IP Library Granted Patent US 8,226,895
Granted Patent B2
US 8,226,895 · App. 12/289,209 · Granted Jul 24, 2012

Reaction apparatus for producing trichlorosilane and method for producing trichlorosilane

Assignee: Mitsubishi Materials Corporation
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Quick Facts
Patent No.
US 8,226,895
App. No.
12/289,209
Granted
Jul 24, 2012
Kind
B2
Abstract

A reaction apparatus for producing trichlorosilane in which metal silicon powder M is reacted with hydrogen chloride gas, thus generating trichlorosilane, includes: an apparatus body into which the metal silicon powder is supplied; and an ejection port for ejecting the hydrogen chloride gas into the apparatus body from the bottom part of the apparatus body, wherein a plurality of holed pieces having a through hole penetrating in the thickness direction and a plurality of pellets interposed between these holed pieces are stacked in a mixed state on the upper side of the ejection port.

Claims (10)

1. A reaction apparatus for producing trichlorosilane in which metal silicon powder is reacted with hydrogen chloride gas to generate trichlorosilane, comprising:

an apparatus body into which the metal silicon powder is supplied;

an ejection port for ejecting the hydrogen chloride gas into the apparatus body, which is opened on the upper face of a partition plate partitioning the bottom part of the apparatus body;

a mixture layer disposed on the upper side of the ejection port in which a plurality of plate-shaped holed pieces having a through hole penetrating in the thickness direction and a plurality of ball members are stacked in a mixed state; and

metal silicon powder supplied on the upper side of the mixture layer,

wherein the ball members are interposed between the plate-shaped holed pieces, and

the ball members and the plate-shaped holed pieces are mixed so as to give a mixture ratio of W 1 /W 2 =0.5 to 5 where a weight of ball members is expressed as W 1 and a weight of the plate-shaped holed pieces is expressed as W 2 .

2. The reaction apparatus for producing trichlorosilane according to claim 1 , wherein the ball member has a diameter of 5 mm to 20 mm,

the holed piece is formed in a circular flat-plate shape, the holed piece is set to be from 4 mm to 20 mm in an outer diameter, and

the through hole is of such a dimension that no ball member is inserted therethrough.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 5, 2023
From: MITSUBISHI MATERIALS CORPORATION
To: HIGH-PURITY SILICON CORPORATION
Reel/Frame 063858/0867 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 16, 2009
From: INABA, CHIKARA
To: MITSUBISHI MATERIALS CORPORATION
Reel/Frame 022120/0303 →
Priority Claims (1)
JP P2007-277787 · Oct 25, 2007 · national
Continuity (1)
Related Publication 20090123359A1 · May 14, 2009