IP Library Granted Patent US 8,119,539
Granted Patent B2
US 8,119,539 · App. 12/502,582 · Granted Feb 21, 2012

Methods of fabricating oxide layers on silicon carbide layers utilizing atomic oxygen

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Quick Facts
Patent No.
US 8,119,539
App. No.
12/502,582
Granted
Feb 21, 2012
Kind
B2
Abstract

Methods of forming oxide layers on silicon carbide layers are disclosed, including placing a silicon carbide layer in a chamber such as an oxidation furnace tube that is substantially free of metallic impurities, heating an atmosphere of the chamber to a temperature of about 500° C. to about 1300° C., introducing atomic oxygen in the chamber, and flowing the atomic oxygen over a surface of the silicon carbide layer to thereby form an oxide layer on the silicon carbide layer. In some embodiments, introducing atomic includes oxygen providing a source oxide in the chamber and flowing a mixture of nitrogen and oxygen gas over the source oxide. The source oxide may comprise aluminum oxide or another oxide such as manganese oxide. Some methods include forming an oxide layer on a silicon carbide layer and annealing the oxide layer in an atmosphere including atomic oxygen.

Claims (17)

1. A method of forming an oxide layer on a silicon carbide layer, comprising:

placing a silicon carbide layer in a chamber;

placing an alumina wafer in the chamber;

heating an atmosphere of the chamber to a temperature of about 500° C. to about 1300° C.;

nitriding the alumina wafer to liberate atomic oxygen; and

flowing the atomic oxygen over a surface of the silicon carbide layer to form an oxide layer on the silicon carbide layer.

2. The method of claim 1 , wherein heating an atmosphere of the chamber comprises heating an atmosphere of the chamber to a temperature of about 1000° C. to about 1100° C.

3. The method of claim 1 , further comprising flowing oxygen gas over the alumina wafer.

4. A method of forming an oxide layer on a silicon carbide layer, comprising:

placing a silicon carbide layer in a chamber;

placing an alumina wafer in the chamber;

heating an atmosphere of the chamber to a temperature of about 500° C. to about 1300° C.;

nitriding the alumina wafer to liberate first atomic oxygen;

reacting the first atomic oxygen with oxygen gas to produce ozone;

cracking the ozone to produce second atomic oxygen in the vicinity of the silicon carbide layer; and

flowing the second atomic oxygen over a surface of the silicon carbide layer to form an oxide layer on the silicon carbide layer.

5. The method of claim 1 , wherein a major surface of the alumina wafer is parallel to a major surface of the silicon carbide layer.

Assignments (6)
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY COLLATERAL AT REEL/FRAME NO. 64185/0755 Recorded Sep 30, 2025
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: WOLFSPEED, INC.
Reel/Frame 072989/0001 →
NOTICE OF GRANT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Sep 30, 2025
From: WOLFSPEED, INC.
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 072992/0113 →
NOTICE OF GRANT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Sep 30, 2025
From: WOLFSPEED, INC.
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 072992/0381 →
NOTICE OF GRANT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Sep 30, 2025
From: WOLFSPEED, INC.
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 072992/0467 →
NOTICE OF GRANT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Sep 30, 2025
From: WOLFSPEED, INC.
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 072992/0588 →
SECURITY INTEREST Recorded Jun 30, 2023
From: WOLFSPEED, INC.
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION
Reel/Frame 064185/0755 →