IP Library Granted Patent US 7,670,635
Granted Patent B2
US 7,670,635 · App. 12/370,528 · Granted Mar 2, 2010

Aerated frozen suspension with adjusted creaminess and scoop ability based on stress-controlled generation of superfine microstructures

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Quick Facts
Patent No.
US 7,670,635
App. No.
12/370,528
Granted
Mar 2, 2010
Kind
B2
Abstract

Products that are aerated multiphase systems containing an aqueous continuous fluid phase which may include solutes thus forming an aqueous syrup and disperse phases like gas/air cells, water ice crystals and solid/semi-solid fat globules or aggregates thereof, whereas the disperse phases are that finely structured that their mean diameters are below phase specific critical maximum values and thereby generate a most preferred by consumers, full rich silky-creamy mouth feel at much lower fat content than usual in conventional related products like premium and super premium ice creams.

Claims (16)

1. A method for imparting enhanced creaminess to an aerated frozen suspension, which comprises:

partially freezing a solution that includes a gas or air, a liquid watery fluid phase and a solid or semi-solid dispersed phase at a temperature of −10° C. to −18° C. in an extruder device under a shear force to form a partially frozen aerated suspension in which throughout the applied shear force over 55 to 80% of freezable water in the solution is converted to a frozen ice crystal state; and

subjecting the partially frozen aerated suspension to subsequent freezing to convert any remaining freezable water to a frozen ice crystal state and form a aerated frozen suspension that contains a superfine microstructure of ice crystals that imparts enhanced creaminess compared to an aerated frozen suspension made by partially freezing the same solution conventionally at a temperature of about −5° C. wherein less than 55% of freezable water in the solution is initially converted to a frozen ice crystal state.

2. The method of claim 1 , wherein the partial freezing is conducted by passing the solution through an extruder device at a temperature of −12° C. to −18° C.

3. The method of claim 1 , wherein at least 60% of the freezable water is converted to ice crystals throughout during the partial freezing.

4. The method of claim 1 , wherein the subsequent freezing is carried out in a hardening tunnel or a cold storage room at temperatures from −25° C. to −40° C.

5. The method of claim 1 , wherein about 60% of the freezable water is converted to ice crystals throughout during the partial freezing and about 40% of the freezable water is converted to ice crystals during the subsequent freezing.

6. The method of claim 1 , wherein about 70% of the freezable water is converted to ice crystals throughout the partial freezing and about 30% of the freezable water is converted to ice crystals during the subsequent freezing.

7. The method of claim 1 , wherein over 55 to 60% of the freezable water is converted to ice crystals throughout the partial freezing, and the subsequent freezing is conducted to first freeze an additional fraction of about 30 to 40% of the freezable water in a hardening tunnel at −40° C. and then freeze the remaining freezable water in a cold storage room at a temperature of −25° C. to −30° C.

8. The method of claim 1 , wherein 90% in number of the ice crystals have a diameter that is less than 50 to 60 microns, 90% in number of the air cells have a diameter that is less than 30 to 40 microns, and 90% in number of the fat agglomerates have a diameter that is less than 30 to 100 microns.

9. The method of claim 1 , wherein at least 50% in number of the ice crystals have a diameter that is between 5 and 30 microns, at least 50% in number of the air cells have a diameter of between 8 and 10 microns, and more than 20% in volume of the fat globules or agglomerates have a diameter that is between 2 to 20 microns.

10. The method of claim 1 , wherein the liquid watery fluid phase includes solutes and the dispersed phase includes gas/air cells, ice crystals and fat globules or aggregates.

11. The method of claim 1 , wherein the dispersed phase is finely structured with ice crystals having mean diameters that are below about 50-60 microns.

12. The method of claim 1 , wherein the superfine microstructure is created during the partial freezing step using shear stresses within the range of 2500 to 15000 Pa in an extruder device.

13. The method of claim 1 , wherein the creaminess of the product is defined by a loss modulus G″ in the range of 10 5 to 5×10 6 Pa in the state where at least 60% of the watery phase related to the freezable water fraction is frozen; and wherein the loss modulus G″ is measured in an oscillatory shear experiment at oscillation frequencies between 1 and 2 Hz at shear strain amplitudes in the linear viscoelastic range of the material where stress and strain are proportional.

14. The method of claim 13 , wherein the creaminess of the product is further defined by a loss modulus G″ is in the range of 300 to 5000 Pa in a totally melted state of the product at temperatures of +1 to +10° C.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER 16062921 PREVIOUSLY RECORDED ON REEL 049391 FRAME 0756. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT NUMBER SHOULD HAVE BEEN 16062912. Recorded Jul 3, 2020
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 054082/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER 16062921 PREVIOUSLY RECORDED ON REEL 049391 FRAME 0756. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT NUMBER SHOULD HAVE BEEN 16062912. Recorded Jul 3, 2020
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 054082/0165 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ENGLISH TRANSLATION TO SHOW THE FULL AND CORRECT NEW NAME IN SECTION 51. PREVIOUSLY RECORDED AT REEL: 049391 FRAME: 0756. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER. Recorded Jun 13, 2019
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 049853/0398 →
MERGER Recorded Jun 6, 2019
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 049391/0756 →