IP Library Granted Patent US 7,396,385
Granted Patent B1
US 7,396,385 · App. 11/097,535 · Granted Jul 8, 2008

System and method for efficiently separating hydrogen gas from a mixed gas source

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Quick Facts
Patent No.
US 7,396,385
App. No.
11/097,535
Granted
Jul 8, 2008
Kind
B1
Abstract

A hydrogen purification system that is used to separate hydrogen gas from a source gas. The hydrogen purification system has a hydrogen separator into which the source gas is permitted to flow. Within the hydrogen separator is at least one hydrogen permeable tube that is made of a hydrogen permeable material. A support tube is provided for each hydrogen permeable tube. A support tube is coaxially aligned with the hydrogen permeable tube, wherein a gap space exists between the hydrogen permeable tube and the support tube in an area of overlap. The source gas is introduced into the gap space. The source gas spreads thinly over the hydrogen permeable tube in the gap space. Hydrogen from the source gas passes through the hydrogen permeable tube in a highly efficient manner and is collected.

Claims (26)

1. A method of separating hydrogen gas from a source gas, comprising the steps of:

providing a hydrogen permeable tube;

providing a support tube, wherein said hydrogen permeable tube is disposed within said support tube and wherein said hydrogen permeable tube and said support tube are coaxially aligned so that a gap space exists between said hydrogen permeable tube and said support tube; and

passing the source gas through said gap space between said hydrogen permeable tube and said support tube, wherein hydrogen from said source gas passes through said hydrogen permeable tube and is separated from said source gas.

2. The method according to claim 1 , wherein said hydrogen permeable tube has a predetermined wall thickness.

3. The method according to claim 2 , wherein said gap space is between two times and ten times said predetermined wall thickness.

4. The method according to claim 1 , wherein said support tube is disposed within said hydrogen permeable tube.

5. The method according to claim 1 , wherein said step of providing a hydrogen permeable tube, includes providing a plurality of hydrogen permeable tubes, wherein said plurality of hydrogen permeable tubes communicate with a first common chamber.

6. The method according to claim 5 , wherein said step of providing a support tube includes providing a separate support tube for each of said hydrogen permeable tubes.

7. The method according to claim 1 , further including the step of passing said source gas through a catalyst prior to said source gas entering said gap space.

8. The method according to claim 1 , further including the step of passing said source gas through a catalyst within said gap space.

9. A method of separating hydrogen gas from a source gas, comprising the steps of:

providing a hydrogen permeable tube;

providing a support tube, wherein said hydrogen permeable tube and said support tube overlap and are coaxially aligned so that a gap space exists between said hydrogen permeable tube and said support tube;

passing said source gas through a catalyst; and

passing the source gas through said gap space between said hydrogen permeable tube and said support tube after passing through said catalyst, wherein hydrogen from said source gas passes through said hydrogen permeable tube and is separated from said source gas.

10. A hydrogen separator for separating hydrogen gas from a source gas, said hydrogen separator comprising:

a hydrogen permeable tube having an open first end and a closed second end, wherein said hydrogen permeable tube extends inside said support tube, and wherein said hydrogen permeable tube is made of a hydrogen permeable material; and

a support tube coaxially aligned with said hydrogen permeable tube, wherein a gap space exists between said hydrogen permeable tube and said support tube;

wherein the source gas is introduced into said gap space by flowing through said support tube and hydrogen from said source gas passes through said hydrogen permeable tube from said gap space and is collected.

11. The separator according to claim 1 , wherein said hydrogen permeable tube has a predetermined wall thickness and said gap is between two times and ten times said predetermined wall thickness.

12. The separator according to claim 1 , having a plurality of hydrogen permeable tubes that all communicate with a first common chamber, wherein said plurality of hydrogen permeable tubes are coaxially aligned with separate support tubes.

13. The separator according to claim 12 , wherein each of said support tubes communicates with a second common chamber.

14. The separator according to claim 1 , further including a catalyst material, wherein said source gas flows through said catalyst material within said hydrogen separator.

15. The separator according to claim 14 , wherein at least some of said catalyst material is present within said gap space.

16. The separator according to claim 1 , further including at least one heating element for heating said hydrogen permeable tube to a predetermined operating temperature.

Assignments (6)
CHANGE OF NAME Recorded Mar 4, 2026
From: SAES PURE GAS, INC.
To: ENTEGRIS GP, INC.
Reel/Frame 073971/0763 →
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.; CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: TRUIST BANK, AS NOTES COLLATERAL AGENT
Reel/Frame 060613/0072 →
ASSIGNMENT OF PATENT SECURITY INTEREST RECORDED AT REEL/FRAME 048811/0679 Recorded Nov 5, 2019
From: GOLDMAN SACHS BANK USA
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 050965/0035 →
SECURITY INTEREST Recorded Nov 13, 2018
From: ENTEGRIS, INC.; SAES PURE GAS, INC.
To: GOLDMAN SACHS BANK USA
Reel/Frame 048811/0679 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2013
From: POWER & ENERGY, INC.
To: SAES PURE GAS, INC.
Reel/Frame 031782/0052 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 12, 2013
From: METTES, JACQUES
To: POWER & ENERGY, INC.
Reel/Frame 031191/0560 →