H 2 and about 1% of PH 3 added to the H 2 .

12. The method as recited in claim 11 , wherein the SiH 4 , the H 2 and the mixed gas has a flow quantity ranging from about 50 sccm to about 300 sccm, from about 500 sccm to about 10000 sccm and from about 10 sccm to about 50 sccm, respectively.

13. The method as recited in claim 1 , wherein the first doping concentration ranges from about 1×10 19 atoms/cm 3 to about 21×10 20 atoms/cm 3 .

14. The method as recited in claim 1 , wherein the second silicon film is formed in a tube-type chemical vapor deposition equipment.

15. The method as recited in claim 1 , wherein the second silicon film is deposited at a pressure ranging from about 0.1 Torr to about 1 Torr and a temperature ranging from about 510° C. to about 610° C. while providing a mixed gas of SiH 4 , H 2 and about 1% of PH 3 added to the H 2 .

16. The method as recited in claim 1 , wherein the SiH 4 , the H 2 and the mixed gas has a flow quantity ranging from about 200 sccm to about 2000 sccm, from about 500 sccm to about 5000 sccm and from about 100 sccm to about 1000 sccm, respectively.

17. The method as recited in claim 1 , wherein the second predetermined concentration ranges from about 1×10 20 atoms/cm 3 to about 31×10 21 atoms/cm 3 .

Assignments (8)