IP Library Granted Patent US 9,567,988
Granted Patent B2
US 9,567,988 · App. 12/936,129 · Granted Feb 14, 2017

Cryogenic pump employing tin—gallium alloys and methods of use

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Quick Facts
Patent No.
US 9,567,988
App. No.
12/936,129
Granted
Feb 14, 2017
Kind
B2
Abstract

A cryogenic refrigerator includes a regenerative heat exchanger material in thermal contact with a working gas including a tin-antimony (Sn—Sb) alloy or a tin-gallium (Sn—Ga) alloy in at least one cooling stage. The regenerative heat exchanger material can include an Sn—Sb-M alloy, with M including at least one element selected from the group consisting of Bi, Ag, Ge, Cu, La, Mg, Mn, Nd, Ni, Pd, Pt, K, Rh, Sm, Se, S, Y, Fe, In, Al, Ce, Dy, Cd, Ti, Au, P, Pr, Yb and Zn. The cryogenic refrigerator can include a Gifford-McMahon refrigerator, a pulse tube refrigerator, or a Stirling refrigerator. A cryopump includes cryopanels adapted to condense or adsorb gases and a cryogenic refrigerator.

Claims (8)

1. A cryogenic refrigerator comprising at least one cooling stage having a regenerative heat exchanger material in thermal contact with a working gas, including a binary tin-gallium (Sn—Ga) alloy in the at least one cooling stage.

2. The cryogenic refrigerator of claim 1 , wherein the cryogenic refrigerator is selected from the group consisting of a Gifford-McMahon cryogenic refrigerator, a pulse tube cryogenic refrigerator, and a Stirling cryogenic refrigerator.

3. The cryogenic refrigerator of claim 1 , wherein the Sn—Ga alloy comprises a maximum of 3.9% gallium by weight.

4. The cryogenic refrigerator of claim 1 , further including a cryopump that includes at least one cryopanel cooled by the refrigerator and adapted to condense or adsorb gases.

5. The cryogenic refrigerator of claim 1 , wherein the at least one cooling stage includes at least two layers of regenerative heat exchanger material.

6. The cryogenic refrigerator of claim 5 , wherein at least one layer includes the binary tin-gallium (Sn—Ga) alloy and at least one layer includes at least one rare earth element.

7. The cryogenic refrigerator of claim 5 , wherein at least one layer includes the binary tin-gallium (Sn—Ga) alloy and at least one layer includes a rare earth intermetallic compound of one or more rare earth elements with a non-rare earth metal.

8. The cryogenic refrigerator of claim 5 , wherein at least one layer includes the binary tin-gallium (Sn—Ga) alloy and at least one layer includes a solid solution alloy of rare earth elements.

Assignments (6)
RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 038891/0765 Recorded Nov 4, 2025
From: WELLS FARGO BANK, NATIONAL ASSOCIATION
To: AZENTA, INC. (F/K/A BROOKS AUTOMATION, INC.); AZENTA USA, INC. (F/K/A BIOSTORAGE TECHNOLOGIES, INC.)
Reel/Frame 073446/0080 →
RELEASE OF SECURITY INTEREST Recorded Jul 2, 2019
From: MORGAN STANLEY SENIOR FUNDING, INC.
To: BROOKS AUTOMATION, INC.; BIOSTORAGE TECHNOLOGIES, INC.
Reel/Frame 049669/0578 →
PARTIAL RELEASE OF SECURITY INTEREST IN SPECIFIED PATENTS AND SPECIFIED TRADEMARKS Recorded Jul 1, 2019
From: WELLS FARGO BANK, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: BROOKS AUTOMATION, INC.; BIOSTORAGE TECHNOLOGIES, INC.
Reel/Frame 049643/0411 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 1, 2019
From: BROOKS AUTOMATION, INC.
To: EDWARDS VACUUM LLC
Reel/Frame 049648/0016 →
SECURITY INTEREST Recorded Oct 6, 2017
From: BROOKS AUTOMATION, INC.; BIOSTORAGE TECHNOLOGIES, INC.
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 044142/0258 →
SECURITY AGREEMENT Recorded May 31, 2016
From: BROOKS AUTOMATION, INC.; BIOSTORAGE TECHNOLOGIES
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 038891/0765 →