IP Library Granted Patent US 7,407,529
Granted Patent B1
US 7,407,529 · App. 11/027,874 · Granted Aug 5, 2008

System and method for reducing thermal shock in a hydrogen diffusion cell

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Quick Facts
Patent No.
US 7,407,529
App. No.
11/027,874
Granted
Aug 5, 2008
Kind
B1
Abstract

A system and method of purifying hydrogen gas. The system includes heating elements for heating the hydrogen diffusion cell to a predetermined operational temperature. A preheater is provided for heating unpurified gases that will enter the hydrogen diffusion cell. The unpurified gases are heated to the operational temperature of the hydrogen diffusion cell before entering the hydrogen diffusion cell. In this manner, the inflow of unpurified gases into the hydrogen diffusion cell does not cause any thermal shock to the hydrogen diffusion cell. The incoming unpurified gases are heated in two ways. The unpurified gases are heated in a preheater. The unpurified gases are also heated in a heat exchanger. The heat exchanger recycles the heat from the purified hydrogen gas.

Claims (25)

1. A system comprising:

a hydrogen diffusion cell having an input port for receiving unpurified gas and an output port for emitting purified hydrogen;

a heat exchanger through which both said unpurified gas and said hydrogen gas pass, wherein heat is exchanged between said hydrogen gas and said unpurified gas without said hydrogen gas and said unpurified gas mixing;

at least one heating element for heating said hydrogen diffusion cell to a predetermined operational temperature; and

a preheater, disposed between said heat exchanger and said hydrogen diffusion cell, for heating said unpurified gas to said operational temperature prior to said unpurified gas entering said input port of said hydrogen diffusion cell.

2. The system according to claim 1 , wherein said preheater is heated by said at least one heating element that also heats said hydrogen diffusion cell.

3. The system according to claim 1 , wherein said preheater includes tubing that contacts said at least one heating element, and wherein said unpurified gas passes through said tubing to reach said input port of said hydrogen diffusion cell.

4. The system according to claim 3 , wherein said at least one heating element is interposed between said tubing and said hydrogen diffusion cell.

5. In a hydrogen purification system that uses a hydrogen diffusion cell, wherein the hydrogen diffusion cell separates hydrogen gas from unpurified gases, a method of thermal preparation comprising the steps of:

heating said hydrogen diffusion cell to an operational temperature;

introducing unpurified gases into said hydrogen diffusion cell, wherein said hydrogen diffusion cell separates hydrogen gas from said unpurified gases;

providing a heat exchanger through which both said unpurified gas and said hydrogen gas pass, wherein heat is exchanged between said hydrogen gas and said unpurified gas without said hydrogen gas and said unpurified gas mixing; and

providing a preheater, disposed between said heat exchanger and said hydrogen diffusion cell, for heating said unpurified gases to said operational temperature before said unpurified gases enter said hydrogen diffusion cell.

6. The method according to claim 5 , wherein said step of heating said hydrogen diffusion cell includes placing at least one heating element in contact with said hydrogen diffusion cell.

7. The method according to claim 6 , wherein said preheater includes tubing that contacts said at least one heating element being used to heat said hydrogen diffusion cell.

8. The method according to claim 5 , wherein said heat exchanger includes passes said hydrogen gas through a first tube and passes said unpurified gases through a second tube, wherein said first tube is disposed within said second tube.

9. A method of operation for a hydrogen purification system, said method comprising the steps of:

providing a hydrogen diffusion cell;

heating said hydrogen diffusion cell to a predetermined operational temperature;

providing unpurified gases to said hydrogen diffusion cell, wherein said hydrogen diffusion cell separates hydrogen gas from said unpurified gases;

providing a heat exchanger through which both said unpurified gas and said hydrogen gas pass, wherein heat is exchanged between said hydrogen gas and said unpurified gas without said hydrogen gas and said unpurified gas mixing; and

providing a preheater, disposed between said heat exchanger and said hydrogen diffusion cell, for heating said unpurified gases to said operational temperature before said unpurified gases enter said hydrogen diffusion cell.

10. The method according to claim 9 wherein said step of heating said hydrogen diffusion cell to a predetermined operational temperature includes bringing said hydrogen diffusion cell into direct contact with at least one heating element.

11. The method according to claim 10 , wherein said preheater includes tubing that is heated by said at least one heating element.

12. The method according to claim 9 , wherein said heat exchanger heats said unpurified gas to an elevated temperature below said operational temperature.

Assignments (6)
CHANGE OF NAME Recorded Mar 4, 2026
From: SAES PURE GAS, INC.
To: ENTEGRIS GP, INC.
Reel/Frame 073971/0763 →
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.; CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: TRUIST BANK, AS NOTES COLLATERAL AGENT
Reel/Frame 060613/0072 →
ASSIGNMENT OF PATENT SECURITY INTEREST RECORDED AT REEL/FRAME 048811/0679 Recorded Nov 5, 2019
From: GOLDMAN SACHS BANK USA
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 050965/0035 →
SECURITY INTEREST Recorded Nov 13, 2018
From: ENTEGRIS, INC.; SAES PURE GAS, INC.
To: GOLDMAN SACHS BANK USA
Reel/Frame 048811/0679 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2013
From: POWER & ENERGY, INC.
To: SAES PURE GAS, INC.
Reel/Frame 031782/0052 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 30, 2008
From: BOSSARD, PETER
To: POWER & ENERGY, INC.
Reel/Frame 021185/0154 →