IP Library Granted Patent US 9,168,265
Granted Patent B2
US 9,168,265 · App. 13/714,052 · Granted Oct 27, 2015

Tetracycline derivatives with reduced antibiotic activity and neuroprotective benefits

Inventors: Iain W. Duncan (Seattle, WA); Edward A. Kesicki (Bothwell, WA); Carl G. Osborne (Jacksonville, FL); William D. Schwieterman (Mobile, AL); Irina Jacobson (Sammamish, WA)
A61K31/65A61K31/423A61K31/536A61K45/06C07C233/58C07C323/60C07D263/52C07D263/62C07D265/34C07D498/10C07C2103/46
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Quick Facts
Patent No.
US 9,168,265
App. No.
13/714,052
Granted
Oct 27, 2015
Kind
B2
Abstract

The present disclosure is directed to compositions and methods which utilize the tetracycline scaffold, preferably the scaffold of tetracycline or minocycline, and which significantly lack antibiotic activity. The compounds have neuroprotective attributes without interfering with the drugs capacity to pass through the blood brain barrier. These compounds have neuroprotective activity because of their inhibition of neuronal cell cycle progression. The compounds are characterized in part by a fifth ring joining positions 9 and 10.

Claims (13)

1. A compound having the formula:

where R 4 , R 6 R 9 , and R 10 are defined as follows:

R 4 is a substitution selected from the group consisting of —N(CH 3 ) 2 , N(CH 3 ) 2 , NH(CH 2 CH 2 OH), and amino alkyl, or else R 4 is a disubstitution selected from the group consisting of (i) a first substitution of —N(CH 3 ) 2 and a second substitution of substituted alkyl, and (ii) a first substitution of amino alkyl and a second substitution of lower alkyl;

R 6 is H or —CH 2 S—R″, where R″ is aryl or substituted aryl; and

either R 9 is H and R 10 is OH or lower alkyl, or else

R 10 and R 9 taken together have the formula (from R 10 -R 9 ) (a) —O—Y—HN—, where Y is CH and the bond Y—N is double, (b) —O—Y—HN—, where Y is C═O, or (c) —O—CH 2 —C(═O)—HN—;

or a pharmaceutically acceptable salt thereof,

with the proviso that when R 9 is H and R 10 is OH or lower alkyl, R 6 is not H.

2. The compound of claim 1 , where R 4 is NH(CH 2 CH 2 OH) or N(CH 3 ) 2 .

3. The compound of claim 2 , where the compound is an up epimer at R 4 .

4. The compound of claim 1 , where R 4 is the disubstitution.

5. The compound of claim 1 , where R 6 is a substitutent that reduces antibiotic potency.

6. The compound of claim 1 , where R″ at R 6 is benzyl or phenyl.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 12, 2013
From: DUNCAN, IAIN W.; KESICKI, EDWARD A.; OSBORNE, CARL G.; SCHWIETERMAN, WILLIAM D.; JACOBSON, IRINA
To: NEUMEDICS
Reel/Frame 029798/0456 →
Continuity (3)
Continuation 12501202 · Jul 10, 2009
Provisional Application 61080114 · Jul 11, 2008
Related Publication 20130123217A1 · May 16, 2013