IP Library Granted Patent US 9,590,063
Granted Patent B2
US 9,590,063 · App. 14/576,537 · Granted Mar 7, 2017

Method and structure for a large-grain high-K dielectric

Inventor: Rama I. Hegde (Austin, TX)
Assignee: NXP USA, INC.
H01L29/42364H01L21/0228H01L21/02181H01L21/28194H01L21/28556H01L29/517
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Quick Facts
Patent No.
US 9,590,063
App. No.
14/576,537
Granted
Mar 7, 2017
Kind
B2
Abstract

A method of forming a semiconductor device ( 100 ) includes depositing a metal oxide ( 104 ) over the substrate ( 102 ). The depositing includes combining a first metal and oxygen to form the metal oxide having grains and further adding a catalyst during the combining. The catalyst causes the grains to be bigger than would occur in the absence of the catalyst. A conductive layer ( 202 ) is formed over the metal oxide.

Claims (24)

1. A method of forming a semiconductor device using a substrate, comprising:

depositing a metal oxide over the substrate, the depositing comprising combining a first metal and oxygen to form the metal oxide having grains and further adding a catalyst during the combining, wherein the catalyst causes the grains to be bigger than would occur in the absence of the catalyst; and

forming a conductive layer over the metal oxide, the conductive layer comprising a second metal different from the first metal.

2. The method of claim 1 , wherein the first metal comprises hafnium.

3. The method of claim 2 , wherein the catalyst comprises nickel.

4. The method of claim 3 , wherein a concentration of the hafnium in the metal oxide exceeds a concentration of the nickel in the metal oxide by at least a factor of ten thousand.

5. The method of claim 1 , wherein the first metal has a first concentration in the metal oxide and the catalyst has a second concentration in the metal oxide, wherein the first concentration is at least 10 thousand times greater than the second concentration.

6. The method of claim 1 , wherein the combining the first metal and the oxygen comprises combining a precursor comprising the first metal with water.

7. The method of claim 6 , wherein the water is further characterized as being heavy water.

8. The method of claim 1 , wherein the grains have an average lateral dimension, further comprising:

patterning the conductive layer to form a gate having a gate length, wherein the gate length is less than the average lateral dimension.

9. The method of claim 8 , wherein the average lateral dimension is at least four times greater than the gate length.

10. The method of claim 1 wherein:

the first metal comprises hafnium; and

the catalyst comprises one of a group consisting of nickel, platinum, iron, and germanium.

11. The method of claim 10 , wherein the adding a catalyst comprises adding a precursor that comprises components additional to the one of the group consisting of nickel, platinum, iron, and germanium.

12. The method of claim 1 , wherein the depositing is further characterized as performing atomic layer deposition of a plurality of layers wherein at least one layer of the plurality of layers comprises the catalyst and at least one layer of the plurality of layers is free of the catalyst.

13. A method of forming a semiconductor device using a substrate, comprising:

using atomic layer deposition to form a first layer over the substrate, wherein the first layer comprises a first metal and oxygen; and

using atomic layer deposition to form a second layer over the substrate, wherein the second layer comprises the first metal, oxygen, and a catalyst, wherein the catalyst comprises one of a group consisting of nickel, platinum, iron, and germanium; and

forming a conductive layer over the second layer, the conductive layer comprising a second metal different from the first metal.

14. The method of claim 13 , wherein:

the first metal comprises hafnium; and

the catalyst comprises nickel.

Assignments (15)
CORRECTIVE ASSIGNMENT TO CORRECT THE REMOVE APPLICATION 11759915 AND REPLACE IT WITH APPLICATION 11759935 PREVIOUSLY RECORDED ON REEL 040925 FRAME 0001. ASSIGNOR(S) HEREBY CONFIRMS THE RELEASE OF SECURITY INTEREST. Recorded Feb 17, 2020
From: MORGAN STANLEY SENIOR FUNDING, INC.
To: NXP, B.V. F/K/A FREESCALE SEMICONDUCTOR, INC.
Reel/Frame 052917/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE REMOVE APPLICATION 11759915 AND REPLACE IT WITH APPLICATION 11759935 PREVIOUSLY RECORDED ON REEL 040928 FRAME 0001. ASSIGNOR(S) HEREBY CONFIRMS THE RELEASE OF SECURITY INTEREST. Recorded Jan 17, 2020
From: MORGAN STANLEY SENIOR FUNDING, INC.
To: NXP B.V.
Reel/Frame 052915/0001 →
RELEASE OF SECURITY INTEREST Recorded Sep 10, 2019
From: MORGAN STANLEY SENIOR FUNDING, INC.
To: NXP B.V.
Reel/Frame 050744/0097 →
CORRECTIVE ASSIGNMENT TO CORRECT THE NATURE OF CONVEYANCE PREVIOUSLY RECORDED AT REEL: 040626 FRAME: 0683. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER AND CHANGE OF NAME EFFECTIVE NOVEMBER 7, 2016. Recorded Jan 12, 2017
From: NXP SEMICONDUCTORS USA, INC. (MERGED INTO); FREESCALE SEMICONDUCTOR, INC. (UNDER)
To: NXP USA, INC.
Reel/Frame 041414/0883 →
CHANGE OF NAME Recorded Nov 16, 2016
From: FREESCALE SEMICONDUCTOR INC.
To: NXP USA, INC.
Reel/Frame 040626/0683 →
RELEASE OF SECURITY INTEREST Recorded Nov 7, 2016
From: MORGAN STANLEY SENIOR FUNDING, INC.
To: NXP B.V.
Reel/Frame 040928/0001 →
RELEASE OF SECURITY INTEREST Recorded Sep 21, 2016
From: MORGAN STANLEY SENIOR FUNDING, INC.
To: NXP, B.V., F/K/A FREESCALE SEMICONDUCTOR, INC.
Reel/Frame 040925/0001 →
SUPPLEMENT TO THE SECURITY AGREEMENT Recorded Jun 16, 2016
From: FREESCALE SEMICONDUCTOR, INC.
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 039138/0001 →
ASSIGNMENT AND ASSUMPTION OF SECURITY INTEREST IN PATENTS Recorded Jan 5, 2016
From: CITIBANK, N.A.
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 037444/0535 →
ASSIGNMENT AND ASSUMPTION OF SECURITY INTEREST IN PATENTS Recorded Jan 5, 2016
From: CITIBANK, N.A.
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 037444/0444 →
PATENT RELEASE Recorded Dec 21, 2015
From: CITIBANK, N.A., AS COLLATERAL AGENT
To: FREESCALE SEMICONDUCTOR, INC.
Reel/Frame 037358/0001 →
SUPPLEMENT TO IP SECURITY AGREEMENT Recorded Feb 18, 2015
From: FREESCALE SEMICONDUCTOR, INC.
To: CITIBANK, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 035033/0923 →
SUPPLEMENT TO IP SECURITY AGREEMENT Recorded Feb 18, 2015
From: FREESCALE SEMICONDUCTOR, INC.
To: CITIBANK, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 035034/0019 →
SUPPLEMENT TO IP SECURITY AGREEMENT Recorded Feb 18, 2015
From: FREESCALE SEMICONDUCTOR, INC.
To: CITIBANK, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 035033/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 19, 2014
From: HEGDE, RAMA I.
To: FREESCALE SEMICONDUCTOR, INC.
Reel/Frame 034555/0441 →
Continuity (1)
Related Publication 20160181158A1 · Jun 23, 2016