IP Library › Granted Patent US 7,807,217
Granted Patent B2
US 7,807,217 · App. 11/481,388 · Granted Oct 5, 2010

Method of producing self-assembled cubic FePt nanoparticles and apparatus using same

Assignee: Seagate Technology LLC
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Quick Facts
Patent No.
US 7,807,217
App. No.
11/481,388
Granted
Oct 5, 2010
Kind
B2
Abstract

A method comprises: heating a solution of platinum acetylacetonate, Fe(CO) 5 , oleic acid, and oleylamine in dichlorobenzene to a reflux temperature, refluxing the solution, and using the solution to deposit FePt nanoparticles. A magnetic storage medium that includes cubic FePt particles is also provided.

Claims (24)

1. A method comprising:

heating a solution of platinum acetylacetonate, iron pentacarbonyl, oleic acid, and oleylamine in dichlorobenzene to a reflux temperature;

refluxing the solution; and

using the solution to deposit substantially cubic shaped FePt nanoparticles onto a surface, wherein the nanoparticles have facets parallel to (001) crystalline planes and have [100] axes perpendicular to the surface.

2. The method of claim 1 , wherein:

the solution is heated at 4° C. per minute.

3. The method of claim 1 , wherein:

the concentration of the platinum (II) acetylacetonate is 0.5 mmol., the concentration of the Fe(CO) 5 is 0.5 mmol., the concentration of the oleic acid is 4 mmol., and the concentration of the oleylamine is 4 mmol.

4. The method of claim 1 , wherein:

the reflux temperature is 170° C.

5. The method of claim 1 , wherein:

the solution is refluxed for 24 hours.

6. The method of claim 1 , wherein:

the method forms a colloidal solution of the FePt nanoparticles coated with a layer of mixed oleic acid and oleylamine.

7. The method of claim 6 , further comprising:

washing the colloidal solution.

8. The method of claim 6 , further comprising:

adding a 50:50 mixture of hexane to the washed colloidal solution to redisperse the FePt nanoparticles.

9. The method of claim 1 , further comprising:

depositing the FePt nanoparticles in a locking pattern on a substrate.

10. The method of claim 1 , wherein:

the FePt nanoparticles are self-assembled by placing a drop of the refluxed solution onto carbon-coated copper grids and allowing the solvent to dry.

11. The method of claim 1 , wherein:

the concentration of the FePt nanoparticle is approximately 2 mg/ml.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded Jul 23, 2025
From: THE BANK OF NOVA SCOTIA
To: SEAGATE TECHNOLOGY PUBLIC LIMITED COMPANY; SEAGATE TECHNOLOGY; SEAGATE TECHNOLOGY HDD HOLDINGS; I365 INC.; SEAGATE TECHNOLOGY LLC; SEAGATE TECHNOLOGY INTERNATIONAL; SEAGATE HDD CAYMAN; SEAGATE TECHNOLOGY (US) HOLDINGS, INC.
Reel/Frame 072193/0001 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS Recorded Jul 19, 2013
From: WELLS FARGO BANK, NATIONAL ASSOCIATION, AS COLLATERAL AGENT AND SECOND PRIORITY REPRESENTATIVE
To: SEAGATE TECHNOLOGY LLC; EVAULT INC. (F/K/A I365 INC.); SEAGATE TECHNOLOGY INTERNATIONAL; SEAGATE TECHNOLOGY US HOLDINGS, INC.
Reel/Frame 030833/0001 →
SECURITY AGREEMENT Recorded Mar 24, 2011
From: SEAGATE TECHNOLOGY LLC
To: THE BANK OF NOVA SCOTIA, AS ADMINISTRATIVE AGENT
Reel/Frame 026010/0350 →
RELEASE Recorded Jan 19, 2011
From: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: SEAGATE TECHNOLOGY HDD HOLDINGS; MAXTOR CORPORATION; SEAGATE TECHNOLOGY LLC; SEAGATE TECHNOLOGY INTERNATIONAL
Reel/Frame 025662/0001 →
SECURITY AGREEMENT Recorded May 15, 2009
From: MAXTOR CORPORATION; SEAGATE TECHNOLOGY LLC; SEAGATE TECHNOLOGY INTERNATIONAL
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT AND FIRST PRIORITY REPRESENTATIVE; WELLS FARGO BANK, NATIONAL ASSOCIATION, AS COLLATERAL AGENT AND SECOND PRIORITY REPRESENTATIVE
Reel/Frame 022757/0017 →
RERECORD TO CORRECT ASSIGNORS NAME PREVIOUSLY RECORDED AT REEL/FRAME 018360/0703. Recorded Oct 17, 2006
From: KLEMMER, TIMOTHY JOHN; WELLER, DIETER KLAUS; LIU, CHAO
To: SEAGATE TECHNOLOGY LLC
Reel/Frame 018404/0356 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 4, 2006
From: KLEMMER, TIMOTHY JOHN; KLAUS, DIETER; LIU, CHAO
To: SEAGATE TECHNOLOGY LLC
Reel/Frame 018360/0703 →
Continuity (1)
Related Publication 20100080895A1 · Apr 1, 2010