Method of manufacturing a Ni-Pt alloy
View Patent ↗A Ni—Pt alloy and target superior in workability containing 0.1 to 20 wt % Pt and having a Vickers hardness of 40 to 90. A method of manufacturing the Ni—Pt alloy comprises steps of subjecting a raw material Ni having a purity of 3N level to electrochemical dissolution, neutralizing the electrolytically leached solution with ammonia, removing impurities through filtration with activated carbon, blowing carbon dioxide into the resultant solution to form nickel carbonate, exposing the resultant product to a reducing atmosphere to prepare high purity Ni powder, leaching a raw material Pt having a purity of 3N level with acid, subjecting the leached solution to electrolysis to prepare high purity electrodeposited Pt, and dissolving the resultant high purity Ni powder and high purity electrodeposited Pt. The method enables rolling of the Ni—Pt alloy ingot upon reducing the hardness thereof, which results in the stable and efficient manufacture of a rolled target.
1. A method of manufacturing a Ni—Pt alloy superior in workability, comprising the steps of:
subjecting a raw material Ni having a purity of 3N level to electrolytical dissolution to obtain a solution containing Ni;
neutralizing the solution containing Ni with ammonia to obtain a neutralized solution;
removing impurities by filtering the neutralized solution with activated carbon to obtain a filtered solution;
blowing carbon dioxide into the filtered solution to form nickel carbonate;
exposing the nickel carbonate to a reducing atmosphere to prepare high purity Ni powder;
dissolving a raw material Pt having a purity of 3N level into acid to obtain a solution containing Pt;
subjecting the solution containing Pt to electrolysis to prepare high purity electrodeposited Pt; and
melting the high purity Ni powder together with the high purity electrodeposited Pt to obtain the Ni-Pt alloy.
2. A method according to claim 1 , wherein the Ni—Pt alloy has a purity of 99.99% or higher.
3. A method according to claim 2 , wherein the Ni—Pt alloy has Pt in a content of 0.1 to 20 wt % and has a Vickers hardness of 40 to 90.
4. A method according to claim 3 , further comprising the step of manufacturing a Ni—Pt alloy sputtering target from the high purity Ni powder and high purity electrodeposited Pt after said melting step.
5. A method according to claim 1 , wherein the Ni—Pt alloy has Pt in a content of 0.1 to 20 wt % and has a Vickers hardness of 40 to 90.
6. A method according to claim 5 , further comprising the step of manufacturing a Ni—Pt alloy sputtering target from the high purity Ni powder and high purity electrodeposited Pt after said melting step.
7. A method according to claim 1 , further comprising the step of manufacturing a Ni—Pt alloy sputtering target from the high purity Ni powder and high purity electrodeposited Pt after said melting step.