IP Library Granted Patent US 8,283,296
Granted Patent B2
US 8,283,296 · App. 11/545,883 · Granted Oct 9, 2012

Lubricant for hot forging applications

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Quick Facts
Patent No.
US 8,283,296
App. No.
11/545,883
Granted
Oct 9, 2012
Kind
B2
Abstract

A substantially lead-free lubricant for use in hot forging of metals, especially forging of aluminum and aluminum alloy components. The lubricant comprises one or more oils, graphite, and one or more phosphorus-based additives. Additional additives, such as metallic lubricants and dispersants may also be included. The lubricant does not burn when subjected to temperatures in excess of 300° C.

Claims (30)

1. A method of hot forging an aluminum or aluminum alloy comprising the steps of a) applying a coating of a lead-free lubricant to one or both of a hot forging apparatus or a workpiece, inserting the workpiece into the apparatus and forging an article from the workpiece or b) inserting a workpiece into a hot forging apparatus, simultaneously lubricating the workpiece and the hot forging apparatus, and forging the workpiece, wherein the lead-free lubricant comprises about 15 to about 40 weight percent of one or more oils including at least one mineral oil, fine graphite having a particle size distribution with about 90% of the particles below 15 microns in size, and 30 to 80 weight percent of one or more phosphate esters.

2. The method of claim 1 , the lubricant further comprising one or more metallic lubricating additives.

3. The method of claim 2 , wherein the one or more metallic additives are selected from the group consisting of bismuth, zinc, tin, aluminum or any alloys thereof.

4. The method of claim 1 , wherein the graphite comprises in the range of about 1 to about 30 weight percent of the lubricant.

5. The method of claim 1 , wherein the graphite comprises in the range of about 3 to about 20 weight percent of the lubricant.

6. The method of claim 1 , the lubricant further comprising one or more of the group consisting of dispersants, rheology modifiers, biocides, anticorrosives, extreme pressure additives, antifoam agents, wetting agents, metal soaps or mixtures thereof.

7. The method of claim 1 , wherein the phosphate esters are selected such that the lubricant does not burn at temperatures greater than about 300° C.

8. The method of claim 1 , wherein the phosphate esters are selected such that the lubricant does not burn at temperatures in the range of about 300° C. to about 600° C.

9. The method of claim 1 , further comprising the step of coating the workpiece with the lubricant.

10. The method of claim 1 wherein the method is carried out at an application temperature of about 300° C. to about 600° C.

11. The method of claim 1 wherein the method is carried out at an application temperature of 400° C. to 480° C.

12. The method of claim 1 wherein the hot forging apparatus is at a temperature of 400° C. to 480° C. when the coating of the lead-free lubricant is applied.

13. The method of claim 1 , the lubricant further comprising one or more metal-containing fatty acid derivatives.

14. The method of claim 1 , wherein the coating of lead-free lubricant is applied to the hot forging apparatus before inserting the workpiece into the apparatus and forging the article from the workpiece.

15. The method of claim 1 , wherein the coating of lead-free lubricant is applied to the workpiece before inserting the workpiece into the apparatus and forging an article from the workpiece.

16. The method of claim 1 , wherein the coating of lead-free lubricant is applied to both the hot forging apparatus and the workpiece before inserting the workpiece into the apparatus and forging an article from the workpiece.

17. The method of claim 1 , wherein the workpiece is inserted into the hot forging apparatus before simultaneously lubricating the workpiece and the hot forging apparatus, and forging the workpiece.

18. A method of hot forging an aluminum or aluminum alloy comprising the steps of a) applying a coating of a lead-free lubricant to one or both of a hot forging apparatus and a workpiece, inserting the workpiece into the apparatus and forging an article from the workpiece or b) inserting a workpiece into a hot forging apparatus, simultaneously lubricating the workpiece and the hot forging apparatus, and forging the workpiece, wherein the lead-free lubricant consists of:

15-40 weight % of one or more oils, including at least one mineral oil;

3-20 weight % fine graphite having a particle size distribution with about 90% of the particles below 15 microns in size;

30-80 weight % of one or more phosphate esters;

one or more metal-containing fatty acid derivatives; and

one or more dispersants.

19. The method of claim 18 wherein the method is carried out at an application temperature of about 300° C. to about 600° C.

20. The method of claim 18 wherein the method is carried out at an application temperature of 400° C. to 480° C.

21. The method of claim 18 wherein the hot forging apparatus is at a temperature of 400° C. to 480° C. when the coating of the lead-free lubricant is applied.

22. The method of claim 18 , wherein the coating of lead-free lubricant is applied to the hot forging apparatus before inserting the workpiece into the apparatus and forging the article from the workpiece.

23. The method of claim 18 , wherein the coating of lead-free lubricant is applied to the workpiece before inserting the workpiece into the apparatus and forging an article from the workpiece.

24. The method of claim 18 , wherein the coating of lead-free lubricant is applied to both the hot forging apparatus and the workpiece before inserting the workpiece into the apparatus and forging an article from the workpiece.

25. The method of claim 18 , wherein the workpiece is inserted into the hot forging apparatus before simultaneously lubricating the workpiece and the hot forging apparatus, and forging the workpiece.

Assignments (3)
CHANGE OF NAME Recorded Dec 3, 2008
From: HENKEL KGAA
To: HENKEL AG & CO. KGAA
Reel/Frame 022309/0718 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 19, 2008
From: NATIONAL STARCH AND CHEMICAL INVESTMENT HOLDING CORPORATION; INDOPCO, INC.
To: HENKEL KGAA
Reel/Frame 021912/0634 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2006
From: HUGUES, LAURENT; GANKEMA, HAROLD; HEIDEMAN, GEERT; KOK, DOUWE MARTEN; ODINK, GERKO
To: NATIONAL STARCH AND CHEMICAL INVESTMENT HOLDING CORP.
Reel/Frame 018495/0163 →