IP Library Granted Patent US 9,145,616
Granted Patent B2
US 9,145,616 · App. 13/775,167 · Granted Sep 29, 2015

Method of preventing silver tarnishing

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Quick Facts
Patent No.
US 9,145,616
App. No.
13/775,167
Granted
Sep 29, 2015
Kind
B2
Abstract

A thin indium metal layer is electroplated onto silver to prevent silver tarnishing. The indium and silver composite has high electrical conductivity.

Claims (12)

1. A method comprising:

a) providing a substrate comprising a silver layer;

b) providing an indium electroplating bath consisting of one or more sources of indium ions, indium ions in amounts of 0.5 g/L to 6 g/L, one or more acids or salts thereof selected from the group consisting of alkane sulfonic acids, aryl sulfonic acids and sulfamic acid, one or more hydrogen suppressing epihalohydrin copolymers, the one or more hydrogen suppressing epihalohydrin copolymers are composed of an epihalohydrin and one or more nitrogen-containing organic compounds, and water, a pH of the indium electroplating bath is from 0 to 5;

c) immersing the substrate in the indium electroplating bath; and

d) electroplating an indium metal layer adjacent the silver layer to form an indium and silver composite on the substrate, the composite has a contact resistance of 5 mOhms or less.

2. The method of claim 1 , wherein heat is not applied to the indium and silver composite.

3. The method of claim 1 , wherein the contact resistance is 1-5 mOhms.

4. The method of claim 1 , wherein the indium metal layer has a thickness of 0.5-50 nm.

5. The method of claim 4 , wherein the indium metal layer has a thickness of 10-20 nm.

6. The method of claim 5 , wherein the indium metal layer has a thickness of 10-15 nm.

7. The method of claim 1 , wherein the substrate is chosen from jewelry and an electronic component.

8. The method of claim 1 , wherein the indium ions are in amounts of 0.5 g/L to 3 g/L.

Assignments (4)
SECURITY INTEREST Recorded Nov 3, 2025
From: QNITY ELECTRONICS, INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 073515/0243 →
SECURITY INTEREST Recorded Nov 3, 2025
From: QNITY ELECTRONICS, INC.
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 073517/0298 →
CHANGE OF NAME Recorded Oct 29, 2024
From: ROHM & HAAS ELECTRONIC MATERIALS LLC
To: DUPONT ELECTRONIC MATERIALS INTERNATIONAL, LLC
Reel/Frame 069272/0383 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 15, 2015
From: FOYET, ADOLPHE; ZHANG-BEGLINGER, WAN; TOBEN, MICHAEL P; GUEBEY, JONAS
To: ROHM AND HAAS ELECTRONIC MATERIALS LLC
Reel/Frame 036094/0170 →