Method for production of high purity copper sulfate
View Patent ↗High purity copper sulfate having a purity of 99.99% or higher and in which the content of transition metals such as Fe, Cr, Ni is 3 wtppm or less is provided. A method for producing such high purity copper sulfate includes the steps of dissolving copper sulfate crystals in purified water, performing evaporative concentration thereto, removing the crystals precipitated initially, performing further evaporative concentration to effect crystallization, and subjecting this to filtration to obtain high purity copper sulfate. This manufacturing method of high purity copper sulfate allows the efficient removal of impurities from commercially available copper sulfate crystals at a low cost through dissolution with purified water and thermal concentration.
1. A method of manufacturing copper sulfate having a purity of 99.99 wt % or higher and a content of transition metals such as Fe, Cr, and Ni of 3 wtppm or less, comprising the steps of dissolving copper sulfate crystals in purified water, performing evaporative concentration thereto, removing crystals precipitated initially, performing further evaporative concentration to effect crystallization, subjecting this to filtration to obtain high purity copper sulfate, and performing desiccation thereto.
2. A method according to claim 1 , wherein the initial pH of the solution in which the copper sulfate was dissolved in purified water is 2 to 4, and the pH of the solution after removing the crystals precipitated initially is 2 or less.
3. A method according to claim 2 , wherein 10 wt % or more of the initial crystals is removed in relation to an initial input.
4. A method according to claim 3 , wherein after the filtration, a remaining filtration solution is 2 to 40% of an original fluid volume.
5. A method according to claim 4 , wherein desiccation temperature is 40 to 100° C.
6. A method according to claim 1 , wherein 10 wt % or more of the initial crystals is removed in relation to an initial input.
7. A method according to claim 1 , wherein after the filtration, a remaining filtration solution is 2 to 40% of an original fluid volume.
8. A method according to claim 1 , wherein desiccation temperature is 40 to 100° C.