IP Library Granted Patent US 8,399,043
Granted Patent B2
US 8,399,043 · App. 12/280,244 · Granted Mar 19, 2013

Whey protein micelles

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Quick Facts
Patent No.
US 8,399,043
App. No.
12/280,244
Granted
Mar 19, 2013
Kind
B2
Abstract

The present invention relates to whey protein micelles, particularly to whey protein micelle concentrates or powders thereof and to a method for producing them. The present invention also pertains to the use of these micelles concentrates or powders thereof in nutrition and/or cosmetics and/or pharmaceutics.

Claims (22)

1. A process for the production of a whey protein micelles concentrate consisting of the steps of:

a. adjusting the pH of a demineralized whey protein aqueous solution to a value between 5.8 and 6.6 wherein the concentration of the whey protein aqueous solution is less than 12%, wherein if the whey protein aqueous solution comprises additional compounds, the amount of the additional compounds does not exceed 10% by weight of the total weight of the solution;

b. subjecting the aqueous solution to a temperature of between 80 and 89 C, wherein the heating is carried out for a time range of 10 s to 2 hours; and

c. concentrating a dispersion obtained in step b;

wherein in the concentrated dispersion, the proportion of micelles with an average size of between 100 nm and 700 nm is greater than 80%.

2. The process of claim 1 , wherein the whey protein aqueous solution concentration is less than 4%.

3. The process of claim 1 , wherein the aqueous solution is heated for a time of 15 minutes.

4. The process according to claim 1 , wherein the heating is performed by microwaves.

5. The process according to claim 1 , wherein the yield of micelles before concentration is at least 35%.

6. The process according to claim 5 , wherein the yield of micelles before concentration is at least 50%.

7. The process according to claim 5 , wherein the yield of micelles before concentration is at least 80%.

8. The process according to claim 1 , wherein the concentration is performed by a method selected from the group consisting of evaporation, centrifugation, sedimentation, ultrafiltration and microfiltration.

9. The process of claim 8 , wherein the centrifugation is performed after acidification to a pH of 4.5.

10. The process of claim 8 , wherein spontaneous sedimentation is performed at a pH of 4.5.

11. The process of claim 10 , wherein the sedimentation time is greater than 12 hours.

12. The process according to claim 1 , wherein the concentrating step includes spray-drying or freeze-drying the whey protein micelles concentrate.

13. The process of claim 12 , wherein the spray-drying or freeze-drying is performed with additional ingredients.

14. The process of claim 13 , wherein the additional ingredients are selected from the group consisting of soluble or non-soluble salts, peptides, protein hydrolysates, probiotic bacteria, strains, sugars, maltodextrins, fats, emulsifiers, sweeteners, aroma, plant extracts, ligands, bioactive agents, caffeine, vitamins, minerals, drugs, milk, milk proteins, skimmed milk powder, micellar casein, caseinate, vegetal protein, amino acids, polyphenols, pigment and mixtures thereof.

15. A method for preparing a product selected from the group consisting of nutritional, cosmetic, and pharmaceutical applications consisting of the steps of:

a. adjusting the pH of a demineralized whey protein aqueous solution to a value between 5.8 and 6.6, wherein the concentration of the whey protein aqueous solution is less than 12%, wherein if the whey protein aqueous solution comprises additional compounds, the amount of the additional compounds does not exceed 10% by weight of the total weight of the solution;

b. subjecting the aqueous solution to a temperature of between 80 and 89° C., wherein the heating is carried out for a time range of 10 s to 2 hours; and

c. concentrating a dispersion obtained in step b and using the concentrate to prepare the product.

Assignments (5)
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER 16062921 PREVIOUSLY RECORDED ON REEL 049391 FRAME 0756. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT NUMBER SHOULD HAVE BEEN 16062912. Recorded Jul 3, 2020
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 054082/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER 16062921 PREVIOUSLY RECORDED ON REEL 049391 FRAME 0756. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT NUMBER SHOULD HAVE BEEN 16062912. Recorded Jul 3, 2020
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 054082/0165 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ENGLISH TRANSLATION TO SHOW THE FULL AND CORRECT NEW NAME IN SECTION 51. PREVIOUSLY RECORDED AT REEL: 049391 FRAME: 0756. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER. Recorded Jun 13, 2019
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 049853/0398 →
MERGER Recorded Jun 6, 2019
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 049391/0756 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 8, 2008
From: BOVETTO, LIONEL JEAN RENE; SCHMITT, CHRISTOPHE; ROBIN, FREDERIC; POUZOT, MATTHIEU
To: NESTEC S.A.
Reel/Frame 021493/0324 →