Differential scanning calorimeter
View Patent ↗The differential scanning calorimeter includes: a heat sink, which stores a measuring sample and a reference material; a heater, which heats the heat sink; a cooling block, which is separated away from the heat sink, and positioned below the heat sink; a thermal resistor, which is connected between the heat sink and the cooling block, and forms a heat flow path therebetween; a cooling head, which is detachably fitted to the cooling block, and is cooled by an external cooling device; and differential heat flow detectors, which output a temperature difference between the measuring sample and the reference material as a heat-flow-difference signal, in which: the cooling block forms a side wall to fit the bore of the cooling head outward from the joint of the thermal resistance body; the top surface of the cooling head is lower than the joint.
1. A differential scanning calorimeter, comprising:
a heat sink, which stores a measuring sample and a reference material;
a heater, which heats the heat sink;
a cooling block, which is separated away from the heat sink, and is positioned below the heat sink;
a thermal resistor, which is connected between the heat sink and the cooling block, and forms a heat flow path therebetween;
a cooling head, which is provided with an inner hole for allowing the cooling head to be detachably fitted to the cooling block, and is cooled by an external cooling device; and
differential heat flow detectors, which output a temperature difference between the measuring sample and the reference material as a heat-flow-difference signal, wherein:
the cooling block has a side wall, which is formed on an outside of a connected portion connected to the thermal resistor, and is fitted to the inner hole; and
the cooling head is arranged so that an upper surface thereof is positioned flush with or below the connected portion.
2. A differential scanning calorimeter according to claim 1 , wherein the side wall comprises an outer peripheral surface of a protruding portion protruding upward or downward from the cooling block.
3. A differential scanning calorimeter according to claim 2 , wherein:
in one of an upper surface and a lower surface of the cooling block, an annular groove is formed, the annular groove being sectioned by the protruding portion and an outer peripheral ring surrounding the protruding portion from an outside thereof with the annular groove therebetween; and
the cooling head is housed in the annular groove and the protruding portion is fitted into the inner hole.